Determination of iodide and bromide by flow methods with amperometric detection
Samo za registrovane korisnike
2008
Članak u časopisu (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
Determination of bromide and iodide in real samples (water, pharmaceutical preparations, and biological material) was performed using modified flow injection analyses (FIA) with amperometric detection on platinum electrode. As an additional confirmation of FIA experiments, cyclic voltammetry was employed. Iodide was determined by the kinetic method, its limit of detection was 1.0 nM, and the linearity was 0.1-100 mu M. The limit of detection for bromide determination was 50.0 nM and the calibration was linear for 2.5-100 mu M and 0.1-10 mM. The relative standard deviation for 1 mu M of iodide was 3.03% and, for 5 mu M of bromide, it was 1.23% (n = 6). Both methods enable 60 analyses per hour to be performed.
Izvor:
Journal of Analytical Chemistry, 2008, 63, 9, 907-913Izdavač:
- Maik Nauka/Interperiodica/Springer, New York
DOI: 10.1134/S1061934808090207
ISSN: 1061-9348
WoS: 000258613900020
Scopus: 2-s2.0-50149086748
Kolekcije
Institucija/grupa
Hemijski fakultet / Faculty of ChemistryTY - JOUR AU - Mutić, Jelena AU - Nikolić-Mandić, Snežana D. AU - Lolić, Aleksandar AU - Manojlović, Dragan D. PY - 2008 UR - https://cherry.chem.bg.ac.rs/handle/123456789/964 AB - Determination of bromide and iodide in real samples (water, pharmaceutical preparations, and biological material) was performed using modified flow injection analyses (FIA) with amperometric detection on platinum electrode. As an additional confirmation of FIA experiments, cyclic voltammetry was employed. Iodide was determined by the kinetic method, its limit of detection was 1.0 nM, and the linearity was 0.1-100 mu M. The limit of detection for bromide determination was 50.0 nM and the calibration was linear for 2.5-100 mu M and 0.1-10 mM. The relative standard deviation for 1 mu M of iodide was 3.03% and, for 5 mu M of bromide, it was 1.23% (n = 6). Both methods enable 60 analyses per hour to be performed. PB - Maik Nauka/Interperiodica/Springer, New York T2 - Journal of Analytical Chemistry T1 - Determination of iodide and bromide by flow methods with amperometric detection VL - 63 IS - 9 SP - 907 EP - 913 DO - 10.1134/S1061934808090207 ER -
@article{ author = "Mutić, Jelena and Nikolić-Mandić, Snežana D. and Lolić, Aleksandar and Manojlović, Dragan D.", year = "2008", abstract = "Determination of bromide and iodide in real samples (water, pharmaceutical preparations, and biological material) was performed using modified flow injection analyses (FIA) with amperometric detection on platinum electrode. As an additional confirmation of FIA experiments, cyclic voltammetry was employed. Iodide was determined by the kinetic method, its limit of detection was 1.0 nM, and the linearity was 0.1-100 mu M. The limit of detection for bromide determination was 50.0 nM and the calibration was linear for 2.5-100 mu M and 0.1-10 mM. The relative standard deviation for 1 mu M of iodide was 3.03% and, for 5 mu M of bromide, it was 1.23% (n = 6). Both methods enable 60 analyses per hour to be performed.", publisher = "Maik Nauka/Interperiodica/Springer, New York", journal = "Journal of Analytical Chemistry", title = "Determination of iodide and bromide by flow methods with amperometric detection", volume = "63", number = "9", pages = "907-913", doi = "10.1134/S1061934808090207" }
Mutić, J., Nikolić-Mandić, S. D., Lolić, A.,& Manojlović, D. D.. (2008). Determination of iodide and bromide by flow methods with amperometric detection. in Journal of Analytical Chemistry Maik Nauka/Interperiodica/Springer, New York., 63(9), 907-913. https://doi.org/10.1134/S1061934808090207
Mutić J, Nikolić-Mandić SD, Lolić A, Manojlović DD. Determination of iodide and bromide by flow methods with amperometric detection. in Journal of Analytical Chemistry. 2008;63(9):907-913. doi:10.1134/S1061934808090207 .
Mutić, Jelena, Nikolić-Mandić, Snežana D., Lolić, Aleksandar, Manojlović, Dragan D., "Determination of iodide and bromide by flow methods with amperometric detection" in Journal of Analytical Chemistry, 63, no. 9 (2008):907-913, https://doi.org/10.1134/S1061934808090207 . .