Composition of Essential Oil Obtained From Tubular, Head and Ligulate Flowers of Calendula officinalis L. by Steam Distillation of Plant Material and CO2 Extracts
Abstract
Essential oil content of tubular, head and ligulate flowers of Calendula officinalis L. were determined using official steam distillation procedure. It was found that the ligulate flower sample had the highest oil content (0.16%). Applying SFE by means of CO2 (200 bar, 40 degrees C, 3 h extraction time), the highest extraction yield was found in tubular and ligulate flower samples (3.67% and 3.64%). Head flower had a lower extraction yield (2.60%) as the result of relatively small content of fatty oil, waxes and resins present in plant material. Steam distillation procedure was applied to obtain essential oils from the CO2 extracts devoid from cuticular waxes and resins. The compositions of oils were determined by GC and GC/MS. The main compounds of all investigated oils were alpha-cadinol (11.7-29.1%), delta-cadinene (3.2-20.3%), gamma-cadinene (1.5-11.4%) and cadina-3,9-diene (0.4-11.2%). The oil samples obtained from the CO2 extracts were found to be more complex containing alpha-gu...rjunene, beta-caryophyllene, beta-gurjunene, cis-muurola-4(14)-5-diene and alpha-humulene.
Keywords:
Calendula officinalis L. / Astraceae / Marigold / essential oil composition / alpha-cadinol / delta-cadinene / gamma-cadinene / cadina-3,9-dieneSource:
Journal of Essential Oil Research, 2010, 22, 2, 143-146Publisher:
- Allured Publ Corp, Carol Stream
DOI: 10.1080/10412905.2010.9700287
ISSN: 1041-2905
WoS: 000275213100016
Scopus: 2-s2.0-77950404645
Collections
Institution/Community
Hemijski fakultet / Faculty of ChemistryTY - JOUR AU - Petrović, Lidija AU - Lepojevic, Zika AU - Sovilj, Verica AU - Adamović, Dušan AU - Tešević, Vele PY - 2010 UR - https://cherry.chem.bg.ac.rs/handle/123456789/1056 AB - Essential oil content of tubular, head and ligulate flowers of Calendula officinalis L. were determined using official steam distillation procedure. It was found that the ligulate flower sample had the highest oil content (0.16%). Applying SFE by means of CO2 (200 bar, 40 degrees C, 3 h extraction time), the highest extraction yield was found in tubular and ligulate flower samples (3.67% and 3.64%). Head flower had a lower extraction yield (2.60%) as the result of relatively small content of fatty oil, waxes and resins present in plant material. Steam distillation procedure was applied to obtain essential oils from the CO2 extracts devoid from cuticular waxes and resins. The compositions of oils were determined by GC and GC/MS. The main compounds of all investigated oils were alpha-cadinol (11.7-29.1%), delta-cadinene (3.2-20.3%), gamma-cadinene (1.5-11.4%) and cadina-3,9-diene (0.4-11.2%). The oil samples obtained from the CO2 extracts were found to be more complex containing alpha-gurjunene, beta-caryophyllene, beta-gurjunene, cis-muurola-4(14)-5-diene and alpha-humulene. PB - Allured Publ Corp, Carol Stream T2 - Journal of Essential Oil Research T1 - Composition of Essential Oil Obtained From Tubular, Head and Ligulate Flowers of Calendula officinalis L. by Steam Distillation of Plant Material and CO2 Extracts VL - 22 IS - 2 SP - 143 EP - 146 DO - 10.1080/10412905.2010.9700287 ER -
@article{ author = "Petrović, Lidija and Lepojevic, Zika and Sovilj, Verica and Adamović, Dušan and Tešević, Vele", year = "2010", abstract = "Essential oil content of tubular, head and ligulate flowers of Calendula officinalis L. were determined using official steam distillation procedure. It was found that the ligulate flower sample had the highest oil content (0.16%). Applying SFE by means of CO2 (200 bar, 40 degrees C, 3 h extraction time), the highest extraction yield was found in tubular and ligulate flower samples (3.67% and 3.64%). Head flower had a lower extraction yield (2.60%) as the result of relatively small content of fatty oil, waxes and resins present in plant material. Steam distillation procedure was applied to obtain essential oils from the CO2 extracts devoid from cuticular waxes and resins. The compositions of oils were determined by GC and GC/MS. The main compounds of all investigated oils were alpha-cadinol (11.7-29.1%), delta-cadinene (3.2-20.3%), gamma-cadinene (1.5-11.4%) and cadina-3,9-diene (0.4-11.2%). The oil samples obtained from the CO2 extracts were found to be more complex containing alpha-gurjunene, beta-caryophyllene, beta-gurjunene, cis-muurola-4(14)-5-diene and alpha-humulene.", publisher = "Allured Publ Corp, Carol Stream", journal = "Journal of Essential Oil Research", title = "Composition of Essential Oil Obtained From Tubular, Head and Ligulate Flowers of Calendula officinalis L. by Steam Distillation of Plant Material and CO2 Extracts", volume = "22", number = "2", pages = "143-146", doi = "10.1080/10412905.2010.9700287" }
Petrović, L., Lepojevic, Z., Sovilj, V., Adamović, D.,& Tešević, V.. (2010). Composition of Essential Oil Obtained From Tubular, Head and Ligulate Flowers of Calendula officinalis L. by Steam Distillation of Plant Material and CO2 Extracts. in Journal of Essential Oil Research Allured Publ Corp, Carol Stream., 22(2), 143-146. https://doi.org/10.1080/10412905.2010.9700287
Petrović L, Lepojevic Z, Sovilj V, Adamović D, Tešević V. Composition of Essential Oil Obtained From Tubular, Head and Ligulate Flowers of Calendula officinalis L. by Steam Distillation of Plant Material and CO2 Extracts. in Journal of Essential Oil Research. 2010;22(2):143-146. doi:10.1080/10412905.2010.9700287 .
Petrović, Lidija, Lepojevic, Zika, Sovilj, Verica, Adamović, Dušan, Tešević, Vele, "Composition of Essential Oil Obtained From Tubular, Head and Ligulate Flowers of Calendula officinalis L. by Steam Distillation of Plant Material and CO2 Extracts" in Journal of Essential Oil Research, 22, no. 2 (2010):143-146, https://doi.org/10.1080/10412905.2010.9700287 . .