Filipović, Vladimir

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orcid::0000-0002-7081-8217
  • Filipović, Vladimir (3)
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Author's Bibliography

Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses

Nićetin, Milica; Pezo, Lato; Pergal, Marija V.; Lončar, Biljana; Filipović, Vladimir; Knežević, Violeta; Demir, Hande; Filipović, Jelena; Manojlović, Dragan D.

(2022)

TY  - JOUR
AU  - Nićetin, Milica
AU  - Pezo, Lato
AU  - Pergal, Marija V.
AU  - Lončar, Biljana
AU  - Filipović, Vladimir
AU  - Knežević, Violeta
AU  - Demir, Hande
AU  - Filipović, Jelena
AU  - Manojlović, Dragan D.
PY  - 2022
UR  - https://www.mdpi.com/2304-8158/11/13/1945
UR  - http://cherry.chem.bg.ac.rs/handle/123456789/5502
AB  - The osmotic dehydration (OD) of celery root in sugar beet molasses was studied at three temperatures (20, 35, and 50 °C) and three immersion periods (1, 3, and 5 h) in order to examine the changes in antioxidant potential and phenolic profile of celery root throughout the process. The antioxidant capacity (AOC) of dehydrated samples was evaluated by spectrophotometric and polarographic assays, the total phenolic content by the Folin-Ciocalteu method, and the individual phenolic compounds by HPLC-DAD. As a result of OD in molasses, the AOC and phenols content in samples increased proportionally to the augmentation of temperature and the immersion time. Vanillic acid, syringic acid, and catechin were detected in dehydrated samples as a result of transfer from molasses. Compared to fresh celery root, the content of identified phenols in osmodehydrated samples was improved from 1.5 to 6.2 times. Strong correlations between applied assays were obtained, except for the DPPH. Based on the correlation analysis chlorogenic acid, gallic acid, chrysin, catechin, and kaempferol showed the greatest contribution to the overall AOC of osmodehydrated celery root. Molasses, an agro-industrial waste from sugar production, could be valorized as a valuable osmotic solution.
T2  - Foods
T1  - Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses
VL  - 11
IS  - 13
SP  - 1945
DO  - 10.3390/foods11131945
ER  - 
@article{
author = "Nićetin, Milica and Pezo, Lato and Pergal, Marija V. and Lončar, Biljana and Filipović, Vladimir and Knežević, Violeta and Demir, Hande and Filipović, Jelena and Manojlović, Dragan D.",
year = "2022",
abstract = "The osmotic dehydration (OD) of celery root in sugar beet molasses was studied at three temperatures (20, 35, and 50 °C) and three immersion periods (1, 3, and 5 h) in order to examine the changes in antioxidant potential and phenolic profile of celery root throughout the process. The antioxidant capacity (AOC) of dehydrated samples was evaluated by spectrophotometric and polarographic assays, the total phenolic content by the Folin-Ciocalteu method, and the individual phenolic compounds by HPLC-DAD. As a result of OD in molasses, the AOC and phenols content in samples increased proportionally to the augmentation of temperature and the immersion time. Vanillic acid, syringic acid, and catechin were detected in dehydrated samples as a result of transfer from molasses. Compared to fresh celery root, the content of identified phenols in osmodehydrated samples was improved from 1.5 to 6.2 times. Strong correlations between applied assays were obtained, except for the DPPH. Based on the correlation analysis chlorogenic acid, gallic acid, chrysin, catechin, and kaempferol showed the greatest contribution to the overall AOC of osmodehydrated celery root. Molasses, an agro-industrial waste from sugar production, could be valorized as a valuable osmotic solution.",
journal = "Foods",
title = "Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses",
volume = "11",
number = "13",
pages = "1945",
doi = "10.3390/foods11131945"
}
Nićetin, M., Pezo, L., Pergal, M. V., Lončar, B., Filipović, V., Knežević, V., Demir, H., Filipović, J.,& Manojlović, D. D.. (2022). Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses. in Foods, 11(13), 1945.
https://doi.org/10.3390/foods11131945
Nićetin M, Pezo L, Pergal MV, Lončar B, Filipović V, Knežević V, Demir H, Filipović J, Manojlović DD. Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses. in Foods. 2022;11(13):1945.
doi:10.3390/foods11131945 .
Nićetin, Milica, Pezo, Lato, Pergal, Marija V., Lončar, Biljana, Filipović, Vladimir, Knežević, Violeta, Demir, Hande, Filipović, Jelena, Manojlović, Dragan D., "Celery Root Phenols Content, Antioxidant Capacities and Their Correlations after Osmotic Dehydration in Molasses" in Foods, 11, no. 13 (2022):1945,
https://doi.org/10.3390/foods11131945 . .
5
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The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material

