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Determination of metal content in some herbal drugs - Empirical and chemometric approach

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2005
Authors
Razic, S
Onjia, Antonije E.
Dogo, S
Slavković, Latinka
Popović, Aleksandar R.
Article (Published version)
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Abstract
The concentrations of Cu, Zn, Mn, Fe, K, Ca, Mg, Al, Ba and B in 26 herbal drugs of special importance in phytopharmacywere studied. Flame atomic absorption and emission spectrometry (FAAS, FAES), as well as inductively coupled plasma atomic emission spectrometry (ICP-AES), were applied in this work. The whole procedure, from sample preparation, via dissolution, to measurements, was validated by using CRM (NIST 1573a-tomato leaves), and the obtained recovery values are in the range from 91 to 102%. Drug samples originated from medicinal plants cultivated in Serbia contained Cu (4.47-14.08 mg kg(-1)), Zn (8.4-54.5 mg kg(-1)), Mn (9-155 mg kg(-1)), Fe (47-546 mg kg(-1)), K (0.20-6.24%), Ca (0.18-1.84%), Mg (0.13-1.09%), Al (16-416 mg kg(-1)), Ba (11.70-84.83 mg kg(-1)) and B (5.1-118.7 mg kg(-1)). In order to get a better insight into the elemental patterns, a common chemometric approach to data evaluation was used. Four significant factors identified by principal component analysis (PCA...) were attributed partly to the significant influential sources and high mobility of some elements thus referring to potential anthropogenic contamination as well. (C) 2005 Elsevier B.V. All rights reserved.

Keywords:
herbal drugs / trace elements / AAS / AES / chemometrics / PCA
Source:
Talanta, 2005, 67, 1, 233-239
Publisher:
  • Elsevier Science Bv, Amsterdam

DOI: 10.1016/j.talanta.2005.03.023

ISSN: 0039-9140

PubMed: 18970161

WoS: 000230528500031

Scopus: 2-s2.0-21344461513
[ Google Scholar ]
85
65
URI
https://cherry.chem.bg.ac.rs/handle/123456789/720
Collections
  • Publikacije / Publications
Institution/Community
Hemijski fakultet / Faculty of Chemistry
TY  - JOUR
AU  - Razic, S
AU  - Onjia, Antonije E.
AU  - Dogo, S
AU  - Slavković, Latinka
AU  - Popović, Aleksandar R.
PY  - 2005
UR  - https://cherry.chem.bg.ac.rs/handle/123456789/720
AB  - The concentrations of Cu, Zn, Mn, Fe, K, Ca, Mg, Al, Ba and B in 26 herbal drugs of special importance in phytopharmacywere studied. Flame atomic absorption and emission spectrometry (FAAS, FAES), as well as inductively coupled plasma atomic emission spectrometry (ICP-AES), were applied in this work. The whole procedure, from sample preparation, via dissolution, to measurements, was validated by using CRM (NIST 1573a-tomato leaves), and the obtained recovery values are in the range from 91 to 102%. Drug samples originated from medicinal plants cultivated in Serbia contained Cu (4.47-14.08 mg kg(-1)), Zn (8.4-54.5 mg kg(-1)), Mn (9-155 mg kg(-1)), Fe (47-546 mg kg(-1)), K (0.20-6.24%), Ca (0.18-1.84%), Mg (0.13-1.09%), Al (16-416 mg kg(-1)), Ba (11.70-84.83 mg kg(-1)) and B (5.1-118.7 mg kg(-1)). In order to get a better insight into the elemental patterns, a common chemometric approach to data evaluation was used. Four significant factors identified by principal component analysis (PCA) were attributed partly to the significant influential sources and high mobility of some elements thus referring to potential anthropogenic contamination as well. (C) 2005 Elsevier B.V. All rights reserved.
PB  - Elsevier Science Bv, Amsterdam
T2  - Talanta
T1  - Determination of metal content in some herbal drugs - Empirical and chemometric approach
VL  - 67
IS  - 1
SP  - 233
EP  - 239
DO  - 10.1016/j.talanta.2005.03.023
ER  - 
@article{
author = "Razic, S and Onjia, Antonije E. and Dogo, S and Slavković, Latinka and Popović, Aleksandar R.",
year = "2005",
abstract = "The concentrations of Cu, Zn, Mn, Fe, K, Ca, Mg, Al, Ba and B in 26 herbal drugs of special importance in phytopharmacywere studied. Flame atomic absorption and emission spectrometry (FAAS, FAES), as well as inductively coupled plasma atomic emission spectrometry (ICP-AES), were applied in this work. The whole procedure, from sample preparation, via dissolution, to measurements, was validated by using CRM (NIST 1573a-tomato leaves), and the obtained recovery values are in the range from 91 to 102%. Drug samples originated from medicinal plants cultivated in Serbia contained Cu (4.47-14.08 mg kg(-1)), Zn (8.4-54.5 mg kg(-1)), Mn (9-155 mg kg(-1)), Fe (47-546 mg kg(-1)), K (0.20-6.24%), Ca (0.18-1.84%), Mg (0.13-1.09%), Al (16-416 mg kg(-1)), Ba (11.70-84.83 mg kg(-1)) and B (5.1-118.7 mg kg(-1)). In order to get a better insight into the elemental patterns, a common chemometric approach to data evaluation was used. Four significant factors identified by principal component analysis (PCA) were attributed partly to the significant influential sources and high mobility of some elements thus referring to potential anthropogenic contamination as well. (C) 2005 Elsevier B.V. All rights reserved.",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "Talanta",
title = "Determination of metal content in some herbal drugs - Empirical and chemometric approach",
volume = "67",
number = "1",
pages = "233-239",
doi = "10.1016/j.talanta.2005.03.023"
}
Razic, S., Onjia, A. E., Dogo, S., Slavković, L.,& Popović, A. R.. (2005). Determination of metal content in some herbal drugs - Empirical and chemometric approach. in Talanta
Elsevier Science Bv, Amsterdam., 67(1), 233-239.
https://doi.org/10.1016/j.talanta.2005.03.023
Razic S, Onjia AE, Dogo S, Slavković L, Popović AR. Determination of metal content in some herbal drugs - Empirical and chemometric approach. in Talanta. 2005;67(1):233-239.
doi:10.1016/j.talanta.2005.03.023 .
Razic, S, Onjia, Antonije E., Dogo, S, Slavković, Latinka, Popović, Aleksandar R., "Determination of metal content in some herbal drugs - Empirical and chemometric approach" in Talanta, 67, no. 1 (2005):233-239,
https://doi.org/10.1016/j.talanta.2005.03.023 . .

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