Nikolić-Mandić, Snežana D.

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Authority KeyName Variants
orcid::0000-0002-7816-8095
  • Nikolić-Mandić, Snežana D. (22)
  • Mandić, Snežana D. (1)
Projects

Author's Bibliography

Development of a Flow Injection System for Differential Pulse Amperometry and Its Application for Diazepam Determination

Antunović, Vesna R.; Tešanović, Slavna; Perušković, Danica S.; Stevanović, Nikola R.; Baošić, Rada; Mandić, Snežana D.; Lolić, Aleksandar

(Hindawi Ltd, London, 2018)

TY  - JOUR
AU  - Antunović, Vesna R.
AU  - Tešanović, Slavna
AU  - Perušković, Danica S.
AU  - Stevanović, Nikola R.
AU  - Baošić, Rada
AU  - Mandić, Snežana D.
AU  - Lolić, Aleksandar
PY  - 2018
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/2122
AB  - The is work presents the development of a flow injection system for differential pulse amperometry (DPA) for diazepam determination in the presence of oxygen. The thin flow cell consisted of the bare glassy carbon electrode, reference silver/silver chloride, and stainless steel as the auxiliary electrode. Electrochemical reduction of diazepam (DZP) was characterised by cyclic voltammetry. Azomethine reduction peak was used for DZP quantification. The detector response was linear in the range 20-250 mu mol/dm(3) of diazepam, with a calculated detection limit of 3.83 mu g/cm(3). Intraday and interday precision were 1.53 and 10.8%, respectively. The method was applied on three beverage samples, energetic drink, and two different beer samples, and obtained recoveries were from 93.65 up to 104.96%. The throughoutput of the method was up to 90 analyses per hour.
PB  - Hindawi Ltd, London
T2  - Journal of Analytical Methods in Chemistry
T1  - Development of a Flow Injection System for Differential Pulse Amperometry and Its Application for Diazepam Determination
DO  - 10.1155/2018/6121489
ER  - 
@article{
author = "Antunović, Vesna R. and Tešanović, Slavna and Perušković, Danica S. and Stevanović, Nikola R. and Baošić, Rada and Mandić, Snežana D. and Lolić, Aleksandar",
year = "2018",
abstract = "The is work presents the development of a flow injection system for differential pulse amperometry (DPA) for diazepam determination in the presence of oxygen. The thin flow cell consisted of the bare glassy carbon electrode, reference silver/silver chloride, and stainless steel as the auxiliary electrode. Electrochemical reduction of diazepam (DZP) was characterised by cyclic voltammetry. Azomethine reduction peak was used for DZP quantification. The detector response was linear in the range 20-250 mu mol/dm(3) of diazepam, with a calculated detection limit of 3.83 mu g/cm(3). Intraday and interday precision were 1.53 and 10.8%, respectively. The method was applied on three beverage samples, energetic drink, and two different beer samples, and obtained recoveries were from 93.65 up to 104.96%. The throughoutput of the method was up to 90 analyses per hour.",
publisher = "Hindawi Ltd, London",
journal = "Journal of Analytical Methods in Chemistry",
title = "Development of a Flow Injection System for Differential Pulse Amperometry and Its Application for Diazepam Determination",
doi = "10.1155/2018/6121489"
}
Antunović, V. R., Tešanović, S., Perušković, D. S., Stevanović, N. R., Baošić, R., Mandić, S. D.,& Lolić, A.. (2018). Development of a Flow Injection System for Differential Pulse Amperometry and Its Application for Diazepam Determination. in Journal of Analytical Methods in Chemistry
Hindawi Ltd, London..
https://doi.org/10.1155/2018/6121489
Antunović VR, Tešanović S, Perušković DS, Stevanović NR, Baošić R, Mandić SD, Lolić A. Development of a Flow Injection System for Differential Pulse Amperometry and Its Application for Diazepam Determination. in Journal of Analytical Methods in Chemistry. 2018;.
doi:10.1155/2018/6121489 .
Antunović, Vesna R., Tešanović, Slavna, Perušković, Danica S., Stevanović, Nikola R., Baošić, Rada, Mandić, Snežana D., Lolić, Aleksandar, "Development of a Flow Injection System for Differential Pulse Amperometry and Its Application for Diazepam Determination" in Journal of Analytical Methods in Chemistry (2018),
https://doi.org/10.1155/2018/6121489 . .
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Update on element content profiles in eleven wild edible mushrooms from family Boletaceae

Dimitrijević, Marija V.; Mitić, Violeta D.; Cvetković, Jelena S.; Stankov-Jovanović, Vesna P.; Mutić, Jelena; Nikolić-Mandić, Snežana D.

(Springer, New York, 2016)

TY  - JOUR
AU  - Dimitrijević, Marija V.
AU  - Mitić, Violeta D.
AU  - Cvetković, Jelena S.
AU  - Stankov-Jovanović, Vesna P.
AU  - Mutić, Jelena
AU  - Nikolić-Mandić, Snežana D.
PY  - 2016
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/2028
AB  - The aim of this study was to determine and evaluate the amounts of major elements (Ca, Fe, K, Na and P), essential trace elements (Cu, Zn, Fe and Mn) and some other trace metals (Ag, Al, Co, Ni, Cr, Sr, Se, Bi, Rb) in eleven species of wild-grown common edible mushrooms from family Boletaceae (Boletus appendiculatus, Boletus edulis, Boletus regius, Boletus fechtneri, Boletus impolitus, Boletus purpureus, Boletus rhodoxanthus, Leccinum crocipodium, Leccinum pseudoscaber, Xerocomellus chrysenteron, Xerocomus badius) from Serbia. The measurements of major elements (Ca, Fe, K, Na and P) were carried out by inductively coupled plasma optical emission spectrometer (ICP-OES), while analytical measurements of the rest of studied elements were performed using an inductively coupled plasma mass spectrometer (ICP-MS), after microwave digestion. The results showed that the element concentrations were species-dependent. Potassium and phosphorous concentrations were found to be greater than those of the other mineral constituents in all tested species. Multivariate analysis included principal component analysis (PCA) and hierarchical cluster analyses (HCA). HCA grouped mushrooms in three statistically significant clusters, while PCA indicated connection between analyzed metals. Also, this paper highlights the importance of essential and nonessential elements of human health and their daily intake.
PB  - Springer, New York
T2  - European Food Research and Technology
T1  - Update on element content profiles in eleven wild edible mushrooms from family Boletaceae
VL  - 242
IS  - 1
SP  - 1
EP  - 10
DO  - 10.1007/s00217-015-2512-0
ER  - 
@article{
author = "Dimitrijević, Marija V. and Mitić, Violeta D. and Cvetković, Jelena S. and Stankov-Jovanović, Vesna P. and Mutić, Jelena and Nikolić-Mandić, Snežana D.",
year = "2016",
abstract = "The aim of this study was to determine and evaluate the amounts of major elements (Ca, Fe, K, Na and P), essential trace elements (Cu, Zn, Fe and Mn) and some other trace metals (Ag, Al, Co, Ni, Cr, Sr, Se, Bi, Rb) in eleven species of wild-grown common edible mushrooms from family Boletaceae (Boletus appendiculatus, Boletus edulis, Boletus regius, Boletus fechtneri, Boletus impolitus, Boletus purpureus, Boletus rhodoxanthus, Leccinum crocipodium, Leccinum pseudoscaber, Xerocomellus chrysenteron, Xerocomus badius) from Serbia. The measurements of major elements (Ca, Fe, K, Na and P) were carried out by inductively coupled plasma optical emission spectrometer (ICP-OES), while analytical measurements of the rest of studied elements were performed using an inductively coupled plasma mass spectrometer (ICP-MS), after microwave digestion. The results showed that the element concentrations were species-dependent. Potassium and phosphorous concentrations were found to be greater than those of the other mineral constituents in all tested species. Multivariate analysis included principal component analysis (PCA) and hierarchical cluster analyses (HCA). HCA grouped mushrooms in three statistically significant clusters, while PCA indicated connection between analyzed metals. Also, this paper highlights the importance of essential and nonessential elements of human health and their daily intake.",
publisher = "Springer, New York",
journal = "European Food Research and Technology",
title = "Update on element content profiles in eleven wild edible mushrooms from family Boletaceae",
volume = "242",
number = "1",
pages = "1-10",
doi = "10.1007/s00217-015-2512-0"
}
Dimitrijević, M. V., Mitić, V. D., Cvetković, J. S., Stankov-Jovanović, V. P., Mutić, J.,& Nikolić-Mandić, S. D.. (2016). Update on element content profiles in eleven wild edible mushrooms from family Boletaceae. in European Food Research and Technology
Springer, New York., 242(1), 1-10.
https://doi.org/10.1007/s00217-015-2512-0
Dimitrijević MV, Mitić VD, Cvetković JS, Stankov-Jovanović VP, Mutić J, Nikolić-Mandić SD. Update on element content profiles in eleven wild edible mushrooms from family Boletaceae. in European Food Research and Technology. 2016;242(1):1-10.
doi:10.1007/s00217-015-2512-0 .
Dimitrijević, Marija V., Mitić, Violeta D., Cvetković, Jelena S., Stankov-Jovanović, Vesna P., Mutić, Jelena, Nikolić-Mandić, Snežana D., "Update on element content profiles in eleven wild edible mushrooms from family Boletaceae" in European Food Research and Technology, 242, no. 1 (2016):1-10,
https://doi.org/10.1007/s00217-015-2512-0 . .
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The Influence of Alkyl Polyglucosides (And Highly Ethoxylated Alcohol Boosters) on the Phase Behavior of a Water/Toluene/Technical Alkyl Polyethoxylate Microemulsion System

Ilić, Marija; Haegel, Franz-Hubert; Pavelkić, Vesna; Zlatanović, Dragan; Nikolić-Mandić, Snežana D.; Lolić, Aleksandar; Nedić, Zoran

(Assoc Chemical Eng, Belgrade, 2016)

TY  - JOUR
AU  - Ilić, Marija
AU  - Haegel, Franz-Hubert
AU  - Pavelkić, Vesna
AU  - Zlatanović, Dragan
AU  - Nikolić-Mandić, Snežana D.
AU  - Lolić, Aleksandar
AU  - Nedić, Zoran
PY  - 2016
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1916
AB  - The influence of additives (alkyl polyglucoside, Glucopon 600 CS UP and alcohol ethoxylate C18E100) on the behavior of the water/toluene/Lutensol ON 50 (technical oxoalcohol, i-C10E5) microemulsion system as a function of temperature and composition has been investigated. The phase behavior of the microemulsions was determined by vertical sections through the Gibbs phase prism (fish-like phase diagrams). Alkyl polyglucoside shifts the one phase region to lower temperatures compared with water/toluene/Lutensol ON 50 mixtures. This is contrary to the expectation, considering the extreme hydrophilic nature of the sugar headgroup. The addition of hydrophilic alcohol ethoxylate (C18E100) to the water/toluene/Lutensol ON 50 system increases the solubilization capacity of the surfactant, even if the co-surfactant is used in small quantities, and shifts the one-phase region to higher temperature by a few degrees C.
PB  - Assoc Chemical Eng, Belgrade
T2  - Chemical Industry and Chemical Engineering Quarterly / CICEQ
T1  - The Influence of Alkyl Polyglucosides (And Highly Ethoxylated Alcohol Boosters) on the Phase Behavior of a Water/Toluene/Technical Alkyl Polyethoxylate Microemulsion System
VL  - 22
IS  - 1
SP  - 27
EP  - 32
DO  - 10.2298/CICEQ141105015I
ER  - 
@article{
author = "Ilić, Marija and Haegel, Franz-Hubert and Pavelkić, Vesna and Zlatanović, Dragan and Nikolić-Mandić, Snežana D. and Lolić, Aleksandar and Nedić, Zoran",
year = "2016",
abstract = "The influence of additives (alkyl polyglucoside, Glucopon 600 CS UP and alcohol ethoxylate C18E100) on the behavior of the water/toluene/Lutensol ON 50 (technical oxoalcohol, i-C10E5) microemulsion system as a function of temperature and composition has been investigated. The phase behavior of the microemulsions was determined by vertical sections through the Gibbs phase prism (fish-like phase diagrams). Alkyl polyglucoside shifts the one phase region to lower temperatures compared with water/toluene/Lutensol ON 50 mixtures. This is contrary to the expectation, considering the extreme hydrophilic nature of the sugar headgroup. The addition of hydrophilic alcohol ethoxylate (C18E100) to the water/toluene/Lutensol ON 50 system increases the solubilization capacity of the surfactant, even if the co-surfactant is used in small quantities, and shifts the one-phase region to higher temperature by a few degrees C.",
publisher = "Assoc Chemical Eng, Belgrade",
journal = "Chemical Industry and Chemical Engineering Quarterly / CICEQ",
title = "The Influence of Alkyl Polyglucosides (And Highly Ethoxylated Alcohol Boosters) on the Phase Behavior of a Water/Toluene/Technical Alkyl Polyethoxylate Microemulsion System",
volume = "22",
number = "1",
pages = "27-32",
doi = "10.2298/CICEQ141105015I"
}
Ilić, M., Haegel, F., Pavelkić, V., Zlatanović, D., Nikolić-Mandić, S. D., Lolić, A.,& Nedić, Z.. (2016). The Influence of Alkyl Polyglucosides (And Highly Ethoxylated Alcohol Boosters) on the Phase Behavior of a Water/Toluene/Technical Alkyl Polyethoxylate Microemulsion System. in Chemical Industry and Chemical Engineering Quarterly / CICEQ
Assoc Chemical Eng, Belgrade., 22(1), 27-32.
https://doi.org/10.2298/CICEQ141105015I
Ilić M, Haegel F, Pavelkić V, Zlatanović D, Nikolić-Mandić SD, Lolić A, Nedić Z. The Influence of Alkyl Polyglucosides (And Highly Ethoxylated Alcohol Boosters) on the Phase Behavior of a Water/Toluene/Technical Alkyl Polyethoxylate Microemulsion System. in Chemical Industry and Chemical Engineering Quarterly / CICEQ. 2016;22(1):27-32.
doi:10.2298/CICEQ141105015I .
Ilić, Marija, Haegel, Franz-Hubert, Pavelkić, Vesna, Zlatanović, Dragan, Nikolić-Mandić, Snežana D., Lolić, Aleksandar, Nedić, Zoran, "The Influence of Alkyl Polyglucosides (And Highly Ethoxylated Alcohol Boosters) on the Phase Behavior of a Water/Toluene/Technical Alkyl Polyethoxylate Microemulsion System" in Chemical Industry and Chemical Engineering Quarterly / CICEQ, 22, no. 1 (2016):27-32,
https://doi.org/10.2298/CICEQ141105015I . .
1
1
1
1

Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge

Mandić, Boris; Vlajić, Marina D.; Trifunović, Snežana S.; Simić, Milena R.; Vujisić, Ljubodrag V.; Vučković, Ivan M.; Novaković, Miroslav M.; Nikolić-Mandić, Snežana D.; Tešević, Vele; Vajs, Vlatka; Milosavljević, Slobodan M.

