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Regioselective synthesis of a stereodefined heterocyclic push-pull alkene - H-1 NMR studies and two-dimensional TLC illustrating Z/E isomerization
dc.creator | Marković, R. | |
dc.creator | Baranac-Stojanović, Marija | |
dc.creator | Jovanović, Vesna B. | |
dc.creator | Džambaski, Z. | |
dc.date.accessioned | 2018-11-22T00:07:07Z | |
dc.date.available | 2018-11-22T00:07:07Z | |
dc.date.issued | 2004 | |
dc.identifier.issn | 0021-9584 | |
dc.identifier.uri | https://cherry.chem.bg.ac.rs/handle/123456789/646 | |
dc.description.abstract | Introducing students to the regioselective synthesis of a stereodefined push-pull alkene from inexpensive chemicals can be facilicated through experiment. In the experiment, preparation of the precursor, such as diethyl mercaptosuccinate from mercaptosuccinic acid and ethanol in toluene as a cosolvent, demonstrates the educational significance of binary and tertiary azeotropes in practical organic synthesis. The utility of 1H NMR spectroscopy is illustrated as a tool to identify the configurational isomers and to study the stereodynamic behavior of the isolated heterocyclic product. | en |
dc.publisher | Amer Chemical Soc, Washington | |
dc.rights | restrictedAccess | |
dc.source | Journal of Chemical Education | |
dc.title | Regioselective synthesis of a stereodefined heterocyclic push-pull alkene - H-1 NMR studies and two-dimensional TLC illustrating Z/E isomerization | en |
dc.type | article | |
dc.rights.license | ARR | |
dcterms.abstract | Баранац-Стојановић, Марија; Дзамбаски, З; Марковиц, Р; Јовановиц, В; | |
dc.citation.volume | 81 | |
dc.citation.issue | 7 | |
dc.citation.spage | 1026 | |
dc.citation.epage | 1029 | |
dc.identifier.wos | 000222023200028 | |
dc.citation.other | 81(7): 1026-1029 | |
dc.citation.rank | M23 | |
dc.type.version | publishedVersion | en |
dc.identifier.scopus | 2-s2.0-3142755637 | |
dc.identifier.rcub | https://hdl.handle.net/21.15107/rcub_cherry_646 |