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One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles

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2020
One-pot_combustion_pub_2020.pdf (792.2Kb)
Аутори
Jeremić, Dejan
Anđelković, Ljubica
Milenković, Milica R.
Šuljagić, Marija
Šumar-Ristović, Maja
Ostojić, Sanja
Nikolić, Aleksandar S.
Vulić, Predrag
Brčeski, Ilija
Pavlović, Vladimir
Чланак у часопису (Објављена верзија)
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Апстракт
This work is the first report of a very simple and fast one-pot synthesis of nickel oxide (NiO) and hematite (α-Fe2O3) nanoparticles by thermal decomposition of transition metal aqua complexes with camphor sulfonate anions. Obtained nanopowders were characterized by X-ray powder diffraction, Fourier transform IR analysis, scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. X-ray powder diffraction confirmed the formation of high purity NiO and α-Fe2O3 crystal phases. In the case of α-Fe2O3, about five times larger average crystallite size was obtained. Fourier transform IR spectra of synthesized materials showed characteristic peaks for NiO and α-Fe2O3 nanostructures. To visualize the morphology and the chemical composition of the final products Scanning electron microscopy and Energy-dispersive X-ray spectroscopy were performed. The thermogravimetric analysis was done for a better understanding of the general thermal behavior of precursor compounds. This easy-to-pe...rform and fast preparation method opens a broad range of obtained materials’ usage, particularly due to its economic viability

Кључне речи:
Nanomaterials / Nickel oxide / Hematite / camphor sulfonates / One-pot synthesis
Извор:
Science of Sintering, 2020, 52, 4, 481-490
Пројекти:
  • Министарство просвете, науке и технолошког развоја Републике Србије, Уговор бр. 451-03-68/2020-14/200026 (Универзитет у Београду, Институт за хемију, технологију и металургију - ИХТМ) (RS-200026)
  • Министарство просвете, науке и технолошког развоја Републике Србије, Уговор бр. 451-03-68/2020-14/200168 (Универзитет у Београду, Хемијски факултет) (RS-200168)
  • Министарство просвете, науке и технолошког развоја Републике Србије, Уговор бр. 451-03-68/2020-14/200168 (Универзитет у Београду, Хемијски факултет) (RS-200168)
  • Министарство просвете, науке и технолошког развоја Републике Србије, Уговор бр. 451-03-68/2020-14/200116 (Универзитет у Београду, Пољопривредни факултет) (RS-200116)

DOI: 10.2298/SOS2004481J

ISSN: 0350-820X

WoS: 000600505000009

Scopus: 2-s2.0-85098651318
[ Google Scholar ]
URI
http://cherry.chem.bg.ac.rs/handle/123456789/4306
Колекције
  • Publikacije
  • Publikacije
Институција
Hemijski fakultet
TY  - JOUR
AU  - Jeremić, Dejan
AU  - Anđelković, Ljubica
AU  - Milenković, Milica R.
AU  - Šuljagić, Marija
AU  - Šumar-Ristović, Maja
AU  - Ostojić, Sanja
AU  - Nikolić, Aleksandar S.
AU  - Vulić, Predrag
AU  - Brčeski, Ilija
AU  - Pavlović, Vladimir
PY  - 2020
UR  - http://cherry.chem.bg.ac.rs/handle/123456789/4306
AB  - This work is the first report of a very simple and fast one-pot synthesis of nickel oxide (NiO) and hematite (α-Fe2O3) nanoparticles by thermal decomposition of transition metal aqua complexes with camphor sulfonate anions. Obtained nanopowders were characterized by X-ray powder diffraction, Fourier transform IR analysis, scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. X-ray powder diffraction confirmed the formation of high purity NiO and α-Fe2O3 crystal phases. In the case of α-Fe2O3, about five times larger average crystallite size was obtained. Fourier transform IR spectra of synthesized materials showed characteristic peaks for NiO and α-Fe2O3 nanostructures. To visualize the morphology and the chemical composition of the final products Scanning electron microscopy and Energy-dispersive X-ray spectroscopy were performed. The thermogravimetric analysis was done for a better understanding of the general thermal behavior of precursor compounds. This easy-to-perform and fast preparation method opens a broad range of obtained materials’ usage, particularly due to its economic viability
T2  - Science of Sintering
T1  - One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles
VL  - 52
IS  - 4
SP  - 481
EP  - 490
DO  - 10.2298/SOS2004481J
ER  - 
@article{
author = "Jeremić, Dejan and Anđelković, Ljubica and Milenković, Milica R. and Šuljagić, Marija and Šumar-Ristović, Maja and Ostojić, Sanja and Nikolić, Aleksandar S. and Vulić, Predrag and Brčeski, Ilija and Pavlović, Vladimir",
year = "2020",
url = "http://cherry.chem.bg.ac.rs/handle/123456789/4306",
abstract = "This work is the first report of a very simple and fast one-pot synthesis of nickel oxide (NiO) and hematite (α-Fe2O3) nanoparticles by thermal decomposition of transition metal aqua complexes with camphor sulfonate anions. Obtained nanopowders were characterized by X-ray powder diffraction, Fourier transform IR analysis, scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. X-ray powder diffraction confirmed the formation of high purity NiO and α-Fe2O3 crystal phases. In the case of α-Fe2O3, about five times larger average crystallite size was obtained. Fourier transform IR spectra of synthesized materials showed characteristic peaks for NiO and α-Fe2O3 nanostructures. To visualize the morphology and the chemical composition of the final products Scanning electron microscopy and Energy-dispersive X-ray spectroscopy were performed. The thermogravimetric analysis was done for a better understanding of the general thermal behavior of precursor compounds. This easy-to-perform and fast preparation method opens a broad range of obtained materials’ usage, particularly due to its economic viability",
journal = "Science of Sintering",
title = "One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles",
volume = "52",
number = "4",
pages = "481-490",
doi = "10.2298/SOS2004481J"
}
Jeremić D, Anđelković L, Milenković MR, Šuljagić M, Šumar-Ristović M, Ostojić S, Nikolić AS, Vulić P, Brčeski I, Pavlović V. One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles. Science of Sintering. 2020;52(4):481-490
Jeremić, D., Anđelković, L., Milenković, M. R., Šuljagić, M., Šumar-Ristović, M., Ostojić, S., Nikolić, A. S., Vulić, P., Brčeski, I.,& Pavlović, V. (2020). One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles.
Science of Sintering, 52(4), 481-490.
https://doi.org/10.2298/SOS2004481J
Jeremić Dejan, Anđelković Ljubica, Milenković Milica R., Šuljagić Marija, Šumar-Ristović Maja, Ostojić Sanja, Nikolić Aleksandar S., Vulić Predrag, Brčeski Ilija, Pavlović Vladimir, "One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles" 52, no. 4 (2020):481-490,
https://doi.org/10.2298/SOS2004481J .

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