(Taylor & Francis Ltd, Abingdon, 2015)

TY  - JOUR
AU  - Mandić, Boris
AU  - Vlajić, Marina D.
AU  - Trifunović, Snežana S.
AU  - Simić, Milena R.
AU  - Vujisić, Ljubodrag V.
AU  - Vučković, Ivan M.
AU  - Novaković, Miroslav M.
AU  - Nikolić-Mandić, Snežana D.
AU  - Tešević, Vele
AU  - Vajs, Vlatka
AU  - Milosavljević, Slobodan M.
PY  - 2015
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1692
AB  - Procedure for isolation of pyrrolizidine alkaloids (PAs) from Rindera umbellata Bunge plant species was optimised. Different extraction media (methanol, ethanol and sulphuric acid), concentration and volume of sulphuric acid, pH of PA solution for alkaline extraction, extraction time and techniques (maceration, ultrasonic and overhead rotary mixer assisted extraction) were investigated. The yields of six PAs (7-angeloyl heliotridane, 7-angeloyl heliotridine, lindelofine, 7-angeloyl rinderine, punctanecine and heliosupine) were monitored by GC-MS/FID. The best results for the isolation all of six PAs were obtained when the extraction was performed with 1M sulphuric acid (30mL per 1.00g of dried sample) by overhead rotary mixer during three days. Optimal pH value for alkaline extraction of PAs with CH2Cl2 was 9, and the extraction should be performed with four portions of 30mL of CH2Cl2. This procedure could be also useful for a plant sample preparation for GC and LC analyses of PAs.
PB  - Taylor & Francis Ltd, Abingdon
T2  - Natural Product Research
T1  - Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge
VL  - 29
IS  - 9
SP  - 887
EP  - 890
DO  - 10.1080/14786419.2014.991929
ER  - 
@article{
author = "Mandić, Boris and Vlajić, Marina D. and Trifunović, Snežana S. and Simić, Milena R. and Vujisić, Ljubodrag V. and Vučković, Ivan M. and Novaković, Miroslav M. and Nikolić-Mandić, Snežana D. and Tešević, Vele and Vajs, Vlatka and Milosavljević, Slobodan M.",
year = "2015",
abstract = "Procedure for isolation of pyrrolizidine alkaloids (PAs) from Rindera umbellata Bunge plant species was optimised. Different extraction media (methanol, ethanol and sulphuric acid), concentration and volume of sulphuric acid, pH of PA solution for alkaline extraction, extraction time and techniques (maceration, ultrasonic and overhead rotary mixer assisted extraction) were investigated. The yields of six PAs (7-angeloyl heliotridane, 7-angeloyl heliotridine, lindelofine, 7-angeloyl rinderine, punctanecine and heliosupine) were monitored by GC-MS/FID. The best results for the isolation all of six PAs were obtained when the extraction was performed with 1M sulphuric acid (30mL per 1.00g of dried sample) by overhead rotary mixer during three days. Optimal pH value for alkaline extraction of PAs with CH2Cl2 was 9, and the extraction should be performed with four portions of 30mL of CH2Cl2. This procedure could be also useful for a plant sample preparation for GC and LC analyses of PAs.",
publisher = "Taylor & Francis Ltd, Abingdon",
journal = "Natural Product Research",
title = "Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge",
volume = "29",
number = "9",
pages = "887-890",
doi = "10.1080/14786419.2014.991929"
}
Mandić, B., Vlajić, M. D., Trifunović, S. S., Simić, M. R., Vujisić, L. V., Vučković, I. M., Novaković, M. M., Nikolić-Mandić, S. D., Tešević, V., Vajs, V.,& Milosavljević, S. M.. (2015). Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge. in Natural Product Research
Taylor & Francis Ltd, Abingdon., 29(9), 887-890.
https://doi.org/10.1080/14786419.2014.991929
Mandić B, Vlajić MD, Trifunović SS, Simić MR, Vujisić LV, Vučković IM, Novaković MM, Nikolić-Mandić SD, Tešević V, Vajs V, Milosavljević SM. Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge. in Natural Product Research. 2015;29(9):887-890.
doi:10.1080/14786419.2014.991929 .
Mandić, Boris, Vlajić, Marina D., Trifunović, Snežana S., Simić, Milena R., Vujisić, Ljubodrag V., Vučković, Ivan M., Novaković, Miroslav M., Nikolić-Mandić, Snežana D., Tešević, Vele, Vajs, Vlatka, Milosavljević, Slobodan M., "Optimisation of isolation procedure for pyrrolizidine alkaloids from Rindera umbellata Bunge" in Natural Product Research, 29, no. 9 (2015):887-890,
https://doi.org/10.1080/14786419.2014.991929 . .
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Supplementary data for article: Mandić, B. M.; Vlajić, M. D.; Trifunović, S. S.; Simić, M. R.; Vujisić, L. V.; Vučković, I. M.; Novaković, M. M.; Nikolić-Mandić, S. D.; Tešević, V. V.; Vajs, V. V.; et al. Optimisation of Isolation Procedure for Pyrrolizidine Alkaloids from Rindera Umbellata Bunge. Natural Product Research 2015, 29 (9), 887–890. https://doi.org/10.1080/14786419.2014.991929

Mandić, Boris; Vlajić, Marina D.; Trifunović, Snežana S.; Simić, Milena R.; Vujisić, Ljubodrag V.; Vučković, Ivan M.; Novaković, Miroslav M.; Nikolić-Mandić, Snežana D.; Tešević, Vele; Vajs, Vlatka; Milosavljević, Slobodan M.

(Taylor & Francis Ltd, Abingdon, 2015)

TY  - DATA
AU  - Mandić, Boris
AU  - Vlajić, Marina D.
AU  - Trifunović, Snežana S.
AU  - Simić, Milena R.
AU  - Vujisić, Ljubodrag V.
AU  - Vučković, Ivan M.
AU  - Novaković, Miroslav M.
AU  - Nikolić-Mandić, Snežana D.
AU  - Tešević, Vele
AU  - Vajs, Vlatka
AU  - Milosavljević, Slobodan M.
PY  - 2015
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/3388
PB  - Taylor & Francis Ltd, Abingdon
T2  - Natural Product Research
T1  - Supplementary data for article: Mandić, B. M.; Vlajić, M. D.; Trifunović, S. S.; Simić, M. R.; Vujisić, L. V.; Vučković, I. M.; Novaković, M. M.; Nikolić-Mandić, S. D.; Tešević, V. V.; Vajs, V. V.; et al. Optimisation of Isolation Procedure for Pyrrolizidine Alkaloids from Rindera Umbellata Bunge. Natural Product Research 2015, 29 (9), 887–890. https://doi.org/10.1080/14786419.2014.991929
UR  - https://hdl.handle.net/21.15107/rcub_cherry_3388
ER  - 
@misc{
author = "Mandić, Boris and Vlajić, Marina D. and Trifunović, Snežana S. and Simić, Milena R. and Vujisić, Ljubodrag V. and Vučković, Ivan M. and Novaković, Miroslav M. and Nikolić-Mandić, Snežana D. and Tešević, Vele and Vajs, Vlatka and Milosavljević, Slobodan M.",
year = "2015",
publisher = "Taylor & Francis Ltd, Abingdon",
journal = "Natural Product Research",
title = "Supplementary data for article: Mandić, B. M.; Vlajić, M. D.; Trifunović, S. S.; Simić, M. R.; Vujisić, L. V.; Vučković, I. M.; Novaković, M. M.; Nikolić-Mandić, S. D.; Tešević, V. V.; Vajs, V. V.; et al. Optimisation of Isolation Procedure for Pyrrolizidine Alkaloids from Rindera Umbellata Bunge. Natural Product Research 2015, 29 (9), 887–890. https://doi.org/10.1080/14786419.2014.991929",
url = "https://hdl.handle.net/21.15107/rcub_cherry_3388"
}
Mandić, B., Vlajić, M. D., Trifunović, S. S., Simić, M. R., Vujisić, L. V., Vučković, I. M., Novaković, M. M., Nikolić-Mandić, S. D., Tešević, V., Vajs, V.,& Milosavljević, S. M.. (2015). Supplementary data for article: Mandić, B. M.; Vlajić, M. D.; Trifunović, S. S.; Simić, M. R.; Vujisić, L. V.; Vučković, I. M.; Novaković, M. M.; Nikolić-Mandić, S. D.; Tešević, V. V.; Vajs, V. V.; et al. Optimisation of Isolation Procedure for Pyrrolizidine Alkaloids from Rindera Umbellata Bunge. Natural Product Research 2015, 29 (9), 887–890. https://doi.org/10.1080/14786419.2014.991929. in Natural Product Research
Taylor & Francis Ltd, Abingdon..
https://hdl.handle.net/21.15107/rcub_cherry_3388
Mandić B, Vlajić MD, Trifunović SS, Simić MR, Vujisić LV, Vučković IM, Novaković MM, Nikolić-Mandić SD, Tešević V, Vajs V, Milosavljević SM. Supplementary data for article: Mandić, B. M.; Vlajić, M. D.; Trifunović, S. S.; Simić, M. R.; Vujisić, L. V.; Vučković, I. M.; Novaković, M. M.; Nikolić-Mandić, S. D.; Tešević, V. V.; Vajs, V. V.; et al. Optimisation of Isolation Procedure for Pyrrolizidine Alkaloids from Rindera Umbellata Bunge. Natural Product Research 2015, 29 (9), 887–890. https://doi.org/10.1080/14786419.2014.991929. in Natural Product Research. 2015;.
https://hdl.handle.net/21.15107/rcub_cherry_3388 .
Mandić, Boris, Vlajić, Marina D., Trifunović, Snežana S., Simić, Milena R., Vujisić, Ljubodrag V., Vučković, Ivan M., Novaković, Miroslav M., Nikolić-Mandić, Snežana D., Tešević, Vele, Vajs, Vlatka, Milosavljević, Slobodan M., "Supplementary data for article: Mandić, B. M.; Vlajić, M. D.; Trifunović, S. S.; Simić, M. R.; Vujisić, L. V.; Vučković, I. M.; Novaković, M. M.; Nikolić-Mandić, S. D.; Tešević, V. V.; Vajs, V. V.; et al. Optimisation of Isolation Procedure for Pyrrolizidine Alkaloids from Rindera Umbellata Bunge. Natural Product Research 2015, 29 (9), 887–890. https://doi.org/10.1080/14786419.2014.991929" in Natural Product Research (2015),
https://hdl.handle.net/21.15107/rcub_cherry_3388 .

Electrospray ionization linear trap quadrupole Orbitrap in analysis of old tempera paintings: application to nineteenth-century Orthodox icons

Tripković, T.; Charvy, C.; Alves, S.; Lolić, Aleksandar; Baošić, Rada; Nikolić-Mandić, Snežana D.; Tabet, J. C.

(Im Publications, W Sussex, 2015)

TY  - JOUR
AU  - Tripković, T.
AU  - Charvy, C.
AU  - Alves, S.
AU  - Lolić, Aleksandar
AU  - Baošić, Rada
AU  - Nikolić-Mandić, Snežana D.
AU  - Tabet, J. C.
PY  - 2015
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1959
AB  - Proteomic approach in combination with mass spectrometry demonstrates a great potential for identification of proteinaceous materials in works of art. In this study we used a linear trap quadrupole Orbitrap (LTQ-Orbitraph a state-of-the-art mass spectrometer for parts per million accuracy analyses of peptides behind tryptic hydrolysis. After the efficiency of the proteomic method was confirmed for reference and model samples, micro-samples from historical paintings were for the first time analysed using this technique. Superior performances of the liquid chromatography-mass spectrometry approach using a LTQ-Orbitrap mass spectrometer allowed identification of egg yolk peptides in two samples from nineteenth-century Orthodox icons, indicating egg tempera as the painting technique. Accurate precursor ion masses, in the range of 2 ppm, and retention times of tryptic peptides strengthen protein identification. Additionally, in all historical samples the presence of animal glues suggested that the ground layer was likely bound using bovine collagen. Comparing to results acquired using matrix-assisted laser desorption/ionization time-of-flight tandem mass spectrometry in our previous study, here we achieved higher ion scores and protein scores, better sequence coverage and more identified proteins. In fact, a combination of the two mass spectrometric techniques provided overlapping and complementary data, related to the detection of peptides with different physicochemical properties.
PB  - Im Publications, W Sussex
T2  - European Journal of Mass Spectrometry
T1  - Electrospray ionization linear trap quadrupole Orbitrap in analysis of old tempera paintings: application to nineteenth-century Orthodox icons
VL  - 21
IS  - 4
SP  - 679
EP  - 692
DO  - 10.1255/ejms.1346
ER  - 
@article{
author = "Tripković, T. and Charvy, C. and Alves, S. and Lolić, Aleksandar and Baošić, Rada and Nikolić-Mandić, Snežana D. and Tabet, J. C.",
year = "2015",
abstract = "Proteomic approach in combination with mass spectrometry demonstrates a great potential for identification of proteinaceous materials in works of art. In this study we used a linear trap quadrupole Orbitrap (LTQ-Orbitraph a state-of-the-art mass spectrometer for parts per million accuracy analyses of peptides behind tryptic hydrolysis. After the efficiency of the proteomic method was confirmed for reference and model samples, micro-samples from historical paintings were for the first time analysed using this technique. Superior performances of the liquid chromatography-mass spectrometry approach using a LTQ-Orbitrap mass spectrometer allowed identification of egg yolk peptides in two samples from nineteenth-century Orthodox icons, indicating egg tempera as the painting technique. Accurate precursor ion masses, in the range of 2 ppm, and retention times of tryptic peptides strengthen protein identification. Additionally, in all historical samples the presence of animal glues suggested that the ground layer was likely bound using bovine collagen. Comparing to results acquired using matrix-assisted laser desorption/ionization time-of-flight tandem mass spectrometry in our previous study, here we achieved higher ion scores and protein scores, better sequence coverage and more identified proteins. In fact, a combination of the two mass spectrometric techniques provided overlapping and complementary data, related to the detection of peptides with different physicochemical properties.",
publisher = "Im Publications, W Sussex",
journal = "European Journal of Mass Spectrometry",
title = "Electrospray ionization linear trap quadrupole Orbitrap in analysis of old tempera paintings: application to nineteenth-century Orthodox icons",
volume = "21",
number = "4",
pages = "679-692",
doi = "10.1255/ejms.1346"
}
Tripković, T., Charvy, C., Alves, S., Lolić, A., Baošić, R., Nikolić-Mandić, S. D.,& Tabet, J. C.. (2015). Electrospray ionization linear trap quadrupole Orbitrap in analysis of old tempera paintings: application to nineteenth-century Orthodox icons. in European Journal of Mass Spectrometry
Im Publications, W Sussex., 21(4), 679-692.
https://doi.org/10.1255/ejms.1346
Tripković T, Charvy C, Alves S, Lolić A, Baošić R, Nikolić-Mandić SD, Tabet JC. Electrospray ionization linear trap quadrupole Orbitrap in analysis of old tempera paintings: application to nineteenth-century Orthodox icons. in European Journal of Mass Spectrometry. 2015;21(4):679-692.
doi:10.1255/ejms.1346 .
Tripković, T., Charvy, C., Alves, S., Lolić, Aleksandar, Baošić, Rada, Nikolić-Mandić, Snežana D., Tabet, J. C., "Electrospray ionization linear trap quadrupole Orbitrap in analysis of old tempera paintings: application to nineteenth-century Orthodox icons" in European Journal of Mass Spectrometry, 21, no. 4 (2015):679-692,
https://doi.org/10.1255/ejms.1346 . .
9
5
8
8

