TY  - JOUR
AU  - Anđelković, Katarina K.
AU  - Jakovljević, G
AU  - Zlatović, Mario
AU  - Tešić, Živoslav Lj.
AU  - Sladić, Dušan
AU  - Howing, J
AU  - Tellgren, R
PY  - 2004
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/666
AB  - Complexes of Zn(II), Pd(II) and Pt(II) with 2'-[1-(2- pyridinyl)ethyhdene]oxamohydrazide (Hapsox) were synthesized and their structures were determined. All the complexes are of a neutral type with two apsox ligands coordinated to Zn(II) and one apsox ligand coordinated to Pd(II) or Pt(II). In each case. the polydentate was coordinated via pyridine and hydrazone nitrogens and alpha-oxyazine oxygen. forming an octahedral geometry around Zn(II). and a square planar one around Pd(II) and Pt(II). The structure determination was performed by IR. H-1-NMR and C-13-NMR spectroscopy, and for the Zn(II) complex by X-ray structure analysis.
AB  - U ovom radu opisana je sinteza i strukturna karakterizacija kompleksa Zn(II) Pd(II) i Pt(II) sa 2’-[1-(2-piridinil)etiliden]oksamohidrazidom (Hapsox). Sva tri dobijena kompleksa su neutralnog tipa sa dva koordinovana apsox liganda u slučaju kompleksa Zn(II), odnosno jednim apsox ligandom u slučaju Pd(II) i Pt(II) kompleksa. Koordinacija polidentata je u svim kompleksima ostvarena preko piridinskog azota, hidrazonskog azota i α-oksiazinskog kiseonika gradeći oktaedarsku geometriju oko Zn(II), odnosno kvadratno planarnu geometriju oko Pd(II) i Pt(II).Potvrdu za ovakve strukture dobili smo iz IC 1H-NMR i 13C-NMR spektara, dok je za Zn(II) kompleks urađena i rendgenska strukturna analiza.
PB  - Serbian Chemical Soc, Belgrade
T2  - Journal of the Serbian Chemical Society
T1  - Synthesis and characterization of zinc(II), palladium(II) and platinum(II) complex with 2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazide. The crystal structure of bis {2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazido} zinc(II) trihydrate
T1  - Sinteza I karakterizacija kompleksa cinka(II), paladijuma(II) I platine(II) sa 2’-[1-(2-piridinil)etiliden]oksamohidrazidom - kristalna struktura bis {2’-[1-(2-piridinil)etiliden]oksamohidrazido}cink(II) trihidrata
VL  - 69
IS  - 8-9
SP  - 651
EP  - 660
DO  - 10.2298/JSC0409651A
ER  - 

