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Synthesis and characterization of palladium(II) complexes with glycine coumarin derivatives

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2016
2390.pdf (820.1Kb)
Authors
Stojković, Danijela
Bacchi, Alessia
Capucci, Davide
Milenković, Milica R.
Čobeljić, Božidar
Trifunović, Srećko R.
Anđelković, Katarina K.
Jevtic, Verica V.
Vuković, Nenad L.
Vukic, Milena
Sladić, Dušan
Article (Published version)
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Abstract
A Pd(II) complex with methyl 2-([1-{2,4-dioxochroman-3-ylidene}ethyl]amino)acetate was synthesized. The structures of both the ligand and its Pd(II) complex were determined by elemental analysis, and IR and NMR spectroscopy. Recrystallization of the Pd(II) complex from DMF/water solution resulted in its hydrolysis and the formation of the dimethylamine (2-[{1-(2,4-dioxochroman-3-ylidene) ethyl} amino] acetato) palladium(II) complex, the structure of which was determined by elemental analysis, IR, H-1- and C-13-NMR spectroscopy and X-ray analysis.
Keywords:
coumarin-derived ligands / crystal structure / mechanism of hydrolysis
Source:
Journal of the Serbian Chemical Society, 2016, 81, 12, 1383-1392
Publisher:
  • Serbian Chemical Soc, Belgrade
Projects:
  • Interactions of natural products, their derivatives and coordination compounds with proteins and nucleic acids (RS-172055)
  • Synthesis, modeling, physicochemical and biological properties of organic compounds and related metal complexes (RS-172016)
Note:
  • Supplementary material: http://cherry.chem.bg.ac.rs/handle/123456789/3626

DOI: 10.2298/JSC160915087S

ISSN: 0352-5139

WoS: 000392946100005

Scopus: 2-s2.0-85009841653
[ Google Scholar ]
URI
http://cherry.chem.bg.ac.rs/handle/123456789/2392
Collections
  • Publikacije
Institution
Hemijski fakultet
TY  - JOUR
AU  - Stojković, Danijela
AU  - Bacchi, Alessia
AU  - Capucci, Davide
AU  - Milenković, Milica R.
AU  - Čobeljić, Božidar
AU  - Trifunović, Srećko R.
AU  - Anđelković, Katarina K.
AU  - Jevtic, Verica V.
AU  - Vuković, Nenad L.
AU  - Vukic, Milena
AU  - Sladić, Dušan
PY  - 2016
UR  - http://cherry.chem.bg.ac.rs/handle/123456789/2392
AB  - A Pd(II) complex with methyl 2-([1-{2,4-dioxochroman-3-ylidene}ethyl]amino)acetate was synthesized. The structures of both the ligand and its Pd(II) complex were determined by elemental analysis, and IR and NMR spectroscopy. Recrystallization of the Pd(II) complex from DMF/water solution resulted in its hydrolysis and the formation of the dimethylamine (2-[{1-(2,4-dioxochroman-3-ylidene) ethyl} amino] acetato) palladium(II) complex, the structure of which was determined by elemental analysis, IR, H-1- and C-13-NMR spectroscopy and X-ray analysis.
PB  - Serbian Chemical Soc, Belgrade
T2  - Journal of the Serbian Chemical Society
T1  - Synthesis and characterization of palladium(II) complexes with glycine coumarin derivatives
VL  - 81
IS  - 12
SP  - 1383
EP  - 1392
DO  - 10.2298/JSC160915087S
ER  - 
@article{
author = "Stojković, Danijela and Bacchi, Alessia and Capucci, Davide and Milenković, Milica R. and Čobeljić, Božidar and Trifunović, Srećko R. and Anđelković, Katarina K. and Jevtic, Verica V. and Vuković, Nenad L. and Vukic, Milena and Sladić, Dušan",
year = "2016",
url = "http://cherry.chem.bg.ac.rs/handle/123456789/2392",
abstract = "A Pd(II) complex with methyl 2-([1-{2,4-dioxochroman-3-ylidene}ethyl]amino)acetate was synthesized. The structures of both the ligand and its Pd(II) complex were determined by elemental analysis, and IR and NMR spectroscopy. Recrystallization of the Pd(II) complex from DMF/water solution resulted in its hydrolysis and the formation of the dimethylamine (2-[{1-(2,4-dioxochroman-3-ylidene) ethyl} amino] acetato) palladium(II) complex, the structure of which was determined by elemental analysis, IR, H-1- and C-13-NMR spectroscopy and X-ray analysis.",
publisher = "Serbian Chemical Soc, Belgrade",
journal = "Journal of the Serbian Chemical Society",
title = "Synthesis and characterization of palladium(II) complexes with glycine coumarin derivatives",
volume = "81",
number = "12",
pages = "1383-1392",
doi = "10.2298/JSC160915087S"
}
Stojković D, Bacchi A, Capucci D, Milenković MR, Čobeljić B, Trifunović SR, Anđelković KK, Jevtic VV, Vuković NL, Vukic M, Sladić D. Synthesis and characterization of palladium(II) complexes with glycine coumarin derivatives. Journal of the Serbian Chemical Society. 2016;81(12):1383-1392
Stojković, D., Bacchi, A., Capucci, D., Milenković, M. R., Čobeljić, B., Trifunović, S. R., Anđelković, K. K., Jevtic, V. V., Vuković, N. L., Vukic, M.,& Sladić, D. (2016). Synthesis and characterization of palladium(II) complexes with glycine coumarin derivatives.
Journal of the Serbian Chemical SocietySerbian Chemical Soc, Belgrade., 81(12), 1383-1392.
https://doi.org/10.2298/JSC160915087S
Stojković Danijela, Bacchi Alessia, Capucci Davide, Milenković Milica R., Čobeljić Božidar, Trifunović Srećko R., Anđelković Katarina K., Jevtic Verica V., Vuković Nenad L., Vukic Milena, Sladić Dušan, "Synthesis and characterization of palladium(II) complexes with glycine coumarin derivatives" 81, no. 12 (2016):1383-1392,
https://doi.org/10.2298/JSC160915087S .

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