Pyrrolizidine Alkaloids and Fatty Acids from the Endemic Plant Species Rindera umbellata and the Effect of Lindelofine-N-oxide on Tubulin Polymerization

Mandić, Boris; Simić, Milena R.; Vučković, Ivan M.; Vujisić, Ljubodrag V.; Novaković, Miroslav M.; Trifunović, Snežana S.; Nikolić-Mandić, Snežana D.; Tešević, Vele; Vajs, Vlatka; Milosavljević, Slobodan M.

(Mdpi Ag, Basel, 2013)

TY  - JOUR
AU  - Mandić, Boris
AU  - Simić, Milena R.
AU  - Vučković, Ivan M.
AU  - Vujisić, Ljubodrag V.
AU  - Novaković, Miroslav M.
AU  - Trifunović, Snežana S.
AU  - Nikolić-Mandić, Snežana D.
AU  - Tešević, Vele
AU  - Vajs, Vlatka
AU  - Milosavljević, Slobodan M.
PY  - 2013
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1494
AB  - The examination of the aerial parts, roots, and seeds of the endemic plant Rindera umbellata is reported in this paper for the first time. Phytochemical investigation of R. umbellata led to the isolation and characterization of ten pyrrolizidine alkaloids and eleven fatty acids in the form of triglycerides. Pyrrolizidine alkaloids 1-9 were found in the aerial parts, 7 and 8 in the roots, and 6-10, together with eleven fatty acids, in the seeds of this plant species. The structures of compounds 1-10 were established based on spectroscopic studies (H-1- and C-13-NMR, 2D NMR, IR and CI-MS). After trans-esterification, methyl esters of the fatty acids were analyzed using GC-MS. The effect of lindelofine-N-oxide (7) on tubulin polymerization was determined.
PB  - Mdpi Ag, Basel
T2  - Molecules
T1  - Pyrrolizidine Alkaloids and Fatty Acids from the Endemic Plant Species Rindera umbellata and the Effect of Lindelofine-N-oxide on Tubulin Polymerization
VL  - 18
IS  - 9
SP  - 10694
EP  - 10706
DO  - 10.3390/molecules180910694
ER  - 
@article{
author = "Mandić, Boris and Simić, Milena R. and Vučković, Ivan M. and Vujisić, Ljubodrag V. and Novaković, Miroslav M. and Trifunović, Snežana S. and Nikolić-Mandić, Snežana D. and Tešević, Vele and Vajs, Vlatka and Milosavljević, Slobodan M.",
year = "2013",
abstract = "The examination of the aerial parts, roots, and seeds of the endemic plant Rindera umbellata is reported in this paper for the first time. Phytochemical investigation of R. umbellata led to the isolation and characterization of ten pyrrolizidine alkaloids and eleven fatty acids in the form of triglycerides. Pyrrolizidine alkaloids 1-9 were found in the aerial parts, 7 and 8 in the roots, and 6-10, together with eleven fatty acids, in the seeds of this plant species. The structures of compounds 1-10 were established based on spectroscopic studies (H-1- and C-13-NMR, 2D NMR, IR and CI-MS). After trans-esterification, methyl esters of the fatty acids were analyzed using GC-MS. The effect of lindelofine-N-oxide (7) on tubulin polymerization was determined.",
publisher = "Mdpi Ag, Basel",
journal = "Molecules",
title = "Pyrrolizidine Alkaloids and Fatty Acids from the Endemic Plant Species Rindera umbellata and the Effect of Lindelofine-N-oxide on Tubulin Polymerization",
volume = "18",
number = "9",
pages = "10694-10706",
doi = "10.3390/molecules180910694"
}
Mandić, B., Simić, M. R., Vučković, I. M., Vujisić, L. V., Novaković, M. M., Trifunović, S. S., Nikolić-Mandić, S. D., Tešević, V., Vajs, V.,& Milosavljević, S. M.. (2013). Pyrrolizidine Alkaloids and Fatty Acids from the Endemic Plant Species Rindera umbellata and the Effect of Lindelofine-N-oxide on Tubulin Polymerization. in Molecules
Mdpi Ag, Basel., 18(9), 10694-10706.
https://doi.org/10.3390/molecules180910694
Mandić B, Simić MR, Vučković IM, Vujisić LV, Novaković MM, Trifunović SS, Nikolić-Mandić SD, Tešević V, Vajs V, Milosavljević SM. Pyrrolizidine Alkaloids and Fatty Acids from the Endemic Plant Species Rindera umbellata and the Effect of Lindelofine-N-oxide on Tubulin Polymerization. in Molecules. 2013;18(9):10694-10706.
doi:10.3390/molecules180910694 .
Mandić, Boris, Simić, Milena R., Vučković, Ivan M., Vujisić, Ljubodrag V., Novaković, Miroslav M., Trifunović, Snežana S., Nikolić-Mandić, Snežana D., Tešević, Vele, Vajs, Vlatka, Milosavljević, Slobodan M., "Pyrrolizidine Alkaloids and Fatty Acids from the Endemic Plant Species Rindera umbellata and the Effect of Lindelofine-N-oxide on Tubulin Polymerization" in Molecules, 18, no. 9 (2013):10694-10706,
https://doi.org/10.3390/molecules180910694 . .
17
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15

Determination of copper by indirect gas-diffusion flow injection analysis with amperometric detection in the presence of nickel and zinc

Šaronjić, Uroš; Lolić, Aleksandar; Nikolić-Mandić, Snežana D.

(Escola Superior de Biotecnologia, Universidade Catolica Portuguesa (ESC-UCP), 2013)

TY  - CONF
AU  - Šaronjić, Uroš
AU  - Lolić, Aleksandar
AU  - Nikolić-Mandić, Snežana D.
PY  - 2013
UR  - http://cherry.chem.bg.ac.rs/handle/123456789/4992
AB  - Indirect determination of copper was based on determination of cyanide on working silver electrode. The system was equipped with two injection valves. One for injection of cyanide solution (reagent) and another one for the sample injection (copper solution). Carriers for cyanide and copper were 0.02 mol/L sodium-hydroxide and 0.01 mol/L hydrochloric acid, respectively. The copper determination in such system was severely interfered by the presence of cations forming stable cyano complexes [1]. The interferences were successfully removed off-line by applying appropriate chemical reaction. The most prominent interferants were nickel and zinc. By including the dumper in the FIA system, containing cotton wool soaked in an appropriate solution, nickel and zinc were successfully removed. Interferences from nickel were removed by soaking the wool in the alkaline solution of dimethylglyoxime (DMG) and the zinc was removed by soaking the wool in acidic solution of the p-NIAZOX (7-(4-nitrofenilazo)-8-hydroxyquinoline-5-sulfonic acid) [2]. The method was applied for determination of copper in real samples.
PB  - Escola Superior de Biotecnologia, Universidade Catolica Portuguesa (ESC-UCP)
C3  - 18th International Conference on Flow Injection Analysis (ICFIA), 15-20 Sept 2013, Porto, Portugal, Book of Abstracts PA2
T1  - Determination of copper by indirect gas-diffusion flow injection analysis with amperometric detection in the presence of nickel and zinc
UR  - https://hdl.handle.net/21.15107/rcub_cherry_4992
ER  - 
@conference{
author = "Šaronjić, Uroš and Lolić, Aleksandar and Nikolić-Mandić, Snežana D.",
year = "2013",
abstract = "Indirect determination of copper was based on determination of cyanide on working silver electrode. The system was equipped with two injection valves. One for injection of cyanide solution (reagent) and another one for the sample injection (copper solution). Carriers for cyanide and copper were 0.02 mol/L sodium-hydroxide and 0.01 mol/L hydrochloric acid, respectively. The copper determination in such system was severely interfered by the presence of cations forming stable cyano complexes [1]. The interferences were successfully removed off-line by applying appropriate chemical reaction. The most prominent interferants were nickel and zinc. By including the dumper in the FIA system, containing cotton wool soaked in an appropriate solution, nickel and zinc were successfully removed. Interferences from nickel were removed by soaking the wool in the alkaline solution of dimethylglyoxime (DMG) and the zinc was removed by soaking the wool in acidic solution of the p-NIAZOX (7-(4-nitrofenilazo)-8-hydroxyquinoline-5-sulfonic acid) [2]. The method was applied for determination of copper in real samples.",
publisher = "Escola Superior de Biotecnologia, Universidade Catolica Portuguesa (ESC-UCP)",
journal = "18th International Conference on Flow Injection Analysis (ICFIA), 15-20 Sept 2013, Porto, Portugal, Book of Abstracts PA2",
title = "Determination of copper by indirect gas-diffusion flow injection analysis with amperometric detection in the presence of nickel and zinc",
url = "https://hdl.handle.net/21.15107/rcub_cherry_4992"
}
Šaronjić, U., Lolić, A.,& Nikolić-Mandić, S. D.. (2013). Determination of copper by indirect gas-diffusion flow injection analysis with amperometric detection in the presence of nickel and zinc. in 18th International Conference on Flow Injection Analysis (ICFIA), 15-20 Sept 2013, Porto, Portugal, Book of Abstracts PA2
Escola Superior de Biotecnologia, Universidade Catolica Portuguesa (ESC-UCP)..
https://hdl.handle.net/21.15107/rcub_cherry_4992
Šaronjić U, Lolić A, Nikolić-Mandić SD. Determination of copper by indirect gas-diffusion flow injection analysis with amperometric detection in the presence of nickel and zinc. in 18th International Conference on Flow Injection Analysis (ICFIA), 15-20 Sept 2013, Porto, Portugal, Book of Abstracts PA2. 2013;.
https://hdl.handle.net/21.15107/rcub_cherry_4992 .
Šaronjić, Uroš, Lolić, Aleksandar, Nikolić-Mandić, Snežana D., "Determination of copper by indirect gas-diffusion flow injection analysis with amperometric detection in the presence of nickel and zinc" in 18th International Conference on Flow Injection Analysis (ICFIA), 15-20 Sept 2013, Porto, Portugal, Book of Abstracts PA2 (2013),
https://hdl.handle.net/21.15107/rcub_cherry_4992 .

Supplementary data for article: Tripkovic, T.; Charvy, C.; Alves, S.; Lolić, A.; Baošić, R.; Nikolić-Mandić, S. D.; Tabet, J. C. Identification of Protein Binders in Artworks by MALDI-TOF/TOF Tandem Mass Spectrometry. Talanta 2013, 113, 49–61. https://doi.org/10.1016/j.talanta.2013.03.071

Tripković, T.; Charvy, C.; Alves, S.; Lolić, Aleksandar; Baošić, Rada; Nikolić-Mandić, Snežana D.; Tabet, J. C.

(Elsevier Science Bv, Amsterdam, 2013)

TY  - DATA
AU  - Tripković, T.
AU  - Charvy, C.
AU  - Alves, S.
AU  - Lolić, Aleksandar
AU  - Baošić, Rada
AU  - Nikolić-Mandić, Snežana D.
AU  - Tabet, J. C.
PY  - 2013
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/3500
PB  - Elsevier Science Bv, Amsterdam
T2  - Talanta
T1  - Supplementary data for article: Tripkovic, T.; Charvy, C.; Alves, S.; Lolić, A.; Baošić, R.; Nikolić-Mandić, S. D.; Tabet, J. C. Identification of Protein Binders in Artworks by MALDI-TOF/TOF Tandem Mass Spectrometry. Talanta 2013, 113, 49–61. https://doi.org/10.1016/j.talanta.2013.03.071
UR  - https://hdl.handle.net/21.15107/rcub_cherry_3500
ER  - 
@misc{
author = "Tripković, T. and Charvy, C. and Alves, S. and Lolić, Aleksandar and Baošić, Rada and Nikolić-Mandić, Snežana D. and Tabet, J. C.",
year = "2013",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "Talanta",
title = "Supplementary data for article: Tripkovic, T.; Charvy, C.; Alves, S.; Lolić, A.; Baošić, R.; Nikolić-Mandić, S. D.; Tabet, J. C. Identification of Protein Binders in Artworks by MALDI-TOF/TOF Tandem Mass Spectrometry. Talanta 2013, 113, 49–61. https://doi.org/10.1016/j.talanta.2013.03.071",
url = "https://hdl.handle.net/21.15107/rcub_cherry_3500"
}
Tripković, T., Charvy, C., Alves, S., Lolić, A., Baošić, R., Nikolić-Mandić, S. D.,& Tabet, J. C.. (2013). Supplementary data for article: Tripkovic, T.; Charvy, C.; Alves, S.; Lolić, A.; Baošić, R.; Nikolić-Mandić, S. D.; Tabet, J. C. Identification of Protein Binders in Artworks by MALDI-TOF/TOF Tandem Mass Spectrometry. Talanta 2013, 113, 49–61. https://doi.org/10.1016/j.talanta.2013.03.071. in Talanta
Elsevier Science Bv, Amsterdam..
https://hdl.handle.net/21.15107/rcub_cherry_3500
Tripković T, Charvy C, Alves S, Lolić A, Baošić R, Nikolić-Mandić SD, Tabet JC. Supplementary data for article: Tripkovic, T.; Charvy, C.; Alves, S.; Lolić, A.; Baošić, R.; Nikolić-Mandić, S. D.; Tabet, J. C. Identification of Protein Binders in Artworks by MALDI-TOF/TOF Tandem Mass Spectrometry. Talanta 2013, 113, 49–61. https://doi.org/10.1016/j.talanta.2013.03.071. in Talanta. 2013;.
https://hdl.handle.net/21.15107/rcub_cherry_3500 .
Tripković, T., Charvy, C., Alves, S., Lolić, Aleksandar, Baošić, Rada, Nikolić-Mandić, Snežana D., Tabet, J. C., "Supplementary data for article: Tripkovic, T.; Charvy, C.; Alves, S.; Lolić, A.; Baošić, R.; Nikolić-Mandić, S. D.; Tabet, J. C. Identification of Protein Binders in Artworks by MALDI-TOF/TOF Tandem Mass Spectrometry. Talanta 2013, 113, 49–61. https://doi.org/10.1016/j.talanta.2013.03.071" in Talanta (2013),
https://hdl.handle.net/21.15107/rcub_cherry_3500 .