Aćimović, Milica G.; Tešević, Vele; Mara, Dimitrije; Cvetković, Mirjana; Stanković, Jovana; Filipović, Vladimir

(2016)

TY  - JOUR
AU  - Aćimović, Milica G.
AU  - Tešević, Vele
AU  - Mara, Dimitrije
AU  - Cvetković, Mirjana
AU  - Stanković, Jovana
AU  - Filipović, Vladimir
PY  - 2016
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/219
AB  - The essential oil content in cumin samples from Serbian market ranged between 2.0 and 4.0%, with 22 identified compounds, among which the most abundant were cumin aldehyde, β-pinene, γ-terpinene, γ-terpinene-7-al and p-cymene. Postdistillation cumin seeds waste material that remained after the essential oil extraction contains total polyphenols of between 30.1 and 47.5 mg GAE/g dry extract, as estimated by the Folin-Ciocalteu method. Hydroxybenzoic and hydroxycinnamic acids, as well as glycosides of flavonones and flavonoles, are the dominant polyphenols. However, according to DPPH method, the antioxidative potential of cumin postdistillation seeds waste was poor and it ranged between 0.02 and 0.04 mM TE/g. Further research will be focused on agro-food implementation of postdistillation waste material of cumin and other plants which are used for the essential oil production.
AB  - Sadržaj etarskog ulja u plodovima kumina prisutnog na Srpskom tržištu kreće se između 2.0 i 4.0%. Primenom GC/MS identifikovane je ukupno 22 komponente u etarskim uljima kumina, među kojima su najzastupljenije: kumin aldehid, β-pinen, γ-terpinen, γ-terpinen-7-al i p-cimen. Međutim, kako je sadržaj etarskog ulja u plodovima kumina mali (ispod 5%), veliki deo biljnog materijala ostaje neiskorišćen. Primenom tzv. Folin-Ciocalteu metoda, ustanovljeno je da ostaci nakon destilacije etarskog ulja iz plodova kumina sadrže između 30.1 i 47.5 mg GAE/g suvog ekstrakta ukupnih polifenola. Hidroksibenzoeva i hidroksicimetna kiselina, kao i glikozidi flavonona i flavonola, su najzastupljeniji polifenoli. Na osnovu DPPH-metoda antioksidativni potencijal ostataka nakon destilacije plodova kumina je slab i kreće se između 0.02 i 0.04 mM TE/g. Dalja istraživanja bi trebalo usmeriti ka primeni ostataka nakon destilacije plodova kumina i drugih biljaka koje se koriste za destilaciju etarskih ulja u prehrambenoj industriji i poljoprivredi.
T2  - Advanced Technologies
T1  - The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material
T1  - Analiza etarskog ulja plodova kumina i ukupnih polifenola u ostacima nakon destilacije
VL  - 5
IS  - 1
SP  - 23
EP  - 30
DO  - 10.5937/savteh1601023A
ER  - 
@article{
author = "Aćimović, Milica G. and Tešević, Vele and Mara, Dimitrije and Cvetković, Mirjana and Stanković, Jovana and Filipović, Vladimir",
year = "2016",