@article{
author = "Anđelković, Katarina K. and Jakovljević, G and Zlatović, Mario and Tešić, Živoslav Lj. and Sladić, Dušan and Howing, J and Tellgren, R",
year = "2004",
abstract = "Complexes of Zn(II), Pd(II) and Pt(II) with 2'-[1-(2- pyridinyl)ethyhdene]oxamohydrazide (Hapsox) were synthesized and their structures were determined. All the complexes are of a neutral type with two apsox ligands coordinated to Zn(II) and one apsox ligand coordinated to Pd(II) or Pt(II). In each case. the polydentate was coordinated via pyridine and hydrazone nitrogens and alpha-oxyazine oxygen. forming an octahedral geometry around Zn(II). and a square planar one around Pd(II) and Pt(II). The structure determination was performed by IR. H-1-NMR and C-13-NMR spectroscopy, and for the Zn(II) complex by X-ray structure analysis., U ovom radu opisana je sinteza i strukturna karakterizacija kompleksa Zn(II) Pd(II) i Pt(II) sa 2’-[1-(2-piridinil)etiliden]oksamohidrazidom (Hapsox). Sva tri dobijena kompleksa su neutralnog tipa sa dva koordinovana apsox liganda u slučaju kompleksa Zn(II), odnosno jednim apsox ligandom u slučaju Pd(II) i Pt(II) kompleksa. Koordinacija polidentata je u svim kompleksima ostvarena preko piridinskog azota, hidrazonskog azota i α-oksiazinskog kiseonika gradeći oktaedarsku geometriju oko Zn(II), odnosno kvadratno planarnu geometriju oko Pd(II) i Pt(II).Potvrdu za ovakve strukture dobili smo iz IC 1H-NMR i 13C-NMR spektara, dok je za Zn(II) kompleks urađena i rendgenska strukturna analiza.",
publisher = "Serbian Chemical Soc, Belgrade",
journal = "Journal of the Serbian Chemical Society",
title = "Synthesis and characterization of zinc(II), palladium(II) and platinum(II) complex with 2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazide. The crystal structure of bis {2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazido} zinc(II) trihydrate, Sinteza I karakterizacija kompleksa cinka(II), paladijuma(II) I platine(II) sa 2’-[1-(2-piridinil)etiliden]oksamohidrazidom - kristalna struktura bis {2’-[1-(2-piridinil)etiliden]oksamohidrazido}cink(II) trihidrata",
volume = "69",
number = "8-9",
pages = "651-660",
doi = "10.2298/JSC0409651A"
}

Anđelković, K. K., Jakovljević, G., Zlatović, M., Tešić, Ž. Lj., Sladić, D., Howing, J.,& Tellgren, R.. (2004). Synthesis and characterization of zinc(II), palladium(II) and platinum(II) complex with 2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazide. The crystal structure of bis {2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazido} zinc(II) trihydrate. in Journal of the Serbian Chemical Society
Serbian Chemical Soc, Belgrade., 69(8-9), 651-660.
https://doi.org/10.2298/JSC0409651A

Anđelković KK, Jakovljević G, Zlatović M, Tešić ŽL, Sladić D, Howing J, Tellgren R. Synthesis and characterization of zinc(II), palladium(II) and platinum(II) complex with 2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazide. The crystal structure of bis {2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazido} zinc(II) trihydrate. in Journal of the Serbian Chemical Society. 2004;69(8-9):651-660.
doi:10.2298/JSC0409651A .

Anđelković, Katarina K., Jakovljević, G, Zlatović, Mario, Tešić, Živoslav Lj., Sladić, Dušan, Howing, J, Tellgren, R, "Synthesis and characterization of zinc(II), palladium(II) and platinum(II) complex with 2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazide. The crystal structure of bis {2 '-[1-(2-pyridinyl)ethylidene]oxamohydrazido} zinc(II) trihydrate" in Journal of the Serbian Chemical Society, 69, no. 8-9 (2004):651-660,
https://doi.org/10.2298/JSC0409651A . .

TY  - JOUR
AU  - Anđelković, Katarina K.
AU  - Howing, J
AU  - Tellgren, R
AU  - Jeremić, Dejan
AU  - Ivanović-Burmazović, Ivana
AU  - Sladić, Dušan
PY  - 2003
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/145
AB  - The synthesis of a novel ligand 2'-[1-(2-pyridinyl)-ethylidene]-oxamohydrazide (Hapsox), from a series of 2-acetylpyridine acylhydrazones, and its complex with Co(III), which is the first in this series of complexes are described. Both the ligand and the complex were characterized by elemental analysis, IR, H-1-NMR, and C-13-NMR spectra, and the structure of the complex [Co(apsox)(2)]ClO4 was determined by X-ray structural analysis. It was established that [Co(apsox)(2)]ClO4 has an octahedral geometry with two tridentate apsox ligands in monoanionic form. Structural characteristics, lengths of the bonds, and angles between the bonds were typical for Co(III) complexes of distorted octahedral geometry. Both direct and template synthesis afforded the same geometrical isomer of the complex with two apsox ligands meridionally bound to the central metal ion, even in the case when equimolar quantities of Co(ClO4)(2) and Hapsox were applied.
PB  - Taylor & Francis Ltd, Abingdon
T2  - Journal of Coordination Chemistry
T1  - Synthesis and structural characterization of the Co(III) complex with 2 '-[1-(2-pyridinyl)-ethylidene]oxamohydrazide (Hapsox): The crystal structure of bis-{2 '-[1-(2-pyridinyl)-ethylidene]-oxamohydrazido} cobalt(III) perchlorate, [Co(apsox)(2)]ClO4
VL  - 56
IS  - 7
SP  - 611
EP  - 622
DO  - 10.1080/0095897031000113986
ER  - 