Identification of protein binders in artworks by MALDI-TOF/TOF tandem mass spectrometry

Tripković, T.; Charvy, C.; Alves, S.; Lolić, Aleksandar; Baošić, Rada; Nikolić-Mandić, Snežana D.; Tabet, J. C.

(Elsevier Science Bv, Amsterdam, 2013)

TY  - JOUR
AU  - Tripković, T.
AU  - Charvy, C.
AU  - Alves, S.
AU  - Lolić, Aleksandar
AU  - Baošić, Rada
AU  - Nikolić-Mandić, Snežana D.
AU  - Tabet, J. C.
PY  - 2013
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1366
AB  - Aim of this work is to propose an analytical protocol for proteinaceous binder identification in paintings using tryptic peptide analysis and MALDI-TOF mass spectrometry strengthened with MALDI-TOF/TOF tandem mass spectrometry (LIFT method). Proteinaceous binders are enzymatically digested with trypsin. From each individual protein frequently occurring in binders, a specific set of peptides is releasing during enzymatic digestion giving a peptide mass fingerprint (PMF) of that particular protein. The most intensive peptide peaks in PMF were determined and annotated with their corresponding amino acid sequence by MALDI-TOF/TOF analysis and subsequent database search. Before analyzing historical painting samples, procedure was tested and optimized on several painting model samples for a reliable and efficient identification of proteinaceous materials. The method is avoiding sample manipulation as much as possible in order to reduce sample loss. Since the applied procedures led to protein identification of binding media in model samples, MALDI-TOF/TOF was for the first time applied for analysis of proteinaceous binders in old painting samples.
PB  - Elsevier Science Bv, Amsterdam
T2  - Talanta
T1  - Identification of protein binders in artworks by MALDI-TOF/TOF tandem mass spectrometry
VL  - 113
SP  - 49
EP  - 61
DO  - 10.1016/j.talanta.2013.03.071
ER  - 
@article{
author = "Tripković, T. and Charvy, C. and Alves, S. and Lolić, Aleksandar and Baošić, Rada and Nikolić-Mandić, Snežana D. and Tabet, J. C.",
year = "2013",
abstract = "Aim of this work is to propose an analytical protocol for proteinaceous binder identification in paintings using tryptic peptide analysis and MALDI-TOF mass spectrometry strengthened with MALDI-TOF/TOF tandem mass spectrometry (LIFT method). Proteinaceous binders are enzymatically digested with trypsin. From each individual protein frequently occurring in binders, a specific set of peptides is releasing during enzymatic digestion giving a peptide mass fingerprint (PMF) of that particular protein. The most intensive peptide peaks in PMF were determined and annotated with their corresponding amino acid sequence by MALDI-TOF/TOF analysis and subsequent database search. Before analyzing historical painting samples, procedure was tested and optimized on several painting model samples for a reliable and efficient identification of proteinaceous materials. The method is avoiding sample manipulation as much as possible in order to reduce sample loss. Since the applied procedures led to protein identification of binding media in model samples, MALDI-TOF/TOF was for the first time applied for analysis of proteinaceous binders in old painting samples.",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "Talanta",
title = "Identification of protein binders in artworks by MALDI-TOF/TOF tandem mass spectrometry",
volume = "113",
pages = "49-61",
doi = "10.1016/j.talanta.2013.03.071"
}
Tripković, T., Charvy, C., Alves, S., Lolić, A., Baošić, R., Nikolić-Mandić, S. D.,& Tabet, J. C.. (2013). Identification of protein binders in artworks by MALDI-TOF/TOF tandem mass spectrometry. in Talanta
Elsevier Science Bv, Amsterdam., 113, 49-61.
https://doi.org/10.1016/j.talanta.2013.03.071
Tripković T, Charvy C, Alves S, Lolić A, Baošić R, Nikolić-Mandić SD, Tabet JC. Identification of protein binders in artworks by MALDI-TOF/TOF tandem mass spectrometry. in Talanta. 2013;113:49-61.
doi:10.1016/j.talanta.2013.03.071 .
Tripković, T., Charvy, C., Alves, S., Lolić, Aleksandar, Baošić, Rada, Nikolić-Mandić, Snežana D., Tabet, J. C., "Identification of protein binders in artworks by MALDI-TOF/TOF tandem mass spectrometry" in Talanta, 113 (2013):49-61,
https://doi.org/10.1016/j.talanta.2013.03.071 . .
31
23
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Electrochemical behavior and antioxidant activity of tetradentate Schiff bases and their copper(II) complexes

Aburas, Najat M.; Lolić, Aleksandar; Stevanović, Nikola R.; Tripkovic, Tatjana; Nikolić-Mandić, Snežana D.; Baošić, Rada

(Springer, New York, 2012)

TY  - JOUR
AU  - Aburas, Najat M.
AU  - Lolić, Aleksandar
AU  - Stevanović, Nikola R.
AU  - Tripkovic, Tatjana
AU  - Nikolić-Mandić, Snežana D.
AU  - Baošić, Rada
PY  - 2012
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1547
AB  - This study describes the effects of the substituents on electrochemical behavior and antioxidant activity of the six tetradentate Schiff bases, containing ethane-1,2-diamine or propane-1,2-diamine as the amine part and pentane-2,4-dione and/or 1-phenylbutane-1,3-dione as beta-diketone, and corresponding copper(II) complexes. Cyclic voltammograms of these compounds were recorded in dimethylsulfoxide and 0.1 M sodium perchlorate as supporting electrolyte with glassy carbon as working electrode at different scan rates. The voltammograms of Schiff bases alone showed only one irreversible peak. Voltammograms recorded for complexes showed the presence of quasi-reversible processes taking place at the metal center and reversible process at the ligand part. Both steric and inductive effects of substituents and structure of imine bridge of Schiff base ligands as well as complexes were discussed. These effects appear relevant for the antioxidant activity. Antioxidant activity of the investigated compounds expressed as Trolox equivalent antioxidant capacity is also discussed. The electrochemical behavior showed a high correlation with the antioxidant activity for investigated compounds.
PB  - Springer, New York
T2  - Journal of the Iranian Chemical Society
T1  - Electrochemical behavior and antioxidant activity of tetradentate Schiff bases and their copper(II) complexes
VL  - 9
IS  - 6
SP  - 859
EP  - 864
DO  - 10.1007/s13738-012-0102-7
ER  - 
@article{
author = "Aburas, Najat M. and Lolić, Aleksandar and Stevanović, Nikola R. and Tripkovic, Tatjana and Nikolić-Mandić, Snežana D. and Baošić, Rada",
year = "2012",
abstract = "This study describes the effects of the substituents on electrochemical behavior and antioxidant activity of the six tetradentate Schiff bases, containing ethane-1,2-diamine or propane-1,2-diamine as the amine part and pentane-2,4-dione and/or 1-phenylbutane-1,3-dione as beta-diketone, and corresponding copper(II) complexes. Cyclic voltammograms of these compounds were recorded in dimethylsulfoxide and 0.1 M sodium perchlorate as supporting electrolyte with glassy carbon as working electrode at different scan rates. The voltammograms of Schiff bases alone showed only one irreversible peak. Voltammograms recorded for complexes showed the presence of quasi-reversible processes taking place at the metal center and reversible process at the ligand part. Both steric and inductive effects of substituents and structure of imine bridge of Schiff base ligands as well as complexes were discussed. These effects appear relevant for the antioxidant activity. Antioxidant activity of the investigated compounds expressed as Trolox equivalent antioxidant capacity is also discussed. The electrochemical behavior showed a high correlation with the antioxidant activity for investigated compounds.",
publisher = "Springer, New York",
journal = "Journal of the Iranian Chemical Society",
title = "Electrochemical behavior and antioxidant activity of tetradentate Schiff bases and their copper(II) complexes",
volume = "9",
number = "6",
pages = "859-864",
doi = "10.1007/s13738-012-0102-7"
}
Aburas, N. M., Lolić, A., Stevanović, N. R., Tripkovic, T., Nikolić-Mandić, S. D.,& Baošić, R.. (2012). Electrochemical behavior and antioxidant activity of tetradentate Schiff bases and their copper(II) complexes. in Journal of the Iranian Chemical Society
Springer, New York., 9(6), 859-864.
https://doi.org/10.1007/s13738-012-0102-7
Aburas NM, Lolić A, Stevanović NR, Tripkovic T, Nikolić-Mandić SD, Baošić R. Electrochemical behavior and antioxidant activity of tetradentate Schiff bases and their copper(II) complexes. in Journal of the Iranian Chemical Society. 2012;9(6):859-864.
doi:10.1007/s13738-012-0102-7 .
Aburas, Najat M., Lolić, Aleksandar, Stevanović, Nikola R., Tripkovic, Tatjana, Nikolić-Mandić, Snežana D., Baošić, Rada, "Electrochemical behavior and antioxidant activity of tetradentate Schiff bases and their copper(II) complexes" in Journal of the Iranian Chemical Society, 9, no. 6 (2012):859-864,
https://doi.org/10.1007/s13738-012-0102-7 . .
3
11
9
12
9

Development of a flow injection method with amperometric detection for the indirect determination of copper in drinking water samples

Lolić, Aleksandar; Tripkovic, Tatjana; Baošić, Rada; Nikolić-Mandić, Snežana D.; Stanimirović, Bojana

(Serbian Chemical Soc, Belgrade, 2012)