abstract = "The essential oil content in cumin samples from Serbian market ranged between 2.0 and 4.0%, with 22 identified compounds, among which the most abundant were cumin aldehyde, β-pinene, γ-terpinene, γ-terpinene-7-al and p-cymene. Postdistillation cumin seeds waste material that remained after the essential oil extraction contains total polyphenols of between 30.1 and 47.5 mg GAE/g dry extract, as estimated by the Folin-Ciocalteu method. Hydroxybenzoic and hydroxycinnamic acids, as well as glycosides of flavonones and flavonoles, are the dominant polyphenols. However, according to DPPH method, the antioxidative potential of cumin postdistillation seeds waste was poor and it ranged between 0.02 and 0.04 mM TE/g. Further research will be focused on agro-food implementation of postdistillation waste material of cumin and other plants which are used for the essential oil production., Sadržaj etarskog ulja u plodovima kumina prisutnog na Srpskom tržištu kreće se između 2.0 i 4.0%. Primenom GC/MS identifikovane je ukupno 22 komponente u etarskim uljima kumina, među kojima su najzastupljenije: kumin aldehid, β-pinen, γ-terpinen, γ-terpinen-7-al i p-cimen. Međutim, kako je sadržaj etarskog ulja u plodovima kumina mali (ispod 5%), veliki deo biljnog materijala ostaje neiskorišćen. Primenom tzv. Folin-Ciocalteu metoda, ustanovljeno je da ostaci nakon destilacije etarskog ulja iz plodova kumina sadrže između 30.1 i 47.5 mg GAE/g suvog ekstrakta ukupnih polifenola. Hidroksibenzoeva i hidroksicimetna kiselina, kao i glikozidi flavonona i flavonola, su najzastupljeniji polifenoli. Na osnovu DPPH-metoda antioksidativni potencijal ostataka nakon destilacije plodova kumina je slab i kreće se između 0.02 i 0.04 mM TE/g. Dalja istraživanja bi trebalo usmeriti ka primeni ostataka nakon destilacije plodova kumina i drugih biljaka koje se koriste za destilaciju etarskih ulja u prehrambenoj industriji i poljoprivredi.",
journal = "Advanced Technologies",
title = "The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material, Analiza etarskog ulja plodova kumina i ukupnih polifenola u ostacima nakon destilacije",
volume = "5",
number = "1",
pages = "23-30",
doi = "10.5937/savteh1601023A"
}
Aćimović, M. G., Tešević, V., Mara, D., Cvetković, M., Stanković, J.,& Filipović, V.. (2016). The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material. in Advanced Technologies, 5(1), 23-30.
https://doi.org/10.5937/savteh1601023A
Aćimović MG, Tešević V, Mara D, Cvetković M, Stanković J, Filipović V. The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material. in Advanced Technologies. 2016;5(1):23-30.
doi:10.5937/savteh1601023A .
Aćimović, Milica G., Tešević, Vele, Mara, Dimitrije, Cvetković, Mirjana, Stanković, Jovana, Filipović, Vladimir, "The analysis of cumin seeds essential oil and total polyphenols from postdestillation waste material" in Advanced Technologies, 5, no. 1 (2016):23-30,
https://doi.org/10.5937/savteh1601023A . .
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6