@article{
author = "Anđelković, Katarina K. and Howing, J and Tellgren, R and Jeremić, Dejan and Ivanović-Burmazović, Ivana and Sladić, Dušan",
year = "2003",
abstract = "The synthesis of a novel ligand 2'-[1-(2-pyridinyl)-ethylidene]-oxamohydrazide (Hapsox), from a series of 2-acetylpyridine acylhydrazones, and its complex with Co(III), which is the first in this series of complexes are described. Both the ligand and the complex were characterized by elemental analysis, IR, H-1-NMR, and C-13-NMR spectra, and the structure of the complex [Co(apsox)(2)]ClO4 was determined by X-ray structural analysis. It was established that [Co(apsox)(2)]ClO4 has an octahedral geometry with two tridentate apsox ligands in monoanionic form. Structural characteristics, lengths of the bonds, and angles between the bonds were typical for Co(III) complexes of distorted octahedral geometry. Both direct and template synthesis afforded the same geometrical isomer of the complex with two apsox ligands meridionally bound to the central metal ion, even in the case when equimolar quantities of Co(ClO4)(2) and Hapsox were applied.",
publisher = "Taylor & Francis Ltd, Abingdon",
journal = "Journal of Coordination Chemistry",
title = "Synthesis and structural characterization of the Co(III) complex with 2 '-[1-(2-pyridinyl)-ethylidene]oxamohydrazide (Hapsox): The crystal structure of bis-{2 '-[1-(2-pyridinyl)-ethylidene]-oxamohydrazido} cobalt(III) perchlorate, [Co(apsox)(2)]ClO4",
volume = "56",
number = "7",
pages = "611-622",
doi = "10.1080/0095897031000113986"
}

Anđelković, K. K., Howing, J., Tellgren, R., Jeremić, D., Ivanović-Burmazović, I.,& Sladić, D.. (2003). Synthesis and structural characterization of the Co(III) complex with 2 '-[1-(2-pyridinyl)-ethylidene]oxamohydrazide (Hapsox): The crystal structure of bis-{2 '-[1-(2-pyridinyl)-ethylidene]-oxamohydrazido} cobalt(III) perchlorate, [Co(apsox)(2)]ClO4. in Journal of Coordination Chemistry
Taylor & Francis Ltd, Abingdon., 56(7), 611-622.
https://doi.org/10.1080/0095897031000113986

Anđelković KK, Howing J, Tellgren R, Jeremić D, Ivanović-Burmazović I, Sladić D. Synthesis and structural characterization of the Co(III) complex with 2 '-[1-(2-pyridinyl)-ethylidene]oxamohydrazide (Hapsox): The crystal structure of bis-{2 '-[1-(2-pyridinyl)-ethylidene]-oxamohydrazido} cobalt(III) perchlorate, [Co(apsox)(2)]ClO4. in Journal of Coordination Chemistry. 2003;56(7):611-622.
doi:10.1080/0095897031000113986 .

Anđelković, Katarina K., Howing, J, Tellgren, R, Jeremić, Dejan, Ivanović-Burmazović, Ivana, Sladić, Dušan, "Synthesis and structural characterization of the Co(III) complex with 2 '-[1-(2-pyridinyl)-ethylidene]oxamohydrazide (Hapsox): The crystal structure of bis-{2 '-[1-(2-pyridinyl)-ethylidene]-oxamohydrazido} cobalt(III) perchlorate, [Co(apsox)(2)]ClO4" in Journal of Coordination Chemistry, 56, no. 7 (2003):611-622,
https://doi.org/10.1080/0095897031000113986 . .