TY  - JOUR
AU  - Lolić, Aleksandar
AU  - Tripkovic, Tatjana
AU  - Baošić, Rada
AU  - Nikolić-Mandić, Snežana D.
AU  - Stanimirović, Bojana
PY  - 2012
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1569
AB  - A gas-diffusion flow injection method with amperometric detection for the indirect determination of copper on a silver electrode was developed. The flow through system was equipped with two injection valves and a gas-diffusion unit. In the first step, a signal of a cyanide solution was recorded. In the subsequent step, the signal of cyanide in the presence of copper was measured. Interferences (Cd(II), Co(II), Ag(I), Ni(II), Fe(III), Hg(II) and Zn(II)) were investigated and successfully removed. The calibration graph was linear in the range 1-90 mu mol dm(-3) of copper with a correlation coefficient of 0.993. The regression equation is I = (0.0455 +/- 0.0015)c + (0.4611 +/- 0.0671), where I is the relative signal decrease in mu A and c is concentration in mu mol dm(-3). Relative standard deviation for six consecutive injections of 30 mu mol dm(-3) copper(II) was 1.47 % and for 1 mu mol dm(-3) copper(II), it was 3.40 %. The detection limit, calculated as 3 s/m (where s is a standard deviation of nine measurement of a reagent blank and m is the slope of the calibration curve), was 0.32 mu mol dm(-3), which corresponds to 2.44 ng of copper(II) (the loop volume was 0.12 cm(3)). The method enables 60 analyses per hour and it was successfully applied for the determination of copper in drinking water samples.
AB  - Cilj ovog rada bio je razvoj gasno-difuzione protočno injekcione metode sa amperometrijskom detekcijom za indirektno određivanje bakra na srebrnoj elektrodi. Protočni sistem je opremljen sa dva injekciona ventila i gasno-difuzionom jedinicom. U prvom koraku snima se signal rastvora cijanida, a u drugom snima se signal pri istovremenom ubrizgavanju rastvora cijanida i rastvora bakra. Smetnje od Cd(II), Co(II), Ag(I), Ni(II), Fe(III), Hg(II) i Zn(II) su ispitane i uspešno uklonjene. Kalibraciona kriva je linearna u opsegu 1-90 μmol dm-3 bakra, koeficijent korelacije je 0,993, a jednačina prave I = (0,0455±0,0015)c + (0,4611±0,0671), gde je I razlika visine signala u μA, a c je koncentracija u μmol dm-3. Relativna standardna devijacija za šest uzastopnih ubrizgavanja rastvora bakra koncentracije 30 μmol dm-3 je 1,47 %, a za 1 μmol dm-3 rastvor Cu(II) je 3,40 %. Limit detekcije, izračunat kao 3s/m (gde je s standardna devijacija devet merenja slepe probe i m je nagib kalibracione prave), je 0,32 μmol dm-3, što odgovara 2,44 ng Cu(II) (zapremina petlje za uzorak je 0,12 cm3). Metoda omogućava 60 analiza po jednom satu i uspešno je primenjena za određivanje bakra u pijaćoj vodi.
PB  - Serbian Chemical Soc, Belgrade
T2  - Journal of the Serbian Chemical Society
T1  - Development of a flow injection method with amperometric detection for the indirect determination of copper in drinking water samples
T1  - Razvoj protočne injekcione metode za indirektno određivanje bakra sa amperometrijskom detekcijom u pijaćoj vodi
VL  - 77
IS  - 11
SP  - 1641
EP  - 1647
DO  - 10.2298/JSC120616090L
ER  - 
@article{
author = "Lolić, Aleksandar and Tripkovic, Tatjana and Baošić, Rada and Nikolić-Mandić, Snežana D. and Stanimirović, Bojana",
year = "2012",
abstract = "A gas-diffusion flow injection method with amperometric detection for the indirect determination of copper on a silver electrode was developed. The flow through system was equipped with two injection valves and a gas-diffusion unit. In the first step, a signal of a cyanide solution was recorded. In the subsequent step, the signal of cyanide in the presence of copper was measured. Interferences (Cd(II), Co(II), Ag(I), Ni(II), Fe(III), Hg(II) and Zn(II)) were investigated and successfully removed. The calibration graph was linear in the range 1-90 mu mol dm(-3) of copper with a correlation coefficient of 0.993. The regression equation is I = (0.0455 +/- 0.0015)c + (0.4611 +/- 0.0671), where I is the relative signal decrease in mu A and c is concentration in mu mol dm(-3). Relative standard deviation for six consecutive injections of 30 mu mol dm(-3) copper(II) was 1.47 % and for 1 mu mol dm(-3) copper(II), it was 3.40 %. The detection limit, calculated as 3 s/m (where s is a standard deviation of nine measurement of a reagent blank and m is the slope of the calibration curve), was 0.32 mu mol dm(-3), which corresponds to 2.44 ng of copper(II) (the loop volume was 0.12 cm(3)). The method enables 60 analyses per hour and it was successfully applied for the determination of copper in drinking water samples., Cilj ovog rada bio je razvoj gasno-difuzione protočno injekcione metode sa amperometrijskom detekcijom za indirektno određivanje bakra na srebrnoj elektrodi. Protočni sistem je opremljen sa dva injekciona ventila i gasno-difuzionom jedinicom. U prvom koraku snima se signal rastvora cijanida, a u drugom snima se signal pri istovremenom ubrizgavanju rastvora cijanida i rastvora bakra. Smetnje od Cd(II), Co(II), Ag(I), Ni(II), Fe(III), Hg(II) i Zn(II) su ispitane i uspešno uklonjene. Kalibraciona kriva je linearna u opsegu 1-90 μmol dm-3 bakra, koeficijent korelacije je 0,993, a jednačina prave I = (0,0455±0,0015)c + (0,4611±0,0671), gde je I razlika visine signala u μA, a c je koncentracija u μmol dm-3. Relativna standardna devijacija za šest uzastopnih ubrizgavanja rastvora bakra koncentracije 30 μmol dm-3 je 1,47 %, a za 1 μmol dm-3 rastvor Cu(II) je 3,40 %. Limit detekcije, izračunat kao 3s/m (gde je s standardna devijacija devet merenja slepe probe i m je nagib kalibracione prave), je 0,32 μmol dm-3, što odgovara 2,44 ng Cu(II) (zapremina petlje za uzorak je 0,12 cm3). Metoda omogućava 60 analiza po jednom satu i uspešno je primenjena za određivanje bakra u pijaćoj vodi.",
publisher = "Serbian Chemical Soc, Belgrade",
journal = "Journal of the Serbian Chemical Society",
title = "Development of a flow injection method with amperometric detection for the indirect determination of copper in drinking water samples, Razvoj protočne injekcione metode za indirektno određivanje bakra sa amperometrijskom detekcijom u pijaćoj vodi",
volume = "77",
number = "11",
pages = "1641-1647",
doi = "10.2298/JSC120616090L"
}
Lolić, A., Tripkovic, T., Baošić, R., Nikolić-Mandić, S. D.,& Stanimirović, B.. (2012). Development of a flow injection method with amperometric detection for the indirect determination of copper in drinking water samples. in Journal of the Serbian Chemical Society
Serbian Chemical Soc, Belgrade., 77(11), 1641-1647.
https://doi.org/10.2298/JSC120616090L
Lolić A, Tripkovic T, Baošić R, Nikolić-Mandić SD, Stanimirović B. Development of a flow injection method with amperometric detection for the indirect determination of copper in drinking water samples. in Journal of the Serbian Chemical Society. 2012;77(11):1641-1647.
doi:10.2298/JSC120616090L .
Lolić, Aleksandar, Tripkovic, Tatjana, Baošić, Rada, Nikolić-Mandić, Snežana D., Stanimirović, Bojana, "Development of a flow injection method with amperometric detection for the indirect determination of copper in drinking water samples" in Journal of the Serbian Chemical Society, 77, no. 11 (2012):1641-1647,
https://doi.org/10.2298/JSC120616090L . .
1
2
2
1

Enzymatic kinetic method for determination of propranolol hydrochloride in pharmaceuticals based on its inhibitory effect on cholinesterase

Stankov-Jovanović, Vesna P.; Mitić, Violeta D.; Ilić, Marija D.; Mandić, Ljuba M.; Nikolić-Mandić, Snežana D.

(Assoc Chemists & Chemical Engineers Of Serbia, Belgrade, 2012)

TY  - JOUR
AU  - Stankov-Jovanović, Vesna P.
AU  - Mitić, Violeta D.
AU  - Ilić, Marija D.
AU  - Mandić, Ljuba M.
AU  - Nikolić-Mandić, Snežana D.
PY  - 2012
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1598
AB  - Propranolol, a widely used beta-blocker, inhibits the hydrolysis reaction of enzyme cholinesterase. Measurements of the difference in rate of hydrolysis rate between uninhibited and inhibited reactions allow the development of a kinetic method for its determination. Both systems, enzyme-substrate-chromogen and enzyme-substrate-chromogen-inhibitor, were characterized through biochemical kinetic parameters (K-M, 0.326-0.330 mmol/L; V-max, 40.0-43.0 mu mol/Lmin). The inhibition type was recognized as competitive and the inhibition constant, Ki, was determined to be 22.60 mu mol/L. The detection and quantification limits were calculated as 0.004 and 0.0136 mu mol/L, respectively. Accuracy and precision of proposed methods were tested. The proposed method showed good sensitivity, selectivity, simplicity and rapidity, thus it is convenient for clinical applications.
AB  - Za propranolol, često propisivani neselektivni beta blokator, utvrđeno je da inhibira reakciju enzimske hidrolize butiriltioholin-jodida, koja je katalizovana serumskom holinesterazom. Merenjem razlike u brzini osnovne i inhibitorske reakcije hidrolize u prisustvu propranolola kao inhibitora, moguće je razviti kinetičku metodu za određivanje propranolola. Oba sistema, enzim-supstrat-hromogen kao i enzim-supstrat-hromogen-inhibitor, okarakterisani su biohemijskim kinetičkim parametrima (KM, 0,326-0,330 mmol/L; Vmax, 40-42,99 μmol/L min), inhibicija je definisana kao kompetitivna i određena je konstanta inhibicije 22,60 μmol/L. Da bi se u potpunosti iskoristile sve mogućnosti predložene metode u pogledu osetljivosti, tačnosti, preciznosti i selektivnosti, optimizovani su reakcioni uslovi. Konstruisana je kalibraciona prava, izračunata odgovarajuća jednačina i određeni granica detekcije i kvantifikacije i to 0,004 i 0,0136 μmol/L, redom. Tačnost i preciznost predložene metode su ispitane za tri koncentracije propranolola u oblasti kalibracione prave (0,082-21,120 μmol/L) u pet ponavljanja. Takođe, ispitan je uticaj većeg broja supstanci koje se mogu naći u uzorku na brzinu reakcije. Optimizovana metoda je primenjena za određivanje propranolola u farmaceutskim preparatima. Tačnost predložene metode je ispitana primenom metode standardnog dodatka. Predložena metoda ima dobru osetljivost, selektivnost, jednostavna je i brza, i nadasve lako dostupna, i na taj način primenljiva u velikom broju laboratorija.
PB  - Assoc Chemists & Chemical Engineers Of Serbia, Belgrade
T2  - Hemijska industrija
T1  - Enzymatic kinetic method for determination of propranolol hydrochloride in pharmaceuticals based on its inhibitory effect on cholinesterase
T1  - Enzimska kinetička metoda za određivanje propranolol-hidrohlorida u farmaceutskim preparatima zasnovana na njegovom inhibitorskom delovanju na holinesterazu
VL  - 66
IS  - 5
SP  - 677
EP  - 684
DO  - 10.2298/HEMIND120128032S
ER  - 
@article{
author = "Stankov-Jovanović, Vesna P. and Mitić, Violeta D. and Ilić, Marija D. and Mandić, Ljuba M. and Nikolić-Mandić, Snežana D.",
year = "2012",
abstract = "Propranolol, a widely used beta-blocker, inhibits the hydrolysis reaction of enzyme cholinesterase. Measurements of the difference in rate of hydrolysis rate between uninhibited and inhibited reactions allow the development of a kinetic method for its determination. Both systems, enzyme-substrate-chromogen and enzyme-substrate-chromogen-inhibitor, were characterized through biochemical kinetic parameters (K-M, 0.326-0.330 mmol/L; V-max, 40.0-43.0 mu mol/Lmin). The inhibition type was recognized as competitive and the inhibition constant, Ki, was determined to be 22.60 mu mol/L. The detection and quantification limits were calculated as 0.004 and 0.0136 mu mol/L, respectively. Accuracy and precision of proposed methods were tested. The proposed method showed good sensitivity, selectivity, simplicity and rapidity, thus it is convenient for clinical applications., Za propranolol, često propisivani neselektivni beta blokator, utvrđeno je da inhibira reakciju enzimske hidrolize butiriltioholin-jodida, koja je katalizovana serumskom holinesterazom. Merenjem razlike u brzini osnovne i inhibitorske reakcije hidrolize u prisustvu propranolola kao inhibitora, moguće je razviti kinetičku metodu za određivanje propranolola. Oba sistema, enzim-supstrat-hromogen kao i enzim-supstrat-hromogen-inhibitor, okarakterisani su biohemijskim kinetičkim parametrima (KM, 0,326-0,330 mmol/L; Vmax, 40-42,99 μmol/L min), inhibicija je definisana kao kompetitivna i određena je konstanta inhibicije 22,60 μmol/L. Da bi se u potpunosti iskoristile sve mogućnosti predložene metode u pogledu osetljivosti, tačnosti, preciznosti i selektivnosti, optimizovani su reakcioni uslovi. Konstruisana je kalibraciona prava, izračunata odgovarajuća jednačina i određeni granica detekcije i kvantifikacije i to 0,004 i 0,0136 μmol/L, redom. Tačnost i preciznost predložene metode su ispitane za tri koncentracije propranolola u oblasti kalibracione prave (0,082-21,120 μmol/L) u pet ponavljanja. Takođe, ispitan je uticaj većeg broja supstanci koje se mogu naći u uzorku na brzinu reakcije. Optimizovana metoda je primenjena za određivanje propranolola u farmaceutskim preparatima. Tačnost predložene metode je ispitana primenom metode standardnog dodatka. Predložena metoda ima dobru osetljivost, selektivnost, jednostavna je i brza, i nadasve lako dostupna, i na taj način primenljiva u velikom broju laboratorija.",
publisher = "Assoc Chemists & Chemical Engineers Of Serbia, Belgrade",
journal = "Hemijska industrija",
title = "Enzymatic kinetic method for determination of propranolol hydrochloride in pharmaceuticals based on its inhibitory effect on cholinesterase, Enzimska kinetička metoda za određivanje propranolol-hidrohlorida u farmaceutskim preparatima zasnovana na njegovom inhibitorskom delovanju na holinesterazu",
volume = "66",
number = "5",
pages = "677-684",
doi = "10.2298/HEMIND120128032S"
}
Stankov-Jovanović, V. P., Mitić, V. D., Ilić, M. D., Mandić, L. M.,& Nikolić-Mandić, S. D.. (2012). Enzymatic kinetic method for determination of propranolol hydrochloride in pharmaceuticals based on its inhibitory effect on cholinesterase. in Hemijska industrija
Assoc Chemists & Chemical Engineers Of Serbia, Belgrade., 66(5), 677-684.
https://doi.org/10.2298/HEMIND120128032S
Stankov-Jovanović VP, Mitić VD, Ilić MD, Mandić LM, Nikolić-Mandić SD. Enzymatic kinetic method for determination of propranolol hydrochloride in pharmaceuticals based on its inhibitory effect on cholinesterase. in Hemijska industrija. 2012;66(5):677-684.
doi:10.2298/HEMIND120128032S .
Stankov-Jovanović, Vesna P., Mitić, Violeta D., Ilić, Marija D., Mandić, Ljuba M., Nikolić-Mandić, Snežana D., "Enzymatic kinetic method for determination of propranolol hydrochloride in pharmaceuticals based on its inhibitory effect on cholinesterase" in Hemijska industrija, 66, no. 5 (2012):677-684,
https://doi.org/10.2298/HEMIND120128032S . .
3
2
3

Distribution and availability of potentially toxic metals in soil in central area of Belgrade, Serbia

Ghariani, Rabia Ahmed; Gržetić, Ivan; Antić, Mališa; Nikolić-Mandić, Snežana D.

