TY  - JOUR
AU  - Tripković, Tatjana
AU  - Vasić, Ružica
AU  - Lolić, Aleksandar
AU  - Baošić, Rada
PY  - 2022
UR  - http://cherry.chem.bg.ac.rs/handle/123456789/4948
AB  - Graphite furnace atomic absorption spectroscopy (GFAAS) was applied to identification of historical pigments. The method is adapted to determine different metals, usually found in pigments. Operating conditions were optimized, such as sample drying step, pyrolysis and atomization temperatures, modifiers, and volume of sample introduced into the atomizer, to reduce interferences due to a complex sample matrix. Using the optimized method pigments in samples from the painting Coronation of the Virgin from the Church of the Shroud of the Holy Virgin in Barič were identified. The samples were analyzed also by Raman microscopy to verify the identification achieved by GFAAS. Raman microscopy confirmed the assumptionsmade based on GFAAS results. Using the two techniques a variety of pigments have been identified, such as calcite, leadwhite, goethite, hematite, ultramarine, vermilion, minium, carbon black. Based on GFAAS results the presence of azuritewas observed in the blue paint sample, although this finding was not confirmed by Raman microscopy.
PB  - Springer
T2  - Chemical Papers
T1  - Determination of metals in artistic pigments using the optimized GFAAS method and Raman spectroscopy
VL  - 76
SP  - 3607
EP  - 3618
DO  - 10.1007/s11696-022-02110-6
ER  - 

@article{
author = "Tripković, Tatjana and Vasić, Ružica and Lolić, Aleksandar and Baošić, Rada",
year = "2022",
abstract = "Graphite furnace atomic absorption spectroscopy (GFAAS) was applied to identification of historical pigments. The method is adapted to determine different metals, usually found in pigments. Operating conditions were optimized, such as sample drying step, pyrolysis and atomization temperatures, modifiers, and volume of sample introduced into the atomizer, to reduce interferences due to a complex sample matrix. Using the optimized method pigments in samples from the painting Coronation of the Virgin from the Church of the Shroud of the Holy Virgin in Barič were identified. The samples were analyzed also by Raman microscopy to verify the identification achieved by GFAAS. Raman microscopy confirmed the assumptionsmade based on GFAAS results. Using the two techniques a variety of pigments have been identified, such as calcite, leadwhite, goethite, hematite, ultramarine, vermilion, minium, carbon black. Based on GFAAS results the presence of azuritewas observed in the blue paint sample, although this finding was not confirmed by Raman microscopy.",
publisher = "Springer",
journal = "Chemical Papers",
title = "Determination of metals in artistic pigments using the optimized GFAAS method and Raman spectroscopy",
volume = "76",
pages = "3607-3618",
doi = "10.1007/s11696-022-02110-6"
}

Tripković, T., Vasić, R., Lolić, A.,& Baošić, R.. (2022). Determination of metals in artistic pigments using the optimized GFAAS method and Raman spectroscopy. in Chemical Papers
Springer., 76, 3607-3618.
https://doi.org/10.1007/s11696-022-02110-6

Tripković T, Vasić R, Lolić A, Baošić R. Determination of metals in artistic pigments using the optimized GFAAS method and Raman spectroscopy. in Chemical Papers. 2022;76:3607-3618.
doi:10.1007/s11696-022-02110-6 .

Tripković, Tatjana, Vasić, Ružica, Lolić, Aleksandar, Baošić, Rada, "Determination of metals in artistic pigments using the optimized GFAAS method and Raman spectroscopy" in Chemical Papers, 76 (2022):3607-3618,
https://doi.org/10.1007/s11696-022-02110-6 . .

TY  - DATA
AU  - Tripković, Tatjana
AU  - Vasić, Ružica
AU  - Lolić, Aleksandar
AU  - Baošić, Rada
PY  - 2022
UR  - http://cherry.chem.bg.ac.rs/handle/123456789/4949
PB  - Springer
T2  - Chemical Papers
T1  - Supplementary data for the article: Tripković, T.; Vasić, R.; Lolić, A.; Baošić, R. Determination of Metals in Artistic Pigments Using the Optimized GFAAS Method and Raman Spectroscopy. Chemical Papers 2022, n/a. https://doi.org/10.1007/s11696-022-02110-6.
VL  - 76
UR  - https://hdl.handle.net/21.15107/rcub_cherry_4949
ER  - 

@misc{
author = "Tripković, Tatjana and Vasić, Ružica and Lolić, Aleksandar and Baošić, Rada",
year = "2022",
publisher = "Springer",
journal = "Chemical Papers",
title = "Supplementary data for the article: Tripković, T.; Vasić, R.; Lolić, A.; Baošić, R. Determination of Metals in Artistic Pigments Using the Optimized GFAAS Method and Raman Spectroscopy. Chemical Papers 2022, n/a. https://doi.org/10.1007/s11696-022-02110-6.",
volume = "76",
url = "https://hdl.handle.net/21.15107/rcub_cherry_4949"
}

Tripković, T., Vasić, R., Lolić, A.,& Baošić, R.. (2022). Supplementary data for the article: Tripković, T.; Vasić, R.; Lolić, A.; Baošić, R. Determination of Metals in Artistic Pigments Using the Optimized GFAAS Method and Raman Spectroscopy. Chemical Papers 2022, n/a. https://doi.org/10.1007/s11696-022-02110-6.. in Chemical Papers
Springer., 76.
https://hdl.handle.net/21.15107/rcub_cherry_4949

Tripković T, Vasić R, Lolić A, Baošić R. Supplementary data for the article: Tripković, T.; Vasić, R.; Lolić, A.; Baošić, R. Determination of Metals in Artistic Pigments Using the Optimized GFAAS Method and Raman Spectroscopy. Chemical Papers 2022, n/a. https://doi.org/10.1007/s11696-022-02110-6.. in Chemical Papers. 2022;76.
https://hdl.handle.net/21.15107/rcub_cherry_4949 .

Tripković, Tatjana, Vasić, Ružica, Lolić, Aleksandar, Baošić, Rada, "Supplementary data for the article: Tripković, T.; Vasić, R.; Lolić, A.; Baošić, R. Determination of Metals in Artistic Pigments Using the Optimized GFAAS Method and Raman Spectroscopy. Chemical Papers 2022, n/a. https://doi.org/10.1007/s11696-022-02110-6." in Chemical Papers, 76 (2022),
https://hdl.handle.net/21.15107/rcub_cherry_4949 .