Calculation of cost price for production of anise fruit and anise essential oil by application of fertilizers used in organic and conventional growing systems

Aćimović, Milica G.; Oljača, Snežana; Kovačević, Dušan; Filipović, Vladimir; Tasić, Slavoljub; Tešević, Vele

(2013)

TY  - JOUR
AU  - Aćimović, Milica G.
AU  - Oljača, Snežana
AU  - Kovačević, Dušan
AU  - Filipović, Vladimir
AU  - Tasić, Slavoljub
AU  - Tešević, Vele
PY  - 2013
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/92
AB  - Anise is an annual plant from family Apiaceae, originating from Egypt, Greece, Crete and Asia Minor, that has been cultivated since ancient times. During the Middle Ages its cultivation spread throughout Europe, all the way to Great Britain. However, in the northern parts of Europe, due to insufficient hours of sunshine and sum of effective temperature, this plant cannot bear fruit. In Serbia, the years 2011/12 recorded optimal conditions for growth and development of this plant, which resulted in an average high fruit yield (average 1551 kg/ha) and contents of essential oil (3.72 %). The experiments conducted on three locations in Vojvodina Province (Mošorin, Veliki Radinci and Ostojićevo) tested the growth of anise with implementation of four types of fertilizers approved for organic production system (Slavol, Bactofil B-10, Royal Ofert biohumus and vermicompost), as well as the growth of anise with implementation of fertilizers used in conventional agriculture (NPK in formulation 15:15:15). Plots where no fertilizer was applied were used for control purposes. Cost price calculations for cultivation of anise, with commercial price of 2.5 €/kg for anise fruit (Anisi fructus), show that the highest income from anise fruit (Anisi fructus) is achieved by implementation of either a synthetic NPK fertilizer, or biofertilizers Bactofil B- 10 and Slavol. However, having in mind that organically produced plants achieve around 20% higher price, the application of bio fertilizers is fully cost-effective for this type of production. As for the anise essential oil (Anisi aethroleum), it is rarely obtained by distillation of anise fruits (Pimpinella anisum), but through a semisynthetic procedure using star anise (Illicum verum), wood originating from Indochina whose fruits are also rich in anethole. Since the demand for organic products is increasing, especially in the food industry, essential oil from an organically produced anise could have great income potential, in which case the application of bio fertilizers is the most profitable form of production.
AB  - U ogledima izvedenim na tri lokacije u Vojvodini (Mošorin, Veliki Radinci i Ostojićevo) ispitivano je gajenje anisa pri primeni četiri vrste đubriva dozvoljenih pri proizvodnji u sistemu organske poljoprivrede (Slavol, Bactofil B-10, Royal Ofert biohumusa i glistenjaka), ali i đubrivu koje se primenjuje u konvencionalnom sistemu proizvodnje (NPK đubrivo u formulaciji 15:15:15). Kao kontrolna varijanta korišćene su parcele bez primene đubriva. Tokom dve godine (2011/12) anis je imao optimalne uslove za rast i razvoj, što je rezultiralo prosečno visokim prinosom ploda (prosečno 1551 kg/ha) i sadržajem etarskog ulja u plodovima (3,72%). Kalkulacijom proizvodnje anisa može se zaključiti da se najveći prihod od ploda anisa (Anisi fructus) pri komercijalnoj otkupnoj ceni od 270 din/kg ostvaruje pri primeni mineralno sintetičkog NPK đubriva, a od organskih pri primeni biofertilizatora Bactofil B-10 i Slavola. Međutim, ako imamo u vidu da organski proizvedene biljke postižu oko 20% veću cenu, primena biofertilizatora je u potpunosti isplativa za ovaj vid proizvodnje. Organski proizvedeno etarsko ulje anisa (Anisi aethroleum) takođe bi moglo imati veliki potencijal za prihod, pri čemu kao najisplativija takođe figurira primena biofertilizatora.
T2  - Lekovite sirovine
T1  - Calculation of cost price for production of anise fruit and anise essential oil by application of fertilizers used in organic and conventional growing systems
T1  - Kalkulacija proizvodnje ploda i etarskog ulja anisa u sistemu organske i konvencionalne poljoprivrede
IS  - 33
SP  - 73
EP  - 81
UR  - https://hdl.handle.net/21.15107/rcub_cherry_92
ER  - 
@article{
author = "Aćimović, Milica G. and Oljača, Snežana and Kovačević, Dušan and Filipović, Vladimir and Tasić, Slavoljub and Tešević, Vele",
year = "2013",