(Springer Heidelberg, Heidelberg, 2010)

TY  - JOUR
AU  - Ghariani, Rabia Ahmed
AU  - Gržetić, Ivan
AU  - Antić, Mališa
AU  - Nikolić-Mandić, Snežana D.
PY  - 2010
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1114
AB  - Belgrade, capital city of Serbia, has over 1,600,000 inhabitants and over 400,000 vehicles trafficking every day on its streets. The investigation of soil pollution was performed by sequential extraction analysis to investigate the availability of potentially toxic metals (Zn, Cd, Pb, Co, Ni, Cu, Cr and Mn) under different oxidation and pH conditions. All investigated metals were mainly extracted from soils with neutral or acidic extractants. Serious pollution was observed along roads and streets with high traffic frequency, but Pb and Ni pollution was the highest since their concentrations exceed both soil Serbian standard and Canadian guidance values and is characteristic for all investigated sites. Cd, Cu, Cr and Zn concentrations are moderately high since they are between Canadian guideline and Serbian standard.
PB  - Springer Heidelberg, Heidelberg
T2  - Environmental Chemistry Letters
T1  - Distribution and availability of potentially toxic metals in soil in central area of Belgrade, Serbia
VL  - 8
IS  - 3
SP  - 261
EP  - 269
DO  - 10.1007/s10311-009-0215-0
ER  - 
@article{
author = "Ghariani, Rabia Ahmed and Gržetić, Ivan and Antić, Mališa and Nikolić-Mandić, Snežana D.",
year = "2010",
abstract = "Belgrade, capital city of Serbia, has over 1,600,000 inhabitants and over 400,000 vehicles trafficking every day on its streets. The investigation of soil pollution was performed by sequential extraction analysis to investigate the availability of potentially toxic metals (Zn, Cd, Pb, Co, Ni, Cu, Cr and Mn) under different oxidation and pH conditions. All investigated metals were mainly extracted from soils with neutral or acidic extractants. Serious pollution was observed along roads and streets with high traffic frequency, but Pb and Ni pollution was the highest since their concentrations exceed both soil Serbian standard and Canadian guidance values and is characteristic for all investigated sites. Cd, Cu, Cr and Zn concentrations are moderately high since they are between Canadian guideline and Serbian standard.",
publisher = "Springer Heidelberg, Heidelberg",
journal = "Environmental Chemistry Letters",
title = "Distribution and availability of potentially toxic metals in soil in central area of Belgrade, Serbia",
volume = "8",
number = "3",
pages = "261-269",
doi = "10.1007/s10311-009-0215-0"
}
Ghariani, R. A., Gržetić, I., Antić, M.,& Nikolić-Mandić, S. D.. (2010). Distribution and availability of potentially toxic metals in soil in central area of Belgrade, Serbia. in Environmental Chemistry Letters
Springer Heidelberg, Heidelberg., 8(3), 261-269.
https://doi.org/10.1007/s10311-009-0215-0
Ghariani RA, Gržetić I, Antić M, Nikolić-Mandić SD. Distribution and availability of potentially toxic metals in soil in central area of Belgrade, Serbia. in Environmental Chemistry Letters. 2010;8(3):261-269.
doi:10.1007/s10311-009-0215-0 .
Ghariani, Rabia Ahmed, Gržetić, Ivan, Antić, Mališa, Nikolić-Mandić, Snežana D., "Distribution and availability of potentially toxic metals in soil in central area of Belgrade, Serbia" in Environmental Chemistry Letters, 8, no. 3 (2010):261-269,
https://doi.org/10.1007/s10311-009-0215-0 . .
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Use of the sulfide minerals pyrite and chalcopyrite as electrochemical sensors in non-aqueous solutions. The potentiometric titration of weak acids in alcohols

Mihajlović, Ljiljana; Nikolić-Mandić, Snežana D.; Vukanovic, Branislav; Mihajlovic, Randel

(Versita, Warsaw 41, 2009)

TY  - JOUR
AU  - Mihajlović, Ljiljana
AU  - Nikolić-Mandić, Snežana D.
AU  - Vukanovic, Branislav
AU  - Mihajlovic, Randel
PY  - 2009
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/1016
AB  - Natural monocrystalline pyrite and chalcopyrite were examined as new indicator electrodes for the potentiometric titration of weak acids in tert-butanol and iso-propanol. The electrodes investigated demonstrated a linear dynamic response for p-toluenesulfonic acid concentrations in the range from 0.1 to 0.001 M, with a Nernstian slope of 48 mV per decade for pyrite in tert-butanol. Sodium methylate, potassium hydroxide and tetrabutylammonium hydroxide (TBAH) proved to be suitable titrating agents. The response time was less than 12 s and the lifetime of the electrodes was higher than 1 year. The advantages of the electrodes are long-term stability, rapid response, reproducibility, easy preparation and low cost.
PB  - Versita, Warsaw 41
T2  - Central European Journal of Chemistry
T1  - Use of the sulfide minerals pyrite and chalcopyrite as electrochemical sensors in non-aqueous solutions. The potentiometric titration of weak acids in alcohols
VL  - 7
IS  - 4
SP  - 900
EP  - 908
DO  - 10.2478/s11532-009-0074-3
ER  - 
@article{
author = "Mihajlović, Ljiljana and Nikolić-Mandić, Snežana D. and Vukanovic, Branislav and Mihajlovic, Randel",
year = "2009",
abstract = "Natural monocrystalline pyrite and chalcopyrite were examined as new indicator electrodes for the potentiometric titration of weak acids in tert-butanol and iso-propanol. The electrodes investigated demonstrated a linear dynamic response for p-toluenesulfonic acid concentrations in the range from 0.1 to 0.001 M, with a Nernstian slope of 48 mV per decade for pyrite in tert-butanol. Sodium methylate, potassium hydroxide and tetrabutylammonium hydroxide (TBAH) proved to be suitable titrating agents. The response time was less than 12 s and the lifetime of the electrodes was higher than 1 year. The advantages of the electrodes are long-term stability, rapid response, reproducibility, easy preparation and low cost.",
publisher = "Versita, Warsaw 41",
journal = "Central European Journal of Chemistry",
title = "Use of the sulfide minerals pyrite and chalcopyrite as electrochemical sensors in non-aqueous solutions. The potentiometric titration of weak acids in alcohols",
volume = "7",
number = "4",
pages = "900-908",
doi = "10.2478/s11532-009-0074-3"
}
Mihajlović, L., Nikolić-Mandić, S. D., Vukanovic, B.,& Mihajlovic, R.. (2009). Use of the sulfide minerals pyrite and chalcopyrite as electrochemical sensors in non-aqueous solutions. The potentiometric titration of weak acids in alcohols. in Central European Journal of Chemistry
Versita, Warsaw 41., 7(4), 900-908.
https://doi.org/10.2478/s11532-009-0074-3
Mihajlović L, Nikolić-Mandić SD, Vukanovic B, Mihajlovic R. Use of the sulfide minerals pyrite and chalcopyrite as electrochemical sensors in non-aqueous solutions. The potentiometric titration of weak acids in alcohols. in Central European Journal of Chemistry. 2009;7(4):900-908.
doi:10.2478/s11532-009-0074-3 .
Mihajlović, Ljiljana, Nikolić-Mandić, Snežana D., Vukanovic, Branislav, Mihajlovic, Randel, "Use of the sulfide minerals pyrite and chalcopyrite as electrochemical sensors in non-aqueous solutions. The potentiometric titration of weak acids in alcohols" in Central European Journal of Chemistry, 7, no. 4 (2009):900-908,
https://doi.org/10.2478/s11532-009-0074-3 . .
4
4
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3

Determination of iodide and bromide by flow methods with amperometric detection

Mutić, Jelena; Nikolić-Mandić, Snežana D.; Lolić, Aleksandar; Manojlović, Dragan D.

(Maik Nauka/Interperiodica/Springer, New York, 2008)

TY  - JOUR
AU  - Mutić, Jelena
AU  - Nikolić-Mandić, Snežana D.
AU  - Lolić, Aleksandar
AU  - Manojlović, Dragan D.
PY  - 2008
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/964
AB  - Determination of bromide and iodide in real samples (water, pharmaceutical preparations, and biological material) was performed using modified flow injection analyses (FIA) with amperometric detection on platinum electrode. As an additional confirmation of FIA experiments, cyclic voltammetry was employed. Iodide was determined by the kinetic method, its limit of detection was 1.0 nM, and the linearity was 0.1-100 mu M. The limit of detection for bromide determination was 50.0 nM and the calibration was linear for 2.5-100 mu M and 0.1-10 mM. The relative standard deviation for 1 mu M of iodide was 3.03% and, for 5 mu M of bromide, it was 1.23% (n = 6). Both methods enable 60 analyses per hour to be performed.
PB  - Maik Nauka/Interperiodica/Springer, New York
T2  - Journal of Analytical Chemistry
T1  - Determination of iodide and bromide by flow methods with amperometric detection
VL  - 63
IS  - 9
SP  - 907
EP  - 913
DO  - 10.1134/S1061934808090207
ER  - 
@article{
author = "Mutić, Jelena and Nikolić-Mandić, Snežana D. and Lolić, Aleksandar and Manojlović, Dragan D.",
year = "2008",
abstract = "Determination of bromide and iodide in real samples (water, pharmaceutical preparations, and biological material) was performed using modified flow injection analyses (FIA) with amperometric detection on platinum electrode. As an additional confirmation of FIA experiments, cyclic voltammetry was employed. Iodide was determined by the kinetic method, its limit of detection was 1.0 nM, and the linearity was 0.1-100 mu M. The limit of detection for bromide determination was 50.0 nM and the calibration was linear for 2.5-100 mu M and 0.1-10 mM. The relative standard deviation for 1 mu M of iodide was 3.03% and, for 5 mu M of bromide, it was 1.23% (n = 6). Both methods enable 60 analyses per hour to be performed.",
publisher = "Maik Nauka/Interperiodica/Springer, New York",
journal = "Journal of Analytical Chemistry",
title = "Determination of iodide and bromide by flow methods with amperometric detection",
volume = "63",
number = "9",
pages = "907-913",
doi = "10.1134/S1061934808090207"
}
Mutić, J., Nikolić-Mandić, S. D., Lolić, A.,& Manojlović, D. D.. (2008). Determination of iodide and bromide by flow methods with amperometric detection. in Journal of Analytical Chemistry
Maik Nauka/Interperiodica/Springer, New York., 63(9), 907-913.
https://doi.org/10.1134/S1061934808090207
Mutić J, Nikolić-Mandić SD, Lolić A, Manojlović DD. Determination of iodide and bromide by flow methods with amperometric detection. in Journal of Analytical Chemistry. 2008;63(9):907-913.
doi:10.1134/S1061934808090207 .
Mutić, Jelena, Nikolić-Mandić, Snežana D., Lolić, Aleksandar, Manojlović, Dragan D., "Determination of iodide and bromide by flow methods with amperometric detection" in Journal of Analytical Chemistry, 63, no. 9 (2008):907-913,
https://doi.org/10.1134/S1061934808090207 . .
2
2
2
2

Bromide determination in pharmaceutical preparations using indirect gas-diffusion flow injection method with amperometric detector

Mutić, Jelena; Nikolić-Mandić, Snežana D.; Lolić, Aleksandar; Manojlović, Dragan D.

(Hard, Olsztyn 5, 2007)

TY  - JOUR
AU  - Mutić, Jelena
AU  - Nikolić-Mandić, Snežana D.
AU  - Lolić, Aleksandar
AU  - Manojlović, Dragan D.
PY  - 2007
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/869
AB  - The indirect gas-diffusion flow injection method (FI) was modified, optimized and successfully applied to bromide determination in various samples such as active substances, drugs, organic substances and water samples. The method is based on the oxidation of bromide to bromine in acidic medium, which diffuses through PTFE membrane into the acceptor flow that carried bromine to the amperometric cell. The flow amperometric detection was carried out at the potential of +0.65 V (vs Ag/AgCl) when injected sample volume was 100 mu L. Results obtained by FIA were confirmed by cyclic voltarnmetry (CV). The linear calibration graph was obtained over the concentration range 0.1-10x10(-3) mol/L and 2.5-100x10(-6) mol/L bromide solutions. Relative standard deviation was 1.23% for 5x10(-6) mol/L bromide solution and 0. 11% for 0.25x10(-3)mol/L bromide solution (n=6, for both cases). The limit of detection was 5x10(-1) mol/L. The described method requires small quantities of samples and prior extraction of the analytes is not necessary. The method enables 60 analyses per hour.
PB  - Hard, Olsztyn 5
T2  - Polish Journal of Environmental Studies
T1  - Bromide determination in pharmaceutical preparations using indirect gas-diffusion flow injection method with amperometric detector
VL  - 16
IS  - 5
SP  - 739
EP  - 744
UR  - https://hdl.handle.net/21.15107/rcub_cherry_869
ER  - 
@article{
author = "Mutić, Jelena and Nikolić-Mandić, Snežana D. and Lolić, Aleksandar and Manojlović, Dragan D.",
year = "2007",
abstract = "The indirect gas-diffusion flow injection method (FI) was modified, optimized and successfully applied to bromide determination in various samples such as active substances, drugs, organic substances and water samples. The method is based on the oxidation of bromide to bromine in acidic medium, which diffuses through PTFE membrane into the acceptor flow that carried bromine to the amperometric cell. The flow amperometric detection was carried out at the potential of +0.65 V (vs Ag/AgCl) when injected sample volume was 100 mu L. Results obtained by FIA were confirmed by cyclic voltarnmetry (CV). The linear calibration graph was obtained over the concentration range 0.1-10x10(-3) mol/L and 2.5-100x10(-6) mol/L bromide solutions. Relative standard deviation was 1.23% for 5x10(-6) mol/L bromide solution and 0. 11% for 0.25x10(-3)mol/L bromide solution (n=6, for both cases). The limit of detection was 5x10(-1) mol/L. The described method requires small quantities of samples and prior extraction of the analytes is not necessary. The method enables 60 analyses per hour.",
publisher = "Hard, Olsztyn 5",
journal = "Polish Journal of Environmental Studies",
title = "Bromide determination in pharmaceutical preparations using indirect gas-diffusion flow injection method with amperometric detector",
volume = "16",
number = "5",
pages = "739-744",
url = "https://hdl.handle.net/21.15107/rcub_cherry_869"
}
Mutić, J., Nikolić-Mandić, S. D., Lolić, A.,& Manojlović, D. D.. (2007). Bromide determination in pharmaceutical preparations using indirect gas-diffusion flow injection method with amperometric detector. in Polish Journal of Environmental Studies
Hard, Olsztyn 5., 16(5), 739-744.
https://hdl.handle.net/21.15107/rcub_cherry_869
Mutić J, Nikolić-Mandić SD, Lolić A, Manojlović DD. Bromide determination in pharmaceutical preparations using indirect gas-diffusion flow injection method with amperometric detector. in Polish Journal of Environmental Studies. 2007;16(5):739-744.
https://hdl.handle.net/21.15107/rcub_cherry_869 .
Mutić, Jelena, Nikolić-Mandić, Snežana D., Lolić, Aleksandar, Manojlović, Dragan D., "Bromide determination in pharmaceutical preparations using indirect gas-diffusion flow injection method with amperometric detector" in Polish Journal of Environmental Studies, 16, no. 5 (2007):739-744,
https://hdl.handle.net/21.15107/rcub_cherry_869 .

A modification of the kinetic determination of pancuronium bromide based on its inhibitory effect on cholinesterase

Stankov-Jovanović, Vesna P.; Nikolić-Mandić, Snežana D.; Mandić, Ljuba M.; Mitić, Violeta D.

