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Synthesis of tribological WS 2 powder from WO 3 prepared by ultrasonic spray pyrolysis (USP)
dc.creator | Gajić, Nataša | |
dc.creator | Kamberović, Željko | |
dc.creator | Anđić, Zoran | |
dc.creator | Trpčevská, Jarmila | |
dc.creator | Plešingerova, Beatrice | |
dc.creator | Korać, Marija | |
dc.date.accessioned | 2019-04-05T16:32:02Z | |
dc.date.available | 2019-04-05T16:32:02Z | |
dc.date.issued | 2019 | |
dc.identifier.issn | 2075-4701 | |
dc.identifier.uri | https://cherry.chem.bg.ac.rs/handle/123456789/2868 | |
dc.description.abstract | This paper describes the synthesis of tungsten disulfide (WS 2 ) powder by the sulfurization of tungsten trioxide (WO 3 ) particles in the presence of additive potassium carbonate (K 2 CO 3 ) in nitrogen (N 2 ) atmosphere, first at lower temperature (200 ◦ C) and followed by reduction at higher temperature (900 ◦ C). In addition, the ultrasonic spray pyrolysis of ammonium meta-tungstate hydrate (AMT) was used for the production of WO 3 particles at 650 ◦ C in air. The HSC Chemistry® software package 9.0 was used for the analysis of chemistry and thermodynamic parameters of the processes for WS 2 powder synthesis. The crystalline structure and phase composition of all synthesized powders were analyzed by X-ray diffraction (XRD) measurements. The morphology and chemical composition of these samples were examined by scanning electron microscopy (SEM) combined with energy dispersive X-ray analysis (EDX). | |
dc.publisher | MDPI | |
dc.relation | info:eu-repo/grantAgreement/MESTD/Technological Development (TD or TR)/34033/RS// | |
dc.rights | openAccess | |
dc.rights.uri | https://creativecommons.org/licenses/by/4.0/ | |
dc.source | Metals | |
dc.subject | Tribology materials | |
dc.subject | Tungsten disulfide | |
dc.subject | Tungsten trioxide | |
dc.subject | Ultrasonic spray pyrolysis | |
dc.title | Synthesis of tribological WS 2 powder from WO 3 prepared by ultrasonic spray pyrolysis (USP) | |
dc.type | article | |
dc.rights.license | BY | |
dcterms.abstract | Гајић, Наташа; Aнђић, Зоран; Камберовић, Жељко; Трпчевскá, Јармила; Кораћ, Марија; Плешингерова, Беатрице; | |
dc.citation.volume | 9 | |
dc.citation.issue | 3 | |
dc.citation.spage | 1 | |
dc.citation.epage | 15 | |
dc.identifier.wos | 000464288600001 | |
dc.identifier.doi | 10.3390/met9030277 | |
dc.citation.rank | M21~ | |
dc.type.version | publishedVersion | |
dc.identifier.scopus | 2-s2.0-85063374905 | |
dc.identifier.fulltext | https://cherry.chem.bg.ac.rs/bitstream/id/6627/metals-09-00277-v2.pdf |