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Synthesis, characterization and crystal structures of Ni(II) and Cu(I) complexes with the condensation product of 2-(diphenylphosphino)benzaldehyde and 1-hydrazinophthalazine
dc.creator | Milenković, Milica R. | |
dc.creator | Shcherbakov, Igor N. | |
dc.creator | Popov, Leonid D. | |
dc.creator | Levchenkov, Sergey I. | |
dc.creator | Borodkin, Sergey A. | |
dc.creator | Alexandrov, Grigory G. | |
dc.date.accessioned | 2019-07-16T15:04:19Z | |
dc.date.available | 2017-10-08 | |
dc.date.issued | 2017 | |
dc.identifier.issn | 0277-5387 | |
dc.identifier.uri | https://cherry.chem.bg.ac.rs/handle/123456789/3256 | |
dc.description.abstract | A square-pyramidal Ni(II) complex (1) with the composition [NiL(HL')]CIO4 center dot H2O was synthesized in the reaction of nickel(II) perchlorate and 2[2-(diphenylphosphino)benzylidene]-1-phthalazinylhydrazone (HL). The coordination surrounding the Ni(II) ion consist of a PNN coordinated deprotonated HL ligand and its corresponding oxidation product phosphine oxide HL' coordinated via two nitrogen atoms of the hydrazinophthalazine moiety. The structure of Ni(II) complex 1 was determined by X-ray analysis, IR spectroscopy, elemental analysis and magnetic measurements. In the reaction of copper(II) perchlorate with HL, a binuclear phthalazine bridged Cu(I) complex (2) was obtained with the composition [Cu-2(HL)(2)](ClO4)(2)center dot C2H5OH. The structure of Cu(I) complex 2 was determined by X-ray analysis, IR and NMR spectroscopy, elethental analysis and magnetic measurements. | |
dc.publisher | Pergamon-Elsevier Science Ltd, Oxford | |
dc.relation | SFedU [213.01-07-2014/03PChVG] | |
dc.rights | embargoedAccess | |
dc.rights.uri | https://creativecommons.org/licenses/by-nc-nd/4.0/ | |
dc.source | Polyhedron | |
dc.subject | 2-(Diphenylphosphino)benzaldehyde | |
dc.subject | Crystal structure | |
dc.subject | Cu(I) complex | |
dc.subject | Hydralazine | |
dc.subject | Ni(II) complex | |
dc.title | Synthesis, characterization and crystal structures of Ni(II) and Cu(I) complexes with the condensation product of 2-(diphenylphosphino)benzaldehyde and 1-hydrazinophthalazine | |
dc.type | article | |
dc.rights.license | BY-NC-ND | |
dcterms.abstract | Схцхербаков, Игор Н.; Бородкин, Сергеy A.; Миленковић, Милица Р.; Aлеxандров, Григорy Г.; Попов, Леонид Д.; Левцхенков, Сергеy И.; | |
dc.citation.volume | 121 | |
dc.citation.spage | 278 | |
dc.citation.epage | 284 | |
dc.identifier.wos | 000390626200035 | |
dc.identifier.doi | 10.1016/j.poly.2016.10.020 | |
dc.citation.rank | M22 | |
dc.description.other | This is the peer-reviewed version of the following article: Milenković, M.; Shcherbakov, I. N.; Popov, L. D.; Levchenkov, S. I.; Borodkin, S. A.; Alexandrov, G. G. Synthesis, Characterization and Crystal Structures of Ni(II) and Cu(I) Complexes with the Condensation Product of 2-(Diphenylphosphino)Benzaldehyde and 1Hydrazinophthalazine. Polyhedron 2017, 121, 278–284. [https://doi.org/10.1016/j.poly.2016.10.020] | |
dc.description.other | Supplementary material: [http://cherry.chem.bg.ac.rs/handle/123456789/3257] | |
dc.type.version | acceptedVersion | |
dc.identifier.scopus | 2-s2.0-85004019027 | |
dc.identifier.fulltext | https://cherry.chem.bg.ac.rs/bitstream/id/8133/10.1016@j.poly.2016.10.020.pdf |