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Fullerene bisadduct regioisomers containing an asymmetric diamide tether

dc.creatorKop, Tatjana
dc.creatorPopović-Đorđević, Jelena
dc.creatorBjelaković, Mira S.
dc.creatorMilić, Dragana
dc.date.accessioned2018-11-22T00:41:44Z
dc.date.available2018-11-22T00:41:44Z
dc.date.issued2017
dc.identifier.issn0040-4020
dc.identifier.urihttps://cherry.chem.bg.ac.rs/handle/123456789/2565
dc.description.abstractFour macrocyclic bis(pyrrolidino)fullerene regioisomers with e-edge, e-face, trans-4 and cis-2 addition patterns were synthesized from the corresponding monoadduct by Prato's cycloaddition in a yield of 50%, and fully characterized by spectroscopic techniques. Bisadduct regioisomers were isolated easily in a pure form using dry-flash column chromatography. The relative ratio of the isolated regioisomers e-edge/e-face/trans-41cis-2 was 1.0:1.9:1.5:4.9. Morphology of self-assembled structures of the four bisadduct regioisomers in solution was characterized using scanning electron microscopy. (C) 2017 Elsevier Ltd. All rights reserved.en
dc.publisherPergamon-Elsevier Science Ltd, Oxford
dc.relationinfo:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172002/RS//
dc.rightsrestrictedAccess
dc.sourceTetrahedron
dc.subjectbis(pyrrolidino)fullerene regioisomersen
dc.subjectPrato's cycloadditionen
dc.subjectHexamethylene-Gly-Gaba diamide tetheren
dc.subjectNMR analysisen
dc.subjectSelf-orderingen
dc.titleFullerene bisadduct regioisomers containing an asymmetric diamide tetheren
dc.typearticle
dc.rights.licenseARR
dcterms.abstractБјелаковиц, Мира С.; Дордевиц, Јелена; Милић, Драгана; Коп, Татјана Ј.;
dc.citation.volume73
dc.citation.issue50
dc.citation.spage7073
dc.citation.epage7078
dc.identifier.wos000417664100011
dc.identifier.doi10.1016/j.tet.2017.10.069
dc.citation.other73(50): 7073-7078
dc.citation.rankM22
dc.description.otherSupplementary material: [http://cherry.chem.bg.ac.rs/handle/123456789/3011]
dc.type.versionpublishedVersionen
dc.identifier.scopus2-s2.0-85032815771


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