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dc.creatorJeremić, Dejan
dc.creatorAnđelković, Ljubica
dc.creatorMilenković, Milica R.
dc.creatorŠuljagić, Marija
dc.creatorŠumar-Ristović, Maja
dc.creatorOstojić, Sanja
dc.creatorNikolić, Aleksandar S.
dc.creatorVulić, Predrag
dc.creatorBrčeski, Ilija
dc.creatorPavlović, Vladimir
dc.date.accessioned2021-01-20T22:51:54Z
dc.date.available2021-01-20T22:51:54Z
dc.date.issued2020
dc.identifier.issn0350-820X
dc.identifier.urihttp://cherry.chem.bg.ac.rs/handle/123456789/4306
dc.description.abstractThis work is the first report of a very simple and fast one-pot synthesis of nickel oxide (NiO) and hematite (α-Fe2O3) nanoparticles by thermal decomposition of transition metal aqua complexes with camphor sulfonate anions. Obtained nanopowders were characterized by X-ray powder diffraction, Fourier transform IR analysis, scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. X-ray powder diffraction confirmed the formation of high purity NiO and α-Fe2O3 crystal phases. In the case of α-Fe2O3, about five times larger average crystallite size was obtained. Fourier transform IR spectra of synthesized materials showed characteristic peaks for NiO and α-Fe2O3 nanostructures. To visualize the morphology and the chemical composition of the final products Scanning electron microscopy and Energy-dispersive X-ray spectroscopy were performed. The thermogravimetric analysis was done for a better understanding of the general thermal behavior of precursor compounds. This easy-to-perform and fast preparation method opens a broad range of obtained materials’ usage, particularly due to its economic viability
dc.relationinfo:eu-repo/grantAgreement/MESTD/inst-2020/200026/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/inst-2020/200168/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/inst-2020/200168/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/inst-2020/200116/RS//
dc.rightsopenAccess
dc.sourceScience of Sintering
dc.subjectNanomaterials
dc.subjectNickel oxide
dc.subjectHematite
dc.subjectcamphor sulfonates
dc.subjectOne-pot synthesis
dc.titleOne-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles
dc.typearticleen
dc.rights.licenseBY
dcterms.abstractШумар-Ристовић, Маја; Брчески, Илија; Јеремић, Дејан; Aнђелковић, Љубица; Миленковић, Милица Р.; Шуљагић, Марија; Павловић, Владимир; Николић, Aлександар С.; Вулић, Предраг; Остојић, Сања;
dc.citation.volume52
dc.citation.issue4
dc.citation.spage481
dc.citation.epage490
dc.identifier.wos000600505000009
dc.identifier.doi10.2298/SOS2004481J
dc.citation.rankM22~
dc.type.versionpublishedVersion
dc.identifier.scopus2-s2.0-85098651318
dc.identifier.fulltexthttp://cherry.chem.bg.ac.rs/bitstream/id/26537/One-pot_combustion_pub_2020.pdf


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