Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia
Authors
Pantović Spajić, KatarinaSakan, Sanja M.
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Đorđević, Dragana S.
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Šoštarić, Tatjana D.
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Lopičić, Zorica
Janićijević, Aleksandra
Stojanović, Ksenija A.
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Article (Published version)
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The purpose of this paper was to investigate the effectiveness of three different extraction agents for the extraction of 25 elements from sediment samples collected from 4 artificial lakes and 12 rivers in Serbia (33 samples in total). The extraction efficiency of the agents was evaluated by its ability to extract the highest quantity of the elements. For that purpose, three acids (1M HCl, 2M HNO3 and 0.43M CH3COOH) have been used. Inductively coupled plasma atomic emission spectrometry (ICP-OES) was used for quantitative determination of following elements: Al, As, B, Ba, Be, Bi, Ca, Cd, Cr, Co, Cu, Fe, Hg, K, Li, Mg, Mn, Ni, Na, Pb, Sb, Se, Sr, V, and Zn. The extraction with 1M HCl has shown the best results for the majority of investigated elements (especially Sr, Mn and Ca). Antimony (Sb) was detected only after extraction with 0.43M CH3COOOH, while selenium (Se) could not be detected when 2M HNO3 was applied as extraction agents. The present study could be very useful for choosin...g a suitable method for specific elements and also can be helpful in the evaluation of the contaminants in freshwater sediments in Serbia. This might contribute to environmental risk assessment of the present elements.
Keywords:
Metals / Extraction agents / Lake sediments / RiverSource:
Acta Periodica Technologica, 2019, 50, 189-196Funding / projects:
- The study of physicochemical and biochemical processes in living environment that have impacts on pollution and the investigation of possibilities for minimizing the consequences (RS-MESTD-Basic Research (BR or ON)-172001)
- Developing technological processes for nonstandard copper concentrates processing with the aim to decrease pollutants emission (RS-MESTD-Technological Development (TD or TR)-34023)
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Hemijski fakultet / Faculty of ChemistryTY - JOUR AU - Pantović Spajić, Katarina AU - Sakan, Sanja M. AU - Đorđević, Dragana S. AU - Šoštarić, Tatjana D. AU - Lopičić, Zorica AU - Janićijević, Aleksandra AU - Stojanović, Ksenija A. PY - 2019 UR - https://cherry.chem.bg.ac.rs/handle/123456789/3854 AB - The purpose of this paper was to investigate the effectiveness of three different extraction agents for the extraction of 25 elements from sediment samples collected from 4 artificial lakes and 12 rivers in Serbia (33 samples in total). The extraction efficiency of the agents was evaluated by its ability to extract the highest quantity of the elements. For that purpose, three acids (1M HCl, 2M HNO3 and 0.43M CH3COOH) have been used. Inductively coupled plasma atomic emission spectrometry (ICP-OES) was used for quantitative determination of following elements: Al, As, B, Ba, Be, Bi, Ca, Cd, Cr, Co, Cu, Fe, Hg, K, Li, Mg, Mn, Ni, Na, Pb, Sb, Se, Sr, V, and Zn. The extraction with 1M HCl has shown the best results for the majority of investigated elements (especially Sr, Mn and Ca). Antimony (Sb) was detected only after extraction with 0.43M CH3COOOH, while selenium (Se) could not be detected when 2M HNO3 was applied as extraction agents. The present study could be very useful for choosing a suitable method for specific elements and also can be helpful in the evaluation of the contaminants in freshwater sediments in Serbia. This might contribute to environmental risk assessment of the present elements. T2 - Acta Periodica Technologica T1 - Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia VL - 50 SP - 189 EP - 196 DO - 10.2298/APT1950189P ER -
@article{ author = "Pantović Spajić, Katarina and Sakan, Sanja M. and Đorđević, Dragana S. and Šoštarić, Tatjana D. and Lopičić, Zorica and Janićijević, Aleksandra and Stojanović, Ksenija A.", year = "2019", abstract = "The purpose of this paper was to investigate the effectiveness of three different extraction agents for the extraction of 25 elements from sediment samples collected from 4 artificial lakes and 12 rivers in Serbia (33 samples in total). The extraction efficiency of the agents was evaluated by its ability to extract the highest quantity of the elements. For that purpose, three acids (1M HCl, 2M HNO3 and 0.43M CH3COOH) have been used. Inductively coupled plasma atomic emission spectrometry (ICP-OES) was used for quantitative determination of following elements: Al, As, B, Ba, Be, Bi, Ca, Cd, Cr, Co, Cu, Fe, Hg, K, Li, Mg, Mn, Ni, Na, Pb, Sb, Se, Sr, V, and Zn. The extraction with 1M HCl has shown the best results for the majority of investigated elements (especially Sr, Mn and Ca). Antimony (Sb) was detected only after extraction with 0.43M CH3COOOH, while selenium (Se) could not be detected when 2M HNO3 was applied as extraction agents. The present study could be very useful for choosing a suitable method for specific elements and also can be helpful in the evaluation of the contaminants in freshwater sediments in Serbia. This might contribute to environmental risk assessment of the present elements.", journal = "Acta Periodica Technologica", title = "Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia", volume = "50", pages = "189-196", doi = "10.2298/APT1950189P" }
Pantović Spajić, K., Sakan, S. M., Đorđević, D. S., Šoštarić, T. D., Lopičić, Z., Janićijević, A.,& Stojanović, K. A.. (2019). Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia. in Acta Periodica Technologica, 50, 189-196. https://doi.org/10.2298/APT1950189P
Pantović Spajić K, Sakan SM, Đorđević DS, Šoštarić TD, Lopičić Z, Janićijević A, Stojanović KA. Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia. in Acta Periodica Technologica. 2019;50:189-196. doi:10.2298/APT1950189P .
Pantović Spajić, Katarina, Sakan, Sanja M., Đorđević, Dragana S., Šoštarić, Tatjana D., Lopičić, Zorica, Janićijević, Aleksandra, Stojanović, Ksenija A., "Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia" in Acta Periodica Technologica, 50 (2019):189-196, https://doi.org/10.2298/APT1950189P . .