The influence of long term soft milling of a mixture of (1) Mg(OH)(2) and alpha-Fe2O3 and (2) Mg(OH)(2) and Fe(OH)(3) powders in a planetary ball mill on the reaction synthesis of nanosized MgFe2O4 ferrites was studied. Soft mechanochemical reaction leading to formation of the MgFe2O4 spinel phase was followed by scanning electron microscopy, transmission electron microscopy, X-ray diffraction and magnetisation measurements. The spinel phase formation was first observed after 5 h of milling and its formation was completed after 15 h in case (2). The synthesised MgFe2O4 ferrite had a nanocrystalline structure with a crystallite size of about 10 and 15 nm respectively for cases (1) and (2). Measurements after 15 h of milling show magnetisation values of 15.23 and 10.14 J T-1 kg(-1) respectively for cases (1) and (2).
TY - JOUR
AU - Pavlović, Miodrag B.
AU - Jovalekic, C.
AU - Nikolić, Aleksandar S.
AU - Manojlović, Dragan D.
AU - Šojić, Nešo
PY - 2010
UR - https://cherry.chem.bg.ac.rs/handle/123456789/1115
AB - The influence of long term soft milling of a mixture of (1) Mg(OH)(2) and alpha-Fe2O3 and (2) Mg(OH)(2) and Fe(OH)(3) powders in a planetary ball mill on the reaction synthesis of nanosized MgFe2O4 ferrites was studied. Soft mechanochemical reaction leading to formation of the MgFe2O4 spinel phase was followed by scanning electron microscopy, transmission electron microscopy, X-ray diffraction and magnetisation measurements. The spinel phase formation was first observed after 5 h of milling and its formation was completed after 15 h in case (2). The synthesised MgFe2O4 ferrite had a nanocrystalline structure with a crystallite size of about 10 and 15 nm respectively for cases (1) and (2). Measurements after 15 h of milling show magnetisation values of 15.23 and 10.14 J T-1 kg(-1) respectively for cases (1) and (2).
PB - Maney Publishing, Leeds
T2 - Materials Science and Technology
T1 - Soft mechanochemical synthesis of MgFe2O4 nanoparticles from the mixture of alpha-Fe2O3 with Mg(OH)(2) and Fe(OH)(3) with Mg(OH)(2)
VL - 26
IS - 8
SP - 968
EP - 974
DO - 10.1179/174328409X415020
UR - Kon_2115
ER -
@article{
author = "Pavlović, Miodrag B. and Jovalekic, C. and Nikolić, Aleksandar S. and Manojlović, Dragan D. and Šojić, Nešo",
year = "2010",
abstract = "The influence of long term soft milling of a mixture of (1) Mg(OH)(2) and alpha-Fe2O3 and (2) Mg(OH)(2) and Fe(OH)(3) powders in a planetary ball mill on the reaction synthesis of nanosized MgFe2O4 ferrites was studied. Soft mechanochemical reaction leading to formation of the MgFe2O4 spinel phase was followed by scanning electron microscopy, transmission electron microscopy, X-ray diffraction and magnetisation measurements. The spinel phase formation was first observed after 5 h of milling and its formation was completed after 15 h in case (2). The synthesised MgFe2O4 ferrite had a nanocrystalline structure with a crystallite size of about 10 and 15 nm respectively for cases (1) and (2). Measurements after 15 h of milling show magnetisation values of 15.23 and 10.14 J T-1 kg(-1) respectively for cases (1) and (2).",
publisher = "Maney Publishing, Leeds",
journal = "Materials Science and Technology",
title = "Soft mechanochemical synthesis of MgFe2O4 nanoparticles from the mixture of alpha-Fe2O3 with Mg(OH)(2) and Fe(OH)(3) with Mg(OH)(2)",
volume = "26",
number = "8",
pages = "968-974",
doi = "10.1179/174328409X415020",
url = "Kon_2115"
}
Pavlović, M. B., Jovalekic, C., Nikolić, A. S., Manojlović, D. D.,& Šojić, N.. (2010). Soft mechanochemical synthesis of MgFe2O4 nanoparticles from the mixture of alpha-Fe2O3 with Mg(OH)(2) and Fe(OH)(3) with Mg(OH)(2). in Materials Science and Technology
Maney Publishing, Leeds., 26(8), 968-974.
https://doi.org/10.1179/174328409X415020
Kon_2115
Pavlović MB, Jovalekic C, Nikolić AS, Manojlović DD, Šojić N. Soft mechanochemical synthesis of MgFe2O4 nanoparticles from the mixture of alpha-Fe2O3 with Mg(OH)(2) and Fe(OH)(3) with Mg(OH)(2). in Materials Science and Technology. 2010;26(8):968-974.
doi:10.1179/174328409X415020
Kon_2115 .
Pavlović, Miodrag B., Jovalekic, C., Nikolić, Aleksandar S., Manojlović, Dragan D., Šojić, Nešo, "Soft mechanochemical synthesis of MgFe2O4 nanoparticles from the mixture of alpha-Fe2O3 with Mg(OH)(2) and Fe(OH)(3) with Mg(OH)(2)" in Materials Science and Technology, 26, no. 8 (2010):968-974,
https://doi.org/10.1179/174328409X415020 .,
Kon_2115 .
