Complete assignments of H-1 and C-13 NMR spectra of leucanthoside A, a new triterpenoid saponin from Cephalaria leucantha L.
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2006
Authors
Gođevac, DejanMandić, Boris
Vajs, Vlatka
Menković, N.
Macura, S.
Milosavljević, Slobodan M.
Article (Published version)
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Leucanthoside A, a new allose-containing triterpenoid saponin (1), was isolated from the aerial parts of Cephalaria leucantha L. Its structure was determined by electrospray ionization mass spectrometry and NMR spectroscopy. Complete assignments of the H-1 and 1 C NMR chemical shifts were achieved by two-dimensional NMR experiments: DQF-COSY, NOESY, TOCSY, HSQC, DINE-HSQC, HMBC, C-13-H-1 2D-J-resolved spectroscopy, and 1,1-ADEQUATE. Copyright (c) 2006 John Wiley & Sons, Ltd.
Keywords:
NMR / H-1 NMR / C-13 NMR / 2D NMR / Cephalaria leucantha / saponin / leucanthoside ASource:
Magnetic Resonance in Chemistry, 2006, 44, 7, 731-735Publisher:
- John Wiley & Sons Ltd, Chichester
Funding / projects:
- Sekundarni metaboliti samoniklih, lekovitih biljaka: izolovanje, karakterizacija i biloška aktivnost (RS-MESTD-MPN2006-2010-142053)
DOI: 10.1002/mrc.1834
ISSN: 0749-1581
PubMed: 16645935
WoS: 000238691300014
Scopus: 2-s2.0-33745712031
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Hemijski fakultet / Faculty of ChemistryTY - JOUR AU - Gođevac, Dejan AU - Mandić, Boris AU - Vajs, Vlatka AU - Menković, N. AU - Macura, S. AU - Milosavljević, Slobodan M. PY - 2006 UR - https://cherry.chem.bg.ac.rs/handle/123456789/784 AB - Leucanthoside A, a new allose-containing triterpenoid saponin (1), was isolated from the aerial parts of Cephalaria leucantha L. Its structure was determined by electrospray ionization mass spectrometry and NMR spectroscopy. Complete assignments of the H-1 and 1 C NMR chemical shifts were achieved by two-dimensional NMR experiments: DQF-COSY, NOESY, TOCSY, HSQC, DINE-HSQC, HMBC, C-13-H-1 2D-J-resolved spectroscopy, and 1,1-ADEQUATE. Copyright (c) 2006 John Wiley & Sons, Ltd. PB - John Wiley & Sons Ltd, Chichester T2 - Magnetic Resonance in Chemistry T1 - Complete assignments of H-1 and C-13 NMR spectra of leucanthoside A, a new triterpenoid saponin from Cephalaria leucantha L. VL - 44 IS - 7 SP - 731 EP - 735 DO - 10.1002/mrc.1834 ER -
@article{ author = "Gođevac, Dejan and Mandić, Boris and Vajs, Vlatka and Menković, N. and Macura, S. and Milosavljević, Slobodan M.", year = "2006", abstract = "Leucanthoside A, a new allose-containing triterpenoid saponin (1), was isolated from the aerial parts of Cephalaria leucantha L. Its structure was determined by electrospray ionization mass spectrometry and NMR spectroscopy. Complete assignments of the H-1 and 1 C NMR chemical shifts were achieved by two-dimensional NMR experiments: DQF-COSY, NOESY, TOCSY, HSQC, DINE-HSQC, HMBC, C-13-H-1 2D-J-resolved spectroscopy, and 1,1-ADEQUATE. Copyright (c) 2006 John Wiley & Sons, Ltd.", publisher = "John Wiley & Sons Ltd, Chichester", journal = "Magnetic Resonance in Chemistry", title = "Complete assignments of H-1 and C-13 NMR spectra of leucanthoside A, a new triterpenoid saponin from Cephalaria leucantha L.", volume = "44", number = "7", pages = "731-735", doi = "10.1002/mrc.1834" }
Gođevac, D., Mandić, B., Vajs, V., Menković, N., Macura, S.,& Milosavljević, S. M.. (2006). Complete assignments of H-1 and C-13 NMR spectra of leucanthoside A, a new triterpenoid saponin from Cephalaria leucantha L.. in Magnetic Resonance in Chemistry John Wiley & Sons Ltd, Chichester., 44(7), 731-735. https://doi.org/10.1002/mrc.1834
Gođevac D, Mandić B, Vajs V, Menković N, Macura S, Milosavljević SM. Complete assignments of H-1 and C-13 NMR spectra of leucanthoside A, a new triterpenoid saponin from Cephalaria leucantha L.. in Magnetic Resonance in Chemistry. 2006;44(7):731-735. doi:10.1002/mrc.1834 .
Gođevac, Dejan, Mandić, Boris, Vajs, Vlatka, Menković, N., Macura, S., Milosavljević, Slobodan M., "Complete assignments of H-1 and C-13 NMR spectra of leucanthoside A, a new triterpenoid saponin from Cephalaria leucantha L." in Magnetic Resonance in Chemistry, 44, no. 7 (2006):731-735, https://doi.org/10.1002/mrc.1834 . .