(Wiley-Liss, Hoboken, 2007)

TY  - JOUR
AU  - Stankov-Jovanović, Vesna P.
AU  - Nikolić-Mandić, Snežana D.
AU  - Mandić, Ljuba M.
AU  - Mitić, Violeta D.
PY  - 2007
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/825
AB  - A modification of the existing spectrophotometric kinetic method for the determination of pancuronium bromide (PCBr), based on pooled human serum cholinesterase (ChE, EC 3.1.1.8 acylcholine acylhydrolase) inhibition, was developed. Butyrylthiocholine iodide (concentration 1.667 mmol/L) was used as substrate and determination was performed at pH 7.6. Essential basic kinetic parameters were also determined: Michaelis-Menten's constant K-M=0.33 mmol/L, maximal reaction rate V-max=42.29 mu mol/ L min, inhibition constant K-I = 0.34 mu mol/L, and IC50=0.235 mu mol/L. Linear dependence between the reaction rate and the inhibitor concentration exists in PCBr concentration range 8.29-265.28 nmol/L, which corresponds to the real sample concentrations from 0.166 to 5.306 mu mol/L. The method detection limit was established to be 1.86 nmol/L and the quantification limit was 6.18 nmol/L. Precision of the method was tested for three pancuronium concentrations (16.58, 99.48, and 198.96 nmol/L). The relative standard deviation (RSD) was in the range 0.78-5.13%. Accuracy was examined by the standard addition method. The influence of substances usually present in serum and urine on the reaction rate was determined. The method developed was applied for PCBr determination in spiked serum and urine samples and in the urine taken during surgery. The method was proven to have good sensitivity, accuracy, and precision and can be considered suitable for clinical practice.
PB  - Wiley-Liss, Hoboken
T2  - Journal of Clinical Laboratory Analysis
T1  - A modification of the kinetic determination of pancuronium bromide based on its inhibitory effect on cholinesterase
VL  - 21
IS  - 2
SP  - 124
EP  - 131
DO  - 10.1002/jcla.20162
ER  - 
@article{
author = "Stankov-Jovanović, Vesna P. and Nikolić-Mandić, Snežana D. and Mandić, Ljuba M. and Mitić, Violeta D.",
year = "2007",
abstract = "A modification of the existing spectrophotometric kinetic method for the determination of pancuronium bromide (PCBr), based on pooled human serum cholinesterase (ChE, EC 3.1.1.8 acylcholine acylhydrolase) inhibition, was developed. Butyrylthiocholine iodide (concentration 1.667 mmol/L) was used as substrate and determination was performed at pH 7.6. Essential basic kinetic parameters were also determined: Michaelis-Menten's constant K-M=0.33 mmol/L, maximal reaction rate V-max=42.29 mu mol/ L min, inhibition constant K-I = 0.34 mu mol/L, and IC50=0.235 mu mol/L. Linear dependence between the reaction rate and the inhibitor concentration exists in PCBr concentration range 8.29-265.28 nmol/L, which corresponds to the real sample concentrations from 0.166 to 5.306 mu mol/L. The method detection limit was established to be 1.86 nmol/L and the quantification limit was 6.18 nmol/L. Precision of the method was tested for three pancuronium concentrations (16.58, 99.48, and 198.96 nmol/L). The relative standard deviation (RSD) was in the range 0.78-5.13%. Accuracy was examined by the standard addition method. The influence of substances usually present in serum and urine on the reaction rate was determined. The method developed was applied for PCBr determination in spiked serum and urine samples and in the urine taken during surgery. The method was proven to have good sensitivity, accuracy, and precision and can be considered suitable for clinical practice.",
publisher = "Wiley-Liss, Hoboken",
journal = "Journal of Clinical Laboratory Analysis",
title = "A modification of the kinetic determination of pancuronium bromide based on its inhibitory effect on cholinesterase",
volume = "21",
number = "2",
pages = "124-131",
doi = "10.1002/jcla.20162"
}
Stankov-Jovanović, V. P., Nikolić-Mandić, S. D., Mandić, L. M.,& Mitić, V. D.. (2007). A modification of the kinetic determination of pancuronium bromide based on its inhibitory effect on cholinesterase. in Journal of Clinical Laboratory Analysis
Wiley-Liss, Hoboken., 21(2), 124-131.
https://doi.org/10.1002/jcla.20162
Stankov-Jovanović VP, Nikolić-Mandić SD, Mandić LM, Mitić VD. A modification of the kinetic determination of pancuronium bromide based on its inhibitory effect on cholinesterase. in Journal of Clinical Laboratory Analysis. 2007;21(2):124-131.
doi:10.1002/jcla.20162 .
Stankov-Jovanović, Vesna P., Nikolić-Mandić, Snežana D., Mandić, Ljuba M., Mitić, Violeta D., "A modification of the kinetic determination of pancuronium bromide based on its inhibitory effect on cholinesterase" in Journal of Clinical Laboratory Analysis, 21, no. 2 (2007):124-131,
https://doi.org/10.1002/jcla.20162 . .
5
8
7
5

Cholinesterase inhibition based determination of pancuronium bromide in biological samples

Stankov-Jovanović, Vesna P.; Nikolić-Mandić, Snežana D.; Mandić, Ljuba M.; Mitić, Violeta D.

(Springer Heidelberg, Heidelberg, 2006)

TY  - JOUR
AU  - Stankov-Jovanović, Vesna P.
AU  - Nikolić-Mandić, Snežana D.
AU  - Mandić, Ljuba M.
AU  - Mitić, Violeta D.
PY  - 2006
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/794
AB  - Pancuronium bromide (PCBr) inhibition effect on enzyme cholinesterase from pooled human serum (Che, EC 3.1.1.8 acylcholine acylhydrolase) was used for development of a spectrophotometric kinetic method for PCBr determination in human serum and urine. Optimal conditions for the basic and inhibitor reactions were established: pH=7.7 and substrate concentration c(benzoylcholine chloride)=1.33 mmol/L. Kinetic parameters were also determined: Michaelis-Menten's constant K-M=0.40 mmol/L, maximal reaction rate V-max=52.2 mu mol/L min, inhibition constant K-i=0,56 mu mol/L and IC50=1.31 mu mol/L. Linear dependence between the reaction rate and inhibitor concentration exists in PCBr concentration range 8.20-68.25 nmol/L, which corresponds to the real sample concentrations from 0.328 to 2.730 mu mol/L. The method detection and quantification limits were 2.01 nmol/L and 6.67 nmol/L, respectively. Precision of the method was tested for three pancuronium concentrations (10.70, 29.35 and 51.25 nmol/L). Relative standard deviation (RSD) was in the range 0.15-7.45%. Accuracy was examined by standard addition method. Influence of the substances usually present in serum and urine on the reaction rate was tested. The developed method was applied for PCBr content determination in serum model samples, urine model samples and in urine taken during surgery. The method has good sensitivity, accuracy, precision and it is suitable for clinical practice.
PB  - Springer Heidelberg, Heidelberg
T2  - Analytical and Bioanalytical Chemistry
T1  - Cholinesterase inhibition based determination of pancuronium bromide in biological samples
VL  - 385
IS  - 8
SP  - 1462
EP  - 1469
DO  - 10.1007/s00216-006-0556-5
ER  - 
@article{
author = "Stankov-Jovanović, Vesna P. and Nikolić-Mandić, Snežana D. and Mandić, Ljuba M. and Mitić, Violeta D.",
year = "2006",
abstract = "Pancuronium bromide (PCBr) inhibition effect on enzyme cholinesterase from pooled human serum (Che, EC 3.1.1.8 acylcholine acylhydrolase) was used for development of a spectrophotometric kinetic method for PCBr determination in human serum and urine. Optimal conditions for the basic and inhibitor reactions were established: pH=7.7 and substrate concentration c(benzoylcholine chloride)=1.33 mmol/L. Kinetic parameters were also determined: Michaelis-Menten's constant K-M=0.40 mmol/L, maximal reaction rate V-max=52.2 mu mol/L min, inhibition constant K-i=0,56 mu mol/L and IC50=1.31 mu mol/L. Linear dependence between the reaction rate and inhibitor concentration exists in PCBr concentration range 8.20-68.25 nmol/L, which corresponds to the real sample concentrations from 0.328 to 2.730 mu mol/L. The method detection and quantification limits were 2.01 nmol/L and 6.67 nmol/L, respectively. Precision of the method was tested for three pancuronium concentrations (10.70, 29.35 and 51.25 nmol/L). Relative standard deviation (RSD) was in the range 0.15-7.45%. Accuracy was examined by standard addition method. Influence of the substances usually present in serum and urine on the reaction rate was tested. The developed method was applied for PCBr content determination in serum model samples, urine model samples and in urine taken during surgery. The method has good sensitivity, accuracy, precision and it is suitable for clinical practice.",
publisher = "Springer Heidelberg, Heidelberg",
journal = "Analytical and Bioanalytical Chemistry",
title = "Cholinesterase inhibition based determination of pancuronium bromide in biological samples",
volume = "385",
number = "8",
pages = "1462-1469",
doi = "10.1007/s00216-006-0556-5"
}
Stankov-Jovanović, V. P., Nikolić-Mandić, S. D., Mandić, L. M.,& Mitić, V. D.. (2006). Cholinesterase inhibition based determination of pancuronium bromide in biological samples. in Analytical and Bioanalytical Chemistry
Springer Heidelberg, Heidelberg., 385(8), 1462-1469.
https://doi.org/10.1007/s00216-006-0556-5
Stankov-Jovanović VP, Nikolić-Mandić SD, Mandić LM, Mitić VD. Cholinesterase inhibition based determination of pancuronium bromide in biological samples. in Analytical and Bioanalytical Chemistry. 2006;385(8):1462-1469.
doi:10.1007/s00216-006-0556-5 .
Stankov-Jovanović, Vesna P., Nikolić-Mandić, Snežana D., Mandić, Ljuba M., Mitić, Violeta D., "Cholinesterase inhibition based determination of pancuronium bromide in biological samples" in Analytical and Bioanalytical Chemistry, 385, no. 8 (2006):1462-1469,
https://doi.org/10.1007/s00216-006-0556-5 . .
5
5
5
4

Eco-chemical characterisation of fluvisol of Velika Morava River valley (Serbia) based on the physico-chemical. parameters and distribution of heavy metals

Antic, Ana; Cvetković, Olga; Jovančićević, Branimir; Blagojević, Srđan; Nikolić-Mandić, Snežana D.

(Parlar Scientific Publications (P S P), Freising, 2006)

TY  - JOUR
AU  - Antic, Ana
AU  - Cvetković, Olga
AU  - Jovančićević, Branimir
AU  - Blagojević, Srđan
AU  - Nikolić-Mandić, Snežana D.
PY  - 2006
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/810
AB  - Eco-chemical characteristics of the soil from the Velika Morava River valley were examined by analysis of 27 samples of agricultural soil of fluvisol type. The main physico-chemical parameters (pH, carbonate, humus, total nitrogen, available potassium and phosphorus contents), and total and available contents of heavy metals (Pb, Zn, Cu and Cd) were determined. The aim of this research was to have an insight into the current eco-chemical state in the examined agricultural region, by detection of the main substrates of heavy metals, as well as by analysis of their possible origin. In all the examined samples, total Zn, Cu and Cd contents, and in most of the examined samples, total contents of Pb, obtained by sequential extraction, were below maximum allowed concentrations (MAC) for agricultural soils. The increased content of total Pb (104.28-161.03 mg/kg) in some of the examined samples was probably caused by anthropogenic activity. Results of the sequential extraction, as, well as the extraction with diethylene triamine pentaacetic acid (DTPA), used for extraction of available metals, indicated the anthropogenic sources of Pb, Cu and Cd, whereas Zn was most often of geochemical, native origin. The obtained results were subject to correlation and factor analysis. Both methods confirmed the correlation between Zn and Cd, leading to the conclusion that a part of Zn was also of, anthropogenic origin. Factor analysis brought together total contents of Zn and Cd, and pH-value of the soil, and indicated the possibility of its easy mobilisation at slight changes in soil acidity.
PB  - Parlar Scientific Publications (P S P), Freising
T2  - Fresenius Environmental Bulletin
T1  - Eco-chemical characterisation of fluvisol of Velika Morava River valley (Serbia) based on the physico-chemical. parameters and distribution of heavy metals
VL  - 15
IS  - 11
SP  - 1434
EP  - 1441
UR  - https://hdl.handle.net/21.15107/rcub_cherry_810
ER  - 
@article{
author = "Antic, Ana and Cvetković, Olga and Jovančićević, Branimir and Blagojević, Srđan and Nikolić-Mandić, Snežana D.",
year = "2006",
abstract = "Eco-chemical characteristics of the soil from the Velika Morava River valley were examined by analysis of 27 samples of agricultural soil of fluvisol type. The main physico-chemical parameters (pH, carbonate, humus, total nitrogen, available potassium and phosphorus contents), and total and available contents of heavy metals (Pb, Zn, Cu and Cd) were determined. The aim of this research was to have an insight into the current eco-chemical state in the examined agricultural region, by detection of the main substrates of heavy metals, as well as by analysis of their possible origin. In all the examined samples, total Zn, Cu and Cd contents, and in most of the examined samples, total contents of Pb, obtained by sequential extraction, were below maximum allowed concentrations (MAC) for agricultural soils. The increased content of total Pb (104.28-161.03 mg/kg) in some of the examined samples was probably caused by anthropogenic activity. Results of the sequential extraction, as, well as the extraction with diethylene triamine pentaacetic acid (DTPA), used for extraction of available metals, indicated the anthropogenic sources of Pb, Cu and Cd, whereas Zn was most often of geochemical, native origin. The obtained results were subject to correlation and factor analysis. Both methods confirmed the correlation between Zn and Cd, leading to the conclusion that a part of Zn was also of, anthropogenic origin. Factor analysis brought together total contents of Zn and Cd, and pH-value of the soil, and indicated the possibility of its easy mobilisation at slight changes in soil acidity.",
publisher = "Parlar Scientific Publications (P S P), Freising",
journal = "Fresenius Environmental Bulletin",
title = "Eco-chemical characterisation of fluvisol of Velika Morava River valley (Serbia) based on the physico-chemical. parameters and distribution of heavy metals",
volume = "15",
number = "11",
pages = "1434-1441",
url = "https://hdl.handle.net/21.15107/rcub_cherry_810"
}
Antic, A., Cvetković, O., Jovančićević, B., Blagojević, S.,& Nikolić-Mandić, S. D.. (2006). Eco-chemical characterisation of fluvisol of Velika Morava River valley (Serbia) based on the physico-chemical. parameters and distribution of heavy metals. in Fresenius Environmental Bulletin
Parlar Scientific Publications (P S P), Freising., 15(11), 1434-1441.
https://hdl.handle.net/21.15107/rcub_cherry_810
Antic A, Cvetković O, Jovančićević B, Blagojević S, Nikolić-Mandić SD. Eco-chemical characterisation of fluvisol of Velika Morava River valley (Serbia) based on the physico-chemical. parameters and distribution of heavy metals. in Fresenius Environmental Bulletin. 2006;15(11):1434-1441.
https://hdl.handle.net/21.15107/rcub_cherry_810 .
Antic, Ana, Cvetković, Olga, Jovančićević, Branimir, Blagojević, Srđan, Nikolić-Mandić, Snežana D., "Eco-chemical characterisation of fluvisol of Velika Morava River valley (Serbia) based on the physico-chemical. parameters and distribution of heavy metals" in Fresenius Environmental Bulletin, 15, no. 11 (2006):1434-1441,
https://hdl.handle.net/21.15107/rcub_cherry_810 .
5
6

Kinetic spectrophotometric method for gold(III) determination

Rancic, SM; Nikolić-Mandić, Snežana D.; Mandić, Ljuba M.

