Improving the synthesis process of tribological materials based on tin sulphides by adding graphite as additive
Само за регистроване кориснике
2019
Аутори
Gajić, NatašaKamberović, Željko
Anđić, Zoran
Korać, Marija
Trpčevská, Jarmila
Stamatović, Mirko
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
The aim of this research was to study the effect of graphite addition in the process of synthesis of tribological materials based on tin sulphides. The tin sulphides powders were synthesized from selected precursors by pyrometallurgical method in rotary tilting tube furnace. The thermodynamic parameters of the synthesis were determined using HSC Chemistry software modelling package. In addition, the synthesis process was also characterized by the thermal analysis method: simultaneous differential scanning calorimetry and thermogravimetry (DCS-TGA). The characterization of the synthesized tin sulphides powders included analysis of chemical composition by optical emission spectroscopy, phase composition identification by X-ray diffraction (XRD) and examination of morphology, as well as elemental composition by scanning electron microscopy (SEM) with energy-dispersive spectroscopy (EDS). The hexagonal SnS2 and orthorhombic Sn2S3 phases were formed after the thermal treatment of starting p...owders in nitrogen atmosphere. The obtained results indicate the positive effects of the graphite addition which enables the synthesis of tin sulphide powders with appropriate content of sulphide phases with minimal loss of sulphur.
Кључне речи:
Graphite / Pyrometallurgical / Tin sulphide / TribologyИзвор:
Journal of the Serbian Chemical Society, 2019, 84, 4, 423-433Издавач:
- Journal of the Serbian Chemical Society
Финансирање / пројекти:
- Иновативна синергија нус-продуката, минимизације отпада и чистије производње у металургији (RS-MESTD-Technological Development (TD or TR)-34033)
DOI: 10.2298/JSC180628102G
ISSN: 0352-5139
WoS: 000466010400008
Scopus: 2-s2.0-85069298169
Колекције
Институција/група
Hemijski fakultet / Faculty of ChemistryTY - JOUR AU - Gajić, Nataša AU - Kamberović, Željko AU - Anđić, Zoran AU - Korać, Marija AU - Trpčevská, Jarmila AU - Stamatović, Mirko PY - 2019 UR - https://cherry.chem.bg.ac.rs/handle/123456789/3289 AB - The aim of this research was to study the effect of graphite addition in the process of synthesis of tribological materials based on tin sulphides. The tin sulphides powders were synthesized from selected precursors by pyrometallurgical method in rotary tilting tube furnace. The thermodynamic parameters of the synthesis were determined using HSC Chemistry software modelling package. In addition, the synthesis process was also characterized by the thermal analysis method: simultaneous differential scanning calorimetry and thermogravimetry (DCS-TGA). The characterization of the synthesized tin sulphides powders included analysis of chemical composition by optical emission spectroscopy, phase composition identification by X-ray diffraction (XRD) and examination of morphology, as well as elemental composition by scanning electron microscopy (SEM) with energy-dispersive spectroscopy (EDS). The hexagonal SnS2 and orthorhombic Sn2S3 phases were formed after the thermal treatment of starting powders in nitrogen atmosphere. The obtained results indicate the positive effects of the graphite addition which enables the synthesis of tin sulphide powders with appropriate content of sulphide phases with minimal loss of sulphur. PB - Journal of the Serbian Chemical Society T2 - Journal of the Serbian Chemical Society T1 - Improving the synthesis process of tribological materials based on tin sulphides by adding graphite as additive VL - 84 IS - 4 SP - 423 EP - 433 DO - 10.2298/JSC180628102G ER -
@article{ author = "Gajić, Nataša and Kamberović, Željko and Anđić, Zoran and Korać, Marija and Trpčevská, Jarmila and Stamatović, Mirko", year = "2019", abstract = "The aim of this research was to study the effect of graphite addition in the process of synthesis of tribological materials based on tin sulphides. The tin sulphides powders were synthesized from selected precursors by pyrometallurgical method in rotary tilting tube furnace. The thermodynamic parameters of the synthesis were determined using HSC Chemistry software modelling package. In addition, the synthesis process was also characterized by the thermal analysis method: simultaneous differential scanning calorimetry and thermogravimetry (DCS-TGA). The characterization of the synthesized tin sulphides powders included analysis of chemical composition by optical emission spectroscopy, phase composition identification by X-ray diffraction (XRD) and examination of morphology, as well as elemental composition by scanning electron microscopy (SEM) with energy-dispersive spectroscopy (EDS). The hexagonal SnS2 and orthorhombic Sn2S3 phases were formed after the thermal treatment of starting powders in nitrogen atmosphere. The obtained results indicate the positive effects of the graphite addition which enables the synthesis of tin sulphide powders with appropriate content of sulphide phases with minimal loss of sulphur.", publisher = "Journal of the Serbian Chemical Society", journal = "Journal of the Serbian Chemical Society", title = "Improving the synthesis process of tribological materials based on tin sulphides by adding graphite as additive", volume = "84", number = "4", pages = "423-433", doi = "10.2298/JSC180628102G" }
Gajić, N., Kamberović, Ž., Anđić, Z., Korać, M., Trpčevská, J.,& Stamatović, M.. (2019). Improving the synthesis process of tribological materials based on tin sulphides by adding graphite as additive. in Journal of the Serbian Chemical Society Journal of the Serbian Chemical Society., 84(4), 423-433. https://doi.org/10.2298/JSC180628102G
Gajić N, Kamberović Ž, Anđić Z, Korać M, Trpčevská J, Stamatović M. Improving the synthesis process of tribological materials based on tin sulphides by adding graphite as additive. in Journal of the Serbian Chemical Society. 2019;84(4):423-433. doi:10.2298/JSC180628102G .
Gajić, Nataša, Kamberović, Željko, Anđić, Zoran, Korać, Marija, Trpčevská, Jarmila, Stamatović, Mirko, "Improving the synthesis process of tribological materials based on tin sulphides by adding graphite as additive" in Journal of the Serbian Chemical Society, 84, no. 4 (2019):423-433, https://doi.org/10.2298/JSC180628102G . .