abstract = "Anise is an annual plant from family Apiaceae, originating from Egypt, Greece, Crete and Asia Minor, that has been cultivated since ancient times. During the Middle Ages its cultivation spread throughout Europe, all the way to Great Britain. However, in the northern parts of Europe, due to insufficient hours of sunshine and sum of effective temperature, this plant cannot bear fruit. In Serbia, the years 2011/12 recorded optimal conditions for growth and development of this plant, which resulted in an average high fruit yield (average 1551 kg/ha) and contents of essential oil (3.72 %). The experiments conducted on three locations in Vojvodina Province (Mošorin, Veliki Radinci and Ostojićevo) tested the growth of anise with implementation of four types of fertilizers approved for organic production system (Slavol, Bactofil B-10, Royal Ofert biohumus and vermicompost), as well as the growth of anise with implementation of fertilizers used in conventional agriculture (NPK in formulation 15:15:15). Plots where no fertilizer was applied were used for control purposes. Cost price calculations for cultivation of anise, with commercial price of 2.5 €/kg for anise fruit (Anisi fructus), show that the highest income from anise fruit (Anisi fructus) is achieved by implementation of either a synthetic NPK fertilizer, or biofertilizers Bactofil B- 10 and Slavol. However, having in mind that organically produced plants achieve around 20% higher price, the application of bio fertilizers is fully cost-effective for this type of production. As for the anise essential oil (Anisi aethroleum), it is rarely obtained by distillation of anise fruits (Pimpinella anisum), but through a semisynthetic procedure using star anise (Illicum verum), wood originating from Indochina whose fruits are also rich in anethole. Since the demand for organic products is increasing, especially in the food industry, essential oil from an organically produced anise could have great income potential, in which case the application of bio fertilizers is the most profitable form of production., U ogledima izvedenim na tri lokacije u Vojvodini (Mošorin, Veliki Radinci i Ostojićevo) ispitivano je gajenje anisa pri primeni četiri vrste đubriva dozvoljenih pri proizvodnji u sistemu organske poljoprivrede (Slavol, Bactofil B-10, Royal Ofert biohumusa i glistenjaka), ali i đubrivu koje se primenjuje u konvencionalnom sistemu proizvodnje (NPK đubrivo u formulaciji 15:15:15). Kao kontrolna varijanta korišćene su parcele bez primene đubriva. Tokom dve godine (2011/12) anis je imao optimalne uslove za rast i razvoj, što je rezultiralo prosečno visokim prinosom ploda (prosečno 1551 kg/ha) i sadržajem etarskog ulja u plodovima (3,72%). Kalkulacijom proizvodnje anisa može se zaključiti da se najveći prihod od ploda anisa (Anisi fructus) pri komercijalnoj otkupnoj ceni od 270 din/kg ostvaruje pri primeni mineralno sintetičkog NPK đubriva, a od organskih pri primeni biofertilizatora Bactofil B-10 i Slavola. Međutim, ako imamo u vidu da organski proizvedene biljke postižu oko 20% veću cenu, primena biofertilizatora je u potpunosti isplativa za ovaj vid proizvodnje. Organski proizvedeno etarsko ulje anisa (Anisi aethroleum) takođe bi moglo imati veliki potencijal za prihod, pri čemu kao najisplativija takođe figurira primena biofertilizatora.",
journal = "Lekovite sirovine",
title = "Calculation of cost price for production of anise fruit and anise essential oil by application of fertilizers used in organic and conventional growing systems, Kalkulacija proizvodnje ploda i etarskog ulja anisa u sistemu organske i konvencionalne poljoprivrede",
number = "33",
pages = "73-81",
url = "https://hdl.handle.net/21.15107/rcub_cherry_92"
}
Aćimović, M. G., Oljača, S., Kovačević, D., Filipović, V., Tasić, S.,& Tešević, V.. (2013). Calculation of cost price for production of anise fruit and anise essential oil by application of fertilizers used in organic and conventional growing systems. in Lekovite sirovine(33), 73-81.
https://hdl.handle.net/21.15107/rcub_cherry_92
Aćimović MG, Oljača S, Kovačević D, Filipović V, Tasić S, Tešević V. Calculation of cost price for production of anise fruit and anise essential oil by application of fertilizers used in organic and conventional growing systems. in Lekovite sirovine. 2013;(33):73-81.
https://hdl.handle.net/21.15107/rcub_cherry_92 .
Aćimović, Milica G., Oljača, Snežana, Kovačević, Dušan, Filipović, Vladimir, Tasić, Slavoljub, Tešević, Vele, "Calculation of cost price for production of anise fruit and anise essential oil by application of fertilizers used in organic and conventional growing systems" in Lekovite sirovine, no. 33 (2013):73-81,
https://hdl.handle.net/21.15107/rcub_cherry_92 .