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An Fe(III) complex with the dianionic form of 2,6-diacetylpyridine bis(acylhydrazone). The crystal structure of [diaqua-2 ',2 ''-(2,6-pyridinediyldiethylidyne)dioxamo-hydrazide]iron(III) perchlorate trihydrate, [Fe(dapsox)(H2O)(2)]ClO4 center dot 3H(2)O
dc.creator | Anđelković, Katarina K. | |
dc.creator | Bacchi, Alessia | |
dc.creator | Pelizzi, G | |
dc.creator | Jeremić, Dejan | |
dc.creator | Ivanović-Burmazović, Ivana | |
dc.date.accessioned | 2018-11-22T00:05:18Z | |
dc.date.available | 2018-11-22T00:05:18Z | |
dc.date.issued | 2002 | |
dc.identifier.issn | 0095-8972 | |
dc.identifier.uri | https://cherry.chem.bg.ac.rs/handle/123456789/539 | |
dc.description.abstract | The title compound was prepared by a template synthesis from 2,6-diacetylpyridine, dioxamohydrazide and Fe(ClO4)(3) . 6H(2)O (mol ratio 1: 2: 1) in MeOH/H2O (3:1) solution and its structure determined by single-crystal X-ray diffraction; triclinic, space group P (1) over bar, a= 7.5186(7), b = 10.9730(9), c = 14.6110(10) Angstrom, alpha = 95.866(1), beta = 100.252(1), gamma = 92.895(1), z = 2. The polydentate ligand is coordinated as a dianionic pentadentate while water molecules occupy apical positions in the structure. This is the first example of a monomeric, pentagonal bipyramidal structure of an Fe(III) complex with a dianionic bis(acylhydrazone) derivative of 2,6-diacetylpyridine. | en |
dc.publisher | Taylor & Francis Ltd, Abingdon | |
dc.rights | restrictedAccess | |
dc.source | Journal of Coordination Chemistry | |
dc.subject | Fe(III) | en |
dc.subject | bis(acylhydrazone) | en |
dc.subject | X-ray structure | en |
dc.title | An Fe(III) complex with the dianionic form of 2,6-diacetylpyridine bis(acylhydrazone). The crystal structure of [diaqua-2 ',2 ''-(2,6-pyridinediyldiethylidyne)dioxamo-hydrazide]iron(III) perchlorate trihydrate, [Fe(dapsox)(H2O)(2)]ClO4 center dot 3H(2)O | en |
dc.type | article | |
dc.rights.license | ARR | |
dcterms.abstract | Јеремиц, Д; Ивановиц-Бурмазовиц, И; Пелиззи, Г; Aнђелковић, Катарина; Баццхи, A; | |
dc.citation.volume | 55 | |
dc.citation.issue | 12 | |
dc.citation.spage | 1385 | |
dc.citation.epage | 1392 | |
dc.identifier.wos | 000180964400003 | |
dc.identifier.doi | 10.1080/0095897021000058600 | |
dc.citation.other | 55(12): 1385-1392 | |
dc.citation.rank | M23 | |
dc.type.version | publishedVersion | en |
dc.identifier.scopus | 2-s2.0-0036975358 |
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