(Elsevier Science Bv, Amsterdam, 2005)

TY  - JOUR
AU  - Rancic, SM
AU  - Nikolić-Mandić, Snežana D.
AU  - Mandić, Ljuba M.
PY  - 2005
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/726
AB  - The kinetic spectrophotometric method for Au(III) determination was developed and validated. It was based on the catalytic effect of gold on the oxidation of methylene blue B (3,7di-(dimethyl amino)-10-dehydro-phenotiazin chloride) by ammonium peroxo-disulfate in citric buffer solution. There was the linearity of the calibration curve in the concentration range from 0.09 to 2.90 mu g ml(-1) Au(III). The relative standard deviation was 2.50% and correlation coefficient of 0.9999. The limit of detection was determined as signal to noise ratio (3: 1) and it was 5.5 ng ml(-1). The limit of quantification, based on signal to noise ratio 10: 1 was 19.25 ng ml(-1). The selectivity was tested on the basis of influence of known amounts of different ions in the reaction mixture, upon the reaction rate. Kinetic and thermodynamic parameters were reported for both catalytic and non-catalytic reactions. The method was verified by Au(III) determination in anti-rheumatic drug "Thuredon" and in human urine samples, using ICP-AES as the comparative method. As the method is accurate, reliable, quick and simple it could be useful for clinical and toxicological practice. (c) 2004 Elsevier B.V. All rights reserved.
PB  - Elsevier Science Bv, Amsterdam
T2  - Analytica Chimica Acta
T1  - Kinetic spectrophotometric method for gold(III) determination
VL  - 547
IS  - 1
SP  - 144
EP  - 149
DO  - 10.1016/j.aca.2004.11.078
ER  - 
@article{
author = "Rancic, SM and Nikolić-Mandić, Snežana D. and Mandić, Ljuba M.",
year = "2005",
abstract = "The kinetic spectrophotometric method for Au(III) determination was developed and validated. It was based on the catalytic effect of gold on the oxidation of methylene blue B (3,7di-(dimethyl amino)-10-dehydro-phenotiazin chloride) by ammonium peroxo-disulfate in citric buffer solution. There was the linearity of the calibration curve in the concentration range from 0.09 to 2.90 mu g ml(-1) Au(III). The relative standard deviation was 2.50% and correlation coefficient of 0.9999. The limit of detection was determined as signal to noise ratio (3: 1) and it was 5.5 ng ml(-1). The limit of quantification, based on signal to noise ratio 10: 1 was 19.25 ng ml(-1). The selectivity was tested on the basis of influence of known amounts of different ions in the reaction mixture, upon the reaction rate. Kinetic and thermodynamic parameters were reported for both catalytic and non-catalytic reactions. The method was verified by Au(III) determination in anti-rheumatic drug "Thuredon" and in human urine samples, using ICP-AES as the comparative method. As the method is accurate, reliable, quick and simple it could be useful for clinical and toxicological practice. (c) 2004 Elsevier B.V. All rights reserved.",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "Analytica Chimica Acta",
title = "Kinetic spectrophotometric method for gold(III) determination",
volume = "547",
number = "1",
pages = "144-149",
doi = "10.1016/j.aca.2004.11.078"
}
Rancic, S., Nikolić-Mandić, S. D.,& Mandić, L. M.. (2005). Kinetic spectrophotometric method for gold(III) determination. in Analytica Chimica Acta
Elsevier Science Bv, Amsterdam., 547(1), 144-149.
https://doi.org/10.1016/j.aca.2004.11.078
Rancic S, Nikolić-Mandić SD, Mandić LM. Kinetic spectrophotometric method for gold(III) determination. in Analytica Chimica Acta. 2005;547(1):144-149.
doi:10.1016/j.aca.2004.11.078 .
Rancic, SM, Nikolić-Mandić, Snežana D., Mandić, Ljuba M., "Kinetic spectrophotometric method for gold(III) determination" in Analytica Chimica Acta, 547, no. 1 (2005):144-149,
https://doi.org/10.1016/j.aca.2004.11.078 . .
23
26
31
19

Degradation of transformer oil on the basis of polychlorinated bifenyls without degrading the existing quality of the environment

Manojlović, Dragan D.; Cvetković, Olga; Nikolić-Mandić, Snežana D.

(2003)

TY  - JOUR
AU  - Manojlović, Dragan D.
AU  - Cvetković, Olga
AU  - Nikolić-Mandić, Snežana D.
PY  - 2003
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/220
AB  - This paper deals with results of laboratory experiments referring to transformer oil chemical degradation on the basis of polychlorinated bifenyls, results referring to rinsing of transformer insulation material, as well as application of "domestic" sorbent for removal of PCB from the environment. The degradations were performed by means of two different degradation devices and several different degradation procedures. Analysis of obtained degradation products from all applied procedures proved that degradation products are environmentally harmless products.
AB  - U ovom radu su prikazani rezultati eksperimenata hemijske degradacije transformatorskog ulja na bazi PCB, postignuti u laboratorijskim uslovima rezultati ispiranja izolacionog materijala transformatora, kao i primena "domaćeg" sorbenta za odstranjivanje polihlorovanih bifenila iz životne sredine. Degradacije su izvedene sa dva različita degradaciona sredstva i nekoliko različitih degradacionih postupaka. Analizom dobijenih degradacionih proizvoda iz svih primenjenih postupaka, ustanovljeno je da degradacioni proizvodi predstavljaju ekološki bezopasne proizvode.
T2  - Elektroprivreda
T1  - Degradation of transformer oil on the basis of polychlorinated bifenyls without degrading the existing quality of the environment
T1  - Degradacija transformatorskog ulja na bazi polihlorovanih bifenila bez narušavanja postojećeg kvaliteta životne sredine
VL  - 56
IS  - 2
SP  - 35
EP  - 40
UR  - https://hdl.handle.net/21.15107/rcub_cherry_220
ER  - 
@article{
author = "Manojlović, Dragan D. and Cvetković, Olga and Nikolić-Mandić, Snežana D.",
year = "2003",
abstract = "This paper deals with results of laboratory experiments referring to transformer oil chemical degradation on the basis of polychlorinated bifenyls, results referring to rinsing of transformer insulation material, as well as application of "domestic" sorbent for removal of PCB from the environment. The degradations were performed by means of two different degradation devices and several different degradation procedures. Analysis of obtained degradation products from all applied procedures proved that degradation products are environmentally harmless products., U ovom radu su prikazani rezultati eksperimenata hemijske degradacije transformatorskog ulja na bazi PCB, postignuti u laboratorijskim uslovima rezultati ispiranja izolacionog materijala transformatora, kao i primena "domaćeg" sorbenta za odstranjivanje polihlorovanih bifenila iz životne sredine. Degradacije su izvedene sa dva različita degradaciona sredstva i nekoliko različitih degradacionih postupaka. Analizom dobijenih degradacionih proizvoda iz svih primenjenih postupaka, ustanovljeno je da degradacioni proizvodi predstavljaju ekološki bezopasne proizvode.",
journal = "Elektroprivreda",
title = "Degradation of transformer oil on the basis of polychlorinated bifenyls without degrading the existing quality of the environment, Degradacija transformatorskog ulja na bazi polihlorovanih bifenila bez narušavanja postojećeg kvaliteta životne sredine",
volume = "56",
number = "2",
pages = "35-40",
url = "https://hdl.handle.net/21.15107/rcub_cherry_220"
}
Manojlović, D. D., Cvetković, O.,& Nikolić-Mandić, S. D.. (2003). Degradation of transformer oil on the basis of polychlorinated bifenyls without degrading the existing quality of the environment. in Elektroprivreda, 56(2), 35-40.
https://hdl.handle.net/21.15107/rcub_cherry_220
Manojlović DD, Cvetković O, Nikolić-Mandić SD. Degradation of transformer oil on the basis of polychlorinated bifenyls without degrading the existing quality of the environment. in Elektroprivreda. 2003;56(2):35-40.
https://hdl.handle.net/21.15107/rcub_cherry_220 .
Manojlović, Dragan D., Cvetković, Olga, Nikolić-Mandić, Snežana D., "Degradation of transformer oil on the basis of polychlorinated bifenyls without degrading the existing quality of the environment" in Elektroprivreda, 56, no. 2 (2003):35-40,
https://hdl.handle.net/21.15107/rcub_cherry_220 .

Optimization and application of the gas-diffusion flow injection method for the determination of chloride

Lolić, Aleksandar; Nikolić-Mandić, Snežana D.; Polić, Predrag S.

(Serbian Chemical Soc, Belgrade, 2001)

TY  - JOUR
AU  - Lolić, Aleksandar
AU  - Nikolić-Mandić, Snežana D.
AU  - Polić, Predrag S.
PY  - 2001
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/473
AB  - A selective and sensitive procedure for the fast and indirect determination of chloride by the gas-diffusion FIA method has been optimized and applied for the determination of chloride in water samples which contained different amounts of the analyte. The examined samples were: seawater, tap water and very pure water from the water-steam system of the power plant "Nikola Tesla B" in Obrenovac. Application of an amperometric detector (model LC-17A; BAS, West Lafayette, USA) enables the detection limit to be decreased down to 0.05 mu mol/dm(3) of chloride, which col responds to 35.5 pg, and adjustment of the acceptor flow rate and direction inside the gas-diffusion unit. In this way the optimized FIA system has excellent repeatability. For 5 mu mol/dm(3) it was found to be 1.11% (n = 5). The throughput of this method is 60 samples per hour.
AB  - Selektivan i osetljiv postupak za brzo, indirektno određivanje hlorida gasno-difuzionom metodom otpimizovan je i primenjen za određivanje hlorida u uzorcima voda sa vrlo različitim sadržajem ove vrste: morskoj, vodi za piće i vrlo čistim vodama u sistemu voda-para TE "Nikola Tesna B" u Obrenovcu. Upotreba amperometrijskog detektora tipa LC-17A omogućava snižavanje granice detekcije na 0.05 μmol/dm3 hlorida (što za uzorak zapremine 0.2 cm3 iznosi 35.5 pg) i podešavanje brzine i smera toka u gasno-difuzionoj jedinici. Ovako optimizovan protočni sistem ima odličnu reproduktivnost. Za hloridni standard koncentracije 5 μmol/dm3 relativna standardna devijacija iznosi 1.11 % (n = 5).
PB  - Serbian Chemical Soc, Belgrade
T2  - Journal of the Serbian Chemical Society
T1  - Optimization and application of the gas-diffusion flow injection method for the determination of chloride
T1  - Optimizacija i primena gasno-difuzione protočne injekcione metode za određivanje hlorida
VL  - 66
IS  - 9
SP  - 637
EP  - 646
UR  - https://hdl.handle.net/21.15107/rcub_cherry_473
ER  - 
@article{
author = "Lolić, Aleksandar and Nikolić-Mandić, Snežana D. and Polić, Predrag S.",
year = "2001",
abstract = "A selective and sensitive procedure for the fast and indirect determination of chloride by the gas-diffusion FIA method has been optimized and applied for the determination of chloride in water samples which contained different amounts of the analyte. The examined samples were: seawater, tap water and very pure water from the water-steam system of the power plant "Nikola Tesla B" in Obrenovac. Application of an amperometric detector (model LC-17A; BAS, West Lafayette, USA) enables the detection limit to be decreased down to 0.05 mu mol/dm(3) of chloride, which col responds to 35.5 pg, and adjustment of the acceptor flow rate and direction inside the gas-diffusion unit. In this way the optimized FIA system has excellent repeatability. For 5 mu mol/dm(3) it was found to be 1.11% (n = 5). The throughput of this method is 60 samples per hour., Selektivan i osetljiv postupak za brzo, indirektno određivanje hlorida gasno-difuzionom metodom otpimizovan je i primenjen za određivanje hlorida u uzorcima voda sa vrlo različitim sadržajem ove vrste: morskoj, vodi za piće i vrlo čistim vodama u sistemu voda-para TE "Nikola Tesna B" u Obrenovcu. Upotreba amperometrijskog detektora tipa LC-17A omogućava snižavanje granice detekcije na 0.05 μmol/dm3 hlorida (što za uzorak zapremine 0.2 cm3 iznosi 35.5 pg) i podešavanje brzine i smera toka u gasno-difuzionoj jedinici. Ovako optimizovan protočni sistem ima odličnu reproduktivnost. Za hloridni standard koncentracije 5 μmol/dm3 relativna standardna devijacija iznosi 1.11 % (n = 5).",
publisher = "Serbian Chemical Soc, Belgrade",
journal = "Journal of the Serbian Chemical Society",
title = "Optimization and application of the gas-diffusion flow injection method for the determination of chloride, Optimizacija i primena gasno-difuzione protočne injekcione metode za određivanje hlorida",
volume = "66",
number = "9",
pages = "637-646",
url = "https://hdl.handle.net/21.15107/rcub_cherry_473"
}
Lolić, A., Nikolić-Mandić, S. D.,& Polić, P. S.. (2001). Optimization and application of the gas-diffusion flow injection method for the determination of chloride. in Journal of the Serbian Chemical Society
Serbian Chemical Soc, Belgrade., 66(9), 637-646.
https://hdl.handle.net/21.15107/rcub_cherry_473
Lolić A, Nikolić-Mandić SD, Polić PS. Optimization and application of the gas-diffusion flow injection method for the determination of chloride. in Journal of the Serbian Chemical Society. 2001;66(9):637-646.
https://hdl.handle.net/21.15107/rcub_cherry_473 .
Lolić, Aleksandar, Nikolić-Mandić, Snežana D., Polić, Predrag S., "Optimization and application of the gas-diffusion flow injection method for the determination of chloride" in Journal of the Serbian Chemical Society, 66, no. 9 (2001):637-646,
https://hdl.handle.net/21.15107/rcub_cherry_473 .
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