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An Fe(III) complex with the dianionic form of 2,6-diacetylpyridine bis(acylhydrazone). The crystal structure of [diaqua-2 ',2 ''-(2,6-pyridinediyldiethylidyne)dioxamo-hydrazide]iron(III) perchlorate trihydrate, [Fe(dapsox)(H2O)(2)]ClO4 center dot 3H(2)O
(Taylor & Francis Ltd, Abingdon, 2002)
The title compound was prepared by a template synthesis from 2,6-diacetylpyridine, dioxamohydrazide and Fe(ClO4)(3) . 6H(2)O (mol ratio 1: 2: 1) in MeOH/H2O (3:1) solution and its structure determined by single-crystal ...