@article{
author = "Gajić, Nataša and Kamberović, Željko and Anđić, Zoran and Korać, Marija and Trpčevska, Jarmila and Stamatović, Mirko",
year = "2019",
abstract = "The aim of this research was to study the effect of graphite addition in the
process of synthesis of tribological materials based on tin sulphides. The tin sulphides
powders were synthesized from selected precursors by pyrometallurgical
method in rotary tilting tube furnace. The thermodynamic parameters of the synthesis
were determined using HSC Chemistry software modelling package. In
addition, the synthesis process was also characterized by the thermal analysis
method: simultaneous differential scanning calorimetry and thermogravimetry
(DCS-TGA). The characterization of the synthesized tin sulphides powders included
analysis of chemical composition by optical emission spectroscopy, phase
composition identification by X-ray diffraction (XRD) and examination of morphology,
as well as elemental composition by scanning electron microscopy (SEM)
with energy-dispersive spectroscopy (EDS). The hexagonal SnS2 and orthorhombic
Sn2S3 phases were formed after the thermal treatment of starting powders in nitrogen
atmosphere. The obtained results indicate the positive effects of the graphite
addition which enables the synthesis of tin sulphide powders with appropriate
content of sulphide phases with minimal loss of sulphur.",
publisher = "Belgrade : Serbian Chemical Society",
journal = "Journal of the Serbian Chemical Society",
title = "Improving the synthesis process of tribological materials based on tin sulphides by adding graphite as additive",
volume = "84",
number = "4",
pages = "423-433",
doi = "10.2298/JSC180628102G"
}