TY  - JOUR
AU  - Anđelković, Katarina K.
AU  - Tellgren, R
AU  - Niketic, SR
AU  - Sladić, Dušan
AU  - Poleti, D
PY  - 1999
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/425
AB  - The title compound was obtained by a template synthesis from 2,6-diacetylpyridine, ethylhydrazinoacetate and CuCl2 . 2H(2)O (molar ratio 1 : 2 : 1, in methanol), and its structure has been determined by single-crystal X-ray diffraction: monoclinic space group P2(1)/c, a = 13.906(5), b = 18.199(6), c = 16.641(6) Angstrom, beta = 107.18(3)degrees and z = 4. The ligand was found to be tridentate in a trigonal-bipyramidal coordination geometry with two chloride ligands. There are two independent complex molecules, one of which is hydrogen bonded to the water of crystallization.
PB  - Kluwer Academic/Plenum Publ, New York
T2  - Journal of Chemical Crystallography
T1  - Crystal and molecular structure of five coordinate copper(II) complex with 2,6-bis[1-(methoxycarbonylmethyl-hydrazono)ethyl] pyridine
VL  - 29
IS  - 5
SP  - 575
EP  - 580
DO  - 10.1023/A:1009500919942
ER  - 

@article{
author = "Anđelković, Katarina K. and Tellgren, R and Niketic, SR and Sladić, Dušan and Poleti, D",
year = "1999",
abstract = "The title compound was obtained by a template synthesis from 2,6-diacetylpyridine, ethylhydrazinoacetate and CuCl2 . 2H(2)O (molar ratio 1 : 2 : 1, in methanol), and its structure has been determined by single-crystal X-ray diffraction: monoclinic space group P2(1)/c, a = 13.906(5), b = 18.199(6), c = 16.641(6) Angstrom, beta = 107.18(3)degrees and z = 4. The ligand was found to be tridentate in a trigonal-bipyramidal coordination geometry with two chloride ligands. There are two independent complex molecules, one of which is hydrogen bonded to the water of crystallization.",
publisher = "Kluwer Academic/Plenum Publ, New York",
journal = "Journal of Chemical Crystallography",
title = "Crystal and molecular structure of five coordinate copper(II) complex with 2,6-bis[1-(methoxycarbonylmethyl-hydrazono)ethyl] pyridine",
volume = "29",
number = "5",
pages = "575-580",
doi = "10.1023/A:1009500919942"
}

Anđelković, K. K., Tellgren, R., Niketic, S., Sladić, D.,& Poleti, D.. (1999). Crystal and molecular structure of five coordinate copper(II) complex with 2,6-bis[1-(methoxycarbonylmethyl-hydrazono)ethyl] pyridine. in Journal of Chemical Crystallography
Kluwer Academic/Plenum Publ, New York., 29(5), 575-580.
https://doi.org/10.1023/A:1009500919942

Anđelković KK, Tellgren R, Niketic S, Sladić D, Poleti D. Crystal and molecular structure of five coordinate copper(II) complex with 2,6-bis[1-(methoxycarbonylmethyl-hydrazono)ethyl] pyridine. in Journal of Chemical Crystallography. 1999;29(5):575-580.
doi:10.1023/A:1009500919942 .

Anđelković, Katarina K., Tellgren, R, Niketic, SR, Sladić, Dušan, Poleti, D, "Crystal and molecular structure of five coordinate copper(II) complex with 2,6-bis[1-(methoxycarbonylmethyl-hydrazono)ethyl] pyridine" in Journal of Chemical Crystallography, 29, no. 5 (1999):575-580,
https://doi.org/10.1023/A:1